JPS579739A - Purification of methyl methacrylate - Google Patents
Purification of methyl methacrylateInfo
- Publication number
- JPS579739A JPS579739A JP8354280A JP8354280A JPS579739A JP S579739 A JPS579739 A JP S579739A JP 8354280 A JP8354280 A JP 8354280A JP 8354280 A JP8354280 A JP 8354280A JP S579739 A JPS579739 A JP S579739A
- Authority
- JP
- Japan
- Prior art keywords
- methyl methacrylate
- column
- methanol
- mixed solution
- layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 title abstract 5
- 238000000746 purification Methods 0.000 title abstract 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 15
- BHIWKHZACMWKOJ-UHFFFAOYSA-N methyl isobutyrate Chemical compound COC(=O)C(C)C BHIWKHZACMWKOJ-UHFFFAOYSA-N 0.000 abstract 6
- 239000011259 mixed solution Substances 0.000 abstract 4
- 229930195734 saturated hydrocarbon Natural products 0.000 abstract 4
- WDAXFOBOLVPGLV-UHFFFAOYSA-N isobutyric acid ethyl ester Natural products CCOC(=O)C(C)C WDAXFOBOLVPGLV-UHFFFAOYSA-N 0.000 abstract 3
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000002699 waste material Substances 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To remove both hydrocarbons and waste from the top of a rectifying column, by carrying out the rectification of mixed solution of methyl methacrylate containing methanol and methyl isobutyrate in such a way that specific saturated hydrocarbons are made to exist only in parts higher than the feed plate of the mixed solution.
CONSTITUTION: In carrying out the titled purification by rectifying a mixed solution containing methanol, methyl methacrylate, methyl isobutyrate, or, additionally water, 6W8C saturated hydrocarbons are made to exist only in parts higher than the feed plate of the mixed solution and the rectification is done, so that the saturated hydrocarbons, a small amount of methyl methacrylate, and the whole amount of methyl isobutyrate and methanol are distilled from the top of the column, and methyl methacrylate or it and water are recovered from the bottom of the column. The distillate from the top of the column is subjected to layer separation by a layer separating tank into a hydrocarbon layer and a methanol layer. The former is refluxed to the rectifying column, and the latter is distilled. The saturated hydrocarbon and part of methanol are recovered and returned to the two layer separating tank.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8354280A JPS579739A (en) | 1980-06-20 | 1980-06-20 | Purification of methyl methacrylate |
| EP81104673A EP0044409B1 (en) | 1980-06-20 | 1981-06-17 | Process for purifying methyl methacrylate |
| DE8181104673T DE3161884D1 (en) | 1980-06-20 | 1981-06-17 | Process for purifying methyl methacrylate |
| KR1019810002241A KR840001899B1 (en) | 1980-06-20 | 1981-06-19 | Purification Method of Methyl Methacrylate |
| US06/497,783 US4518462A (en) | 1980-06-20 | 1983-05-25 | Distillation process for purifying methyl methacrylate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8354280A JPS579739A (en) | 1980-06-20 | 1980-06-20 | Purification of methyl methacrylate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS579739A true JPS579739A (en) | 1982-01-19 |
| JPH0147454B2 JPH0147454B2 (en) | 1989-10-13 |
Family
ID=13805389
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP8354280A Granted JPS579739A (en) | 1980-06-20 | 1980-06-20 | Purification of methyl methacrylate |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS579739A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58203940A (en) * | 1982-05-25 | 1983-11-28 | Toagosei Chem Ind Co Ltd | Method for recovering methyl methacrylate |
| US5969178A (en) * | 1997-07-08 | 1999-10-19 | Asahi Kasei Kogyo Kabushiki Kaisha | Using methacrolein and methanol as dehydration and absorption agents during production of methyl methacrylate |
| WO2001010811A1 (en) * | 1998-02-09 | 2001-02-15 | Mitsubishi Rayon Co., Ltd. | Process for the preparation of methyl methacrylate |
| US6680405B1 (en) | 1998-02-09 | 2004-01-20 | Mitsubishi Rayon Co., Ltd. | Process for the preparation of methyl methacrylate |
| KR20180094937A (en) * | 2015-12-18 | 2018-08-24 | 다우 글로벌 테크놀로지스 엘엘씨 | Method for purifying methyl methacrylate |
| JP2018537465A (en) * | 2015-12-18 | 2018-12-20 | ローム アンド ハース カンパニーＲｏｈｍ Ａｎｄ Ｈａａｓ Ｃｏｍｐａｎｙ | Process for the purification of methyl methacrylate |
| WO2022244833A1 (en) * | 2021-05-20 | 2022-11-24 | 三菱ケミカル株式会社 | Monomer composition, methacrylic resin composition and resin molded body |
| WO2024075474A1 (en) * | 2022-10-04 | 2024-04-11 | 三菱ケミカル株式会社 | Particulate composition, coating material, ink, and adhesive |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6889322B1 (en) | 2020-09-30 | 2021-06-18 | 住友化学株式会社 | Composition |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS54106412A (en) * | 1978-02-08 | 1979-08-21 | Kyowa Yuka Kk | Method of purifying ester |
-
1980
- 1980-06-20 JP JP8354280A patent/JPS579739A/en active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS54106412A (en) * | 1978-02-08 | 1979-08-21 | Kyowa Yuka Kk | Method of purifying ester |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58203940A (en) * | 1982-05-25 | 1983-11-28 | Toagosei Chem Ind Co Ltd | Method for recovering methyl methacrylate |
| US5969178A (en) * | 1997-07-08 | 1999-10-19 | Asahi Kasei Kogyo Kabushiki Kaisha | Using methacrolein and methanol as dehydration and absorption agents during production of methyl methacrylate |
| WO2001010811A1 (en) * | 1998-02-09 | 2001-02-15 | Mitsubishi Rayon Co., Ltd. | Process for the preparation of methyl methacrylate |
| US6680405B1 (en) | 1998-02-09 | 2004-01-20 | Mitsubishi Rayon Co., Ltd. | Process for the preparation of methyl methacrylate |
| KR20180094937A (en) * | 2015-12-18 | 2018-08-24 | 다우 글로벌 테크놀로지스 엘엘씨 | Method for purifying methyl methacrylate |
| JP2018537465A (en) * | 2015-12-18 | 2018-12-20 | ローム アンド ハース カンパニーＲｏｈｍ Ａｎｄ Ｈａａｓ Ｃｏｍｐａｎｙ | Process for the purification of methyl methacrylate |
| JP2018537466A (en) * | 2015-12-18 | 2018-12-20 | ローム アンド ハース カンパニーＲｏｈｍ Ａｎｄ Ｈａａｓ Ｃｏｍｐａｎｙ | Process for the purification of methyl methacrylate |
| WO2022244833A1 (en) * | 2021-05-20 | 2022-11-24 | 三菱ケミカル株式会社 | Monomer composition, methacrylic resin composition and resin molded body |
| TWI845943B (en) * | 2021-05-20 | 2024-06-21 | 日商三菱化學股份有限公司 | Monomer composition, methacrylic resin composition and resin molded article |
| WO2024075474A1 (en) * | 2022-10-04 | 2024-04-11 | 三菱ケミカル株式会社 | Particulate composition, coating material, ink, and adhesive |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0147454B2 (en) | 1989-10-13 |
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