JPS58187155A - Food raw material and its preparation - Google Patents

Food raw material and its preparation

Info

Publication number
JPS58187155A
JPS58187155A JP57068707A JP6870782A JPS58187155A JP S58187155 A JPS58187155 A JP S58187155A JP 57068707 A JP57068707 A JP 57068707A JP 6870782 A JP6870782 A JP 6870782A JP S58187155 A JPS58187155 A JP S58187155A
Authority
JP
Japan
Prior art keywords
refuse
okara
solvent
fat
defatted
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP57068707A
Other languages
Japanese (ja)
Inventor
Tetsuhiko Maruyama
丸山 哲彦
Yoshiro Yamamoto
山本 良郎
Hiromichi Asano
浅野 紘道
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Meiji Dairies Corp
Original Assignee
Meiji Milk Products Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Meiji Milk Products Co Ltd filed Critical Meiji Milk Products Co Ltd
Priority to JP57068707A priority Critical patent/JPS58187155A/en
Publication of JPS58187155A publication Critical patent/JPS58187155A/en
Pending legal-status Critical Current

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Abstract

PURPOSE:To obtain a food raw material which is tasteless and odorless white powder having high water-retainability and excellent gelling property, and capable of highly absorbing perfumes and extracts, etc., by extracting dried bean-curd refuse with an organic solvent having fat-removing capability to extract the oil and fat from the refuse, removing the solvent from the refuse, and pulverizing the product. CONSTITUTION:Dried bean-curd refuse is extracted with an organic solvent having fat-removing capability (e.g. methyl alcohol, ethyl alcohol, n-hexane, etc.) to extract the oil and fat from the refuse. The solvent is removed from the refuse and the product is pulverized to obtain the objective material. The defatted bean-curd refuse is almost tasteless and odorless white powder having high water-retainability and gelling property, capable of highly absorbing perfumes and extracts, etc., and provided with excellent physical properties as a food raw material. For example, the material obtained by the extraction with an alcohol is a white odorless powder which can be added to all sort of foods. Especially, it contains a large amount of high-quality fibers, has strong swelling and water-retaining tendency, and when added to a food having delicate taste and flavor such as Japanese cakes, Western cakes, etc., increases the stiffness of the pastry and improves the processability without lowering the qualities of the cake.

Description

【発明の詳細な説明】 本発明はおからをオリ用した新規な食品素材並にその製
造方法を提供するものである。
DETAILED DESCRIPTION OF THE INVENTION The present invention provides a novel food material using okara and a method for producing the same.

おからは、豆腐大豆蛋白又は豆乳を製造する際副生する
澱物であLt=lIS食用として大部は家畜の飼料に供
されて来たものである。近時豆乳が健康飲料として脚光
をあびるに到り、その生産も急速に増加し、新規な用途
の開発が要望されている。
Okara is a by-product of starch produced during the production of tofu, soybean protein, or soymilk, and is edible (Lt=lIS), and most of it has been used as feed for livestock. In recent years, soy milk has come into the spotlight as a health drink, and its production is rapidly increasing, creating a demand for the development of new uses.

おからは原料、製造方法の差によりその組成を異にする
のが通常で、今その分析例を第1表に示す。
Okara usually has different compositions depending on the raw materials and manufacturing methods, and Table 1 shows an analysis example of this.

第1表 即ち、豆乳おからは豆腐おからにくらべ、たんはく質、
脂質の含量は少ないが糖質、繊維を多く含む傾向がある
Table 1 shows that soy milk okara has protein quality compared to tofu okara.
It has a low fat content, but tends to be high in carbohydrates and fiber.

上記おからは、何れの場合においても空気中の酸素によ
シ酸化され易い不飽和脂肪酸が高い脂質を含むため急速
に酸化し、生の状態でも乾燥の状態でも異臭があり、且
つ腐敗しやすいので保存性が悪い欠点がある。このため
、佳良なたんばく質を多量に含むにもかかわらず、食用
としての用途が極めて制限されている。
In either case, the okara mentioned above oxidizes rapidly because it contains a high amount of unsaturated fatty acids that are easily oxidized by oxygen in the air, and it has a strange odor both in its raw and dried state, and it is easily spoiled. Therefore, it has the disadvantage of poor storage stability. For this reason, even though it contains a large amount of high-quality protein, its use as food is extremely limited.

本発明は上記事情によシなされたもので、大量に排出さ
れるおからを食品製造原料に使用せんと研究を進めた結
果、前記悪臭は有機溶剤で抽出すれば除去できることを
発見し、おからを乾燥し。
The present invention was made in view of the above circumstances, and as a result of research into using okara, which is produced in large quantities, as a raw material for food production, it was discovered that the odor could be removed by extracting it with an organic solvent. Dry it.

有機溶剤で抽出し溶剤を除去して粉砕することにより解
決した。
The problem was solved by extraction with an organic solvent, removal of the solvent, and pulverization.

本発明の脱脂おからは、殆んど無味、無臭の白色粉末で
保水性が良く、ゲル形成能にも優れ香料やエキス等をよ
く吸収し、食品素材として極めて優れた物性を有するの
である。
The defatted okara of the present invention is an almost tasteless and odorless white powder with good water retention, excellent gel-forming ability, and good absorption of fragrances, extracts, etc., and has extremely excellent physical properties as a food material.

本発明に使用するおからは、前記した豆腐おから、豆乳
おからの外、分離蛋白製造時のおからを使用することが
でき、これらは通常80チ内外の水分を含み、そのま\
抽出に供すると浴斉j濃度を稀釈したり抽出効果を低下
さすので乾燥するl−喪がある。乾燥は火力乾燥天日乾
燥等の乾燥方法は倒れも採用できる。乾燥に際しては蛋
白変性を起こしたり、糖質の分解を伴うような高温はさ
けるべきで、通常原料おからを圧搾又は遠心分離して水
分を減少させ、これを回転式乾燥機、トンネル乾燥機或
いは棚式乾燥機等に入れ、200°C以下の熱風で乾燥
する。乾燥彼の水分は20%以下妙:適当で、好ましく
は3〜10%である。
In addition to the above-mentioned tofu okara and soy milk okara, the okara used in the present invention can be used as okara used in the production of separated protein.
When subjected to extraction, it dilutes the bath concentration and reduces the extraction effect, so there is a risk of drying. For drying, drying methods such as fire drying, sun drying, etc. can also be used. When drying, high temperatures that may cause protein denaturation or decomposition of carbohydrates should be avoided.Usually raw okara is compressed or centrifuged to reduce moisture, and then dried in a rotary dryer, tunnel dryer, or dryer. Place in a rack dryer, etc., and dry with hot air below 200°C. Dry moisture content is below 20%: suitable, preferably 3-10%.

次いで上記乾燥おからは、脱脂能をもつ有機溶剤、例え
ばn−ヘキサン、メチルアルコール、エチルアルコール
、エーテル等の溶剤で抽出する。
Next, the dried okara is extracted with an organic solvent having a degreasing ability, such as n-hexane, methyl alcohol, ethyl alcohol, and ether.

抽出により飽和、不飽和の油脂は大部分除去されるが、
完全に除去する必要はなく異臭が完全に除去される程度
とする。この結果、無臭の蛋白質、糖質、繊維分に富む
脱脂おからとなる。
Extraction removes most of the saturated and unsaturated fats and oils, but
It is not necessary to completely remove the odor, just enough to remove the odor completely. The result is odorless defatted okara rich in protein, carbohydrates, and fiber.

本発明者らの研究によると、抽出後のおからの組成は使
用する溶剤の種類により異なり、例えば第1表に示す乾
燥豆乳おからを使用し、n−へキサンとエタノールで抽
出を行うと第2表に示す組成の脱脂おからが得られる。
According to the research conducted by the present inventors, the composition of okara after extraction differs depending on the type of solvent used. For example, when dry soybean milk okara shown in Table 1 is used and extracted with n-hexane and ethanol, Defatted okara having the composition shown in Table 2 is obtained.

即ち、n−へキサンでは脂質が大部分除去されるが、そ
の他の成分は大きく変動しない。従って、脱脂おからの
収率も向上するが、エタノールで抽出すると脂質の外糖
質が相当量溶出する。このため、収量も低下するが、得
られた脱脂おからは高蛋白、高繊維となり、保水性が増
強されゲル形成能が一層強くなる。従って、有機溶剤の
選択は素材の使用目的によって決定し、必要にして充分
な抽出度が得られる程度とする。
That is, with n-hexane, most of the lipids are removed, but other components do not change significantly. Therefore, the yield of defatted okara is improved, but when extracted with ethanol, a considerable amount of exosaccharides from lipids are eluted. For this reason, although the yield is also lower, the obtained defatted okara has high protein and high fiber content, has enhanced water retention, and has an even stronger gel-forming ability. Therefore, the selection of the organic solvent is determined depending on the intended use of the material, and should be selected to the extent that a sufficient degree of extraction can be obtained as necessary.

前記有機溶剤による抽出は、バッチ式、連続式、向流式
、順流式等測れの抽出方法によってもよく、抽出を効率
よく行うためには溶剤の含水蓄を減少させたものが好ま
しい。従ってアルコールの如き水と任意に混合する溶剤
の場合は、アルコール濃度が60%以上、好ましくは9
0チ前後のものを使用するとよい。
The extraction with the organic solvent may be performed by a batch method, a continuous method, a countercurrent method, a forward flow method, etc., and in order to perform the extraction efficiently, it is preferable that the solvent has a reduced moisture content. Therefore, in the case of a solvent such as alcohol that is optionally mixed with water, the alcohol concentration is 60% or more, preferably 9.
It is best to use one around 0chi.

有機溶剤で抽出後の脱脂おからは、次いで溶剤を除去し
、食品への混入を防止する。通常抽出直後のおからは大
量の溶剤を含むので、先づ圧搾機、圧f器、遠心分離機
等を使用し、大部分の溶剤を分離し、該分離後は脱脂お
からに蒸気を直接吹き込んで溶剤を蒸発、溜去するか、
蒸気により間接加熱を行って溜去する。このようにして
溶剤’klV去した脱脂おからは通常脱脂前の水分に戻
り、白色の粉末となシ原料おからに特有の豆乳臭や脂質
の酸化による異臭は殆んど、或いは全くないものである
。従って、上記の脱脂おからはそのま\或いは更に粉砕
し、篩別、風速等の処理を+4どこして整粒すると食品
素材として好適となる。
After the defatted okara has been extracted with an organic solvent, the solvent is then removed to prevent it from being mixed into food. Normally, okara immediately after extraction contains a large amount of solvent, so most of the solvent is first separated using a compressor, compressor, centrifuge, etc. After separation, steam is directly applied to the defatted okara. Either evaporate or distill off the solvent by blowing it in, or
It is distilled off by indirect heating with steam. Defatted okara from which the solvent has been removed in this way usually returns to its original water content before being defatted, and is turned into a white powder with little or no soymilk odor characteristic of raw okara and other odor caused by lipid oxidation. It is. Therefore, the above-mentioned defatted okara is suitable as a food material if it is used as it is or if it is further pulverized and sized by sieving, wind speed, etc. to +4.

又、分離した溶剤は廃棄することなく回収し、蒸溜塔に
通液して溶剤を回収し、前記の抽出に使用する。又、こ
のときの蒸溜残渣は多量の油脂その他を含むので飼料と
して好適である。
Further, the separated solvent is recovered without being disposed of, and is passed through a distillation column to recover the solvent and used for the above-mentioned extraction. Further, the distillation residue at this time contains a large amount of oil and fat, and is therefore suitable as feed.

本発明の素材を使用して食品を製造する場合は、第2表
で示した如く溶剤の種類により品質に差があり、例えば
、アルコールで抽出した素材は白色、無臭の粉末で、あ
らゆる食品に混合使用できるが、特に良質の繊維が多く
膨潤性保水性が強く、和菓子、洋菓子のように微妙な香
味を生かす食品に混合すると菓子の品質を損うことなく
、且つ生地の腰を強くして作業性が向上する。又、n−
ヘキサンの如き溶剤で抽出した素材は前者にくらべ残存
糖質量も多く回収率も高いので安価に製造でき、魚肉練
り製品、畜肉加工食品、あん、ノ々ン、その細小麦粉製
品等の製造に添加して好適である。
When producing foods using the material of the present invention, there are differences in quality depending on the type of solvent as shown in Table 2. For example, the material extracted with alcohol is a white, odorless powder that can be used in all foods. It can be used in mixtures, but it is particularly high in quality fiber and has strong swelling and water retention properties, so when mixed with foods that make use of delicate flavors such as Japanese and Western sweets, it does not impair the quality of the confectionery and strengthens the elasticity of the dough. Improves work efficiency. Also, n-
Materials extracted with a solvent such as hexane have a higher amount of residual sugar than the former and have a higher recovery rate, so they can be produced at a lower cost and can be added to the production of fish paste products, processed meat foods, bean paste, nonan, and fine flour products, etc. It is suitable.

本発明の素材を食品製造時に使用する場合はそのま\、
或いはこれに香料、エキス等を吸着させて、原料配合時
に添加するか、配合後の混合、混ねつ或いは橿潰時に添
加するのが適当で、粉状のま\添加してもよく必要に応
じては水に分散させた後添加してもよい。添加量は食品
の特性を失なわない範囲で任意の蓋使用することができ
るが、通常10%以下とするのがよい。例えば本発明の
素材をかまぼこやちくわの如き練り製品の製造に使用す
る場合は、すり身の播潰時に5〜10%の範囲で添加す
るとよい。播潰後、常法により成型、蒸煮、焼きの工程
を行うと、成型時の保型性が改良され、蒸煮、焼きの工
程での収縮が少なくなる等の利点がある。又、添加する
本発明の素材に前以て香料、エキス等を含有させておく
と、改良された風味の製品が得られる。又、ノ(ン等の
製造に使用する場合は、小麦粉配合時に粉状で10%以
下の量を添加しておき、添加後は常法により混ねつ、発
酵、成型、焼成を行うとよい。この場合、生地の性質が
改良され、吸水量が増加し腰がでてボリューム、す立が
改良され保水性のよい)くンとなる。又、そうめん、う
どん、そば等のめん麺製品の製造に使用すると、本発明
の素材は添加した水分量に応じて腰の強い生地から軟い
生地となるので作業性を改善し、生地を改良する効果を
奏する。この外、焼き菓子、畜肉製品の製造工程で添加
すると混ねつ時腰が強くなるので製造管理が容易となる
のみならず、本発明の素材は無味、無臭であるから製品
の特性を劣化させることなく更に香料等を添加する場合
は本発明の素材に前以て含有せしめておくと長期間香料
の効果を保有せしめることができるし、保水性がよいの
で外界の湿分変化に対して抵抗性を有し、長期間製品の
劣化を防止できる等多くの利点を有するものである。
When using the material of the present invention during food production,
Alternatively, it is appropriate to adsorb fragrances, extracts, etc. to this and add it when blending raw materials, or add it during mixing, kneading, or crushing after blending, or it may be added in powder form if necessary. Depending on the situation, it may be added after being dispersed in water. Any amount can be used as long as the properties of the food are not lost, but it is usually 10% or less. For example, when the material of the present invention is used to manufacture a paste product such as kamaboko or chikuwa, it is preferable to add it in a range of 5 to 10% when crushing the surimi. After sowing, molding, steaming, and baking are performed using conventional methods, which has the advantage of improving shape retention during molding and reducing shrinkage during the steaming and baking steps. Furthermore, if the material of the present invention to be added contains fragrances, extracts, etc. in advance, a product with improved flavor can be obtained. In addition, when using it for the production of non (non), etc., it is recommended to add 10% or less in powder form when blending flour, and after addition, mix, ferment, mold, and bake in the usual manner. In this case, the properties of the fabric are improved, the amount of water absorbed increases, the waist is increased, the volume and stand are improved, and the fabric has good water retention properties. Furthermore, when used in the production of noodle products such as somen, udon, and soba, the material of the present invention changes from firm to soft dough depending on the amount of water added, improving workability and improving the dough. It has the effect of In addition, when added in the manufacturing process of baked goods and livestock meat products, it not only makes the manufacturing process easier as it increases the stiffness during mixing, but also deteriorates the characteristics of the product because the material of the present invention is tasteless and odorless. If you want to add fragrances, etc., to the material of the present invention in advance, the effect of the fragrance can be retained for a long period of time, and the material has good water retention properties, so it can resist changes in moisture in the outside world. It has many advantages, such as being able to prevent product deterioration over a long period of time.

以下実施例により説明する。This will be explained below using examples.

実施例1 豆乳製造時のおから(水分量83%) 1,000kg
をロータリードライヤーに連続的に供給し、通風温度2
00℃、ドライヤー排出時の品温85℃で平均水分約5
チ迄乾燥し、約160ki9の乾燥おからを得た。この
乾燥おからを向流式抽出装置に供給し、n−へキサンで
室温で抽出し、抽出後は60 klil/cm2の加圧
で圧搾した。圧搾後はぐして容器に入れ120℃の生蒸
気で残存するn−へキサンを完全に除去した。この結果
平均水分約6チの脱脂おから約145kgを得た。脱脂
おからはボールミルで粉砕後100メツシュの篩で篩別
した。
Example 1 Okara (water content 83%) during soy milk production 1,000 kg
is continuously supplied to the rotary dryer, and the ventilation temperature is 2.
00℃, product temperature 85℃ when discharged from dryer, average moisture content is approximately 5
The dried bean curd was dried to about 160 ki9 liters. This dried okara was supplied to a countercurrent extractor, extracted with n-hexane at room temperature, and after extraction was compressed under a pressure of 60 klil/cm2. After squeezing, the mixture was peeled off and placed in a container, and residual n-hexane was completely removed using live steam at 120°C. As a result, about 145 kg of defatted okara with an average moisture content of about 6 g was obtained. The defatted okara was ground in a ball mill and then sieved through a 100-mesh sieve.

上記脱脂おからをたらの冷凍すシ身50kgの塩ずりの
途中で10kg加え、これに澱粉40kLみりん1kg
、砂糖3kg、卵白、グルタミン敵ソーダを少量加えて
混合し、常法により成型後85℃で蒸煮した。製造中、
座シがよく作業性が改善され試食試験の結果弾力性があ
って口あたりが良好で異和感の全くないかまぼこである
ことが判明した。
Add 10 kg of the above defatted okara while salting 50 kg of frozen cod meat, add 40 kL of starch, and 1 kg of mirin.
, 3 kg of sugar, egg white, and a small amount of glutamine soda were added and mixed, molded in a conventional manner, and then steamed at 85°C. During manufacturing,
The kamaboko had a good seat and improved workability, and a tasting test revealed that the kamaboko was elastic, had a good mouthfeel, and had no unpleasant sensations.

実施例2 実施例1のn−へキサンを局方アルコールに代えて抽出
し、抽出後実施例1と園様に加熱してエタノールを溜去
し、乾燥後平均水分約5チの脱脂おから約90kgを得
た。
Example 2 The n-hexane in Example 1 was extracted by replacing it with pharmacopoeial alcohol, and after extraction, the mixture was heated in the same manner as in Example 1 to distill off the ethanol, and after drying, defatted okara with an average water content of about 5 t was obtained. I gained about 90 kg.

この脱脂おからは白色、無臭の粉末で強いゲル化能ヲ有
していた。これをボールミルで粉砕し、200メツシユ
の篩で篩別し、クリーム45.5、脱脂乳38、糖類1
4、ゼラチン0.5、界面活性剤等1及び前記篩別した
脱脂おからにバニラ香料を含有させたもめ10割合で混
合し、均質化波フリーザーで凍らせてアイスクリームと
した。
This defatted okara was a white, odorless powder with strong gelling ability. This was ground in a ball mill and sieved through a 200-mesh sieve. Cream 45.5, skim milk 38, sugar 1.
4. 0.5 parts of gelatin, 1 part of surfactant, and 10 parts of the sieved defatted okara mixed with vanilla flavor were mixed and frozen in a homogenization wave freezer to make ice cream.

得られたアイスクリームは口当りがよく、脱脂おから添
加による異和感は全くなかった。
The obtained ice cream had a good texture and did not have any strange feeling due to the addition of defatted okara.

実施例3 実施例1で得た脱脂おからにタマネギ等より調製したエ
キスを含有せしめ、これをソーセージ製造時原料肉を調
製後、サイレントカッターで他の副資材と混合する除、
原料内100kgに対し前記エキス含有脱脂おから5k
gの割合で添加した。得られたソーセージの風味は良好
で増量効果は顕著であった。
Example 3 The defatted okara obtained in Example 1 was made to contain an extract prepared from onions, etc., and after preparing raw meat for sausage production, this was mixed with other auxiliary materials using a silent cutter.
5 kg of defatted okara containing the above extract per 100 kg of raw materials
g. The flavor of the resulting sausage was good and the weight-increasing effect was remarkable.

実施例4 実施9IJ2で得た脱脂おから3に9を小麦粉100k
lilと共にドーミキサーに入れ水65kg及び砂糖。
Example 4 Example 9 Add 3 to 9 of the defatted okara obtained in IJ2 to 100k of flour
Add 65kg of water and sugar to a dough mixer with lil.

イースト、ショートニング、食塩と共に混合し、ストレ
ート法でパンを製造した。生地は吸水が多いにもかかわ
らず腰が強く、得られたパンはポリ実施例5 実施例2で得た脱脂おから7kg’lk米の粉io。
Bread was made by mixing with yeast, shortening, and salt using the straight method. Although the dough absorbs a lot of water, it has a firm texture, and the resulting bread is made of 7 kg of defatted okara rice flour obtained in Example 2.

kgに混合し、蒸してつき、成型乾燥後焼成してせんべ
いとした。得られたせんべいは、脱脂おからを加えない
ものと殆んど同じ風味を有していた。
kg, steamed, molded, dried and baked to make rice crackers. The resulting rice crackers had almost the same flavor as those without the addition of defatted okara.

特許出願人 明治乳業株式会社patent applicant Meiji Dairies Co., Ltd.

Claims (1)

【特許請求の範囲】 (1)脱脂したおからよりなる食品素材。 (2)おからを乾燥し脱脂能を有する有機溶剤で抽出し
、抽出抜脱溶剤することを特徴とする食品素材の製造方
法。 (4)有機溶剤がn−ヘキサンであることを特徴とする
特許請求の範囲第2項の食品素材の製造方法。 (5)脱溶剤後更に粉化することを特徴とする特許請求
の範囲第2項の食品素材の製造方法。
[Claims] (1) A food material made of defatted okara. (2) A method for producing a food material, which comprises drying okara, extracting it with an organic solvent that has a degreasing ability, and removing and removing the solvent. (4) The method for producing a food material according to claim 2, wherein the organic solvent is n-hexane. (5) The method for producing a food material according to claim 2, which further comprises powdering after removing the solvent.
JP57068707A 1982-04-26 1982-04-26 Food raw material and its preparation Pending JPS58187155A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP57068707A JPS58187155A (en) 1982-04-26 1982-04-26 Food raw material and its preparation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP57068707A JPS58187155A (en) 1982-04-26 1982-04-26 Food raw material and its preparation

Publications (1)

Publication Number Publication Date
JPS58187155A true JPS58187155A (en) 1983-11-01

Family

ID=13381511

Family Applications (1)

Application Number Title Priority Date Filing Date
JP57068707A Pending JPS58187155A (en) 1982-04-26 1982-04-26 Food raw material and its preparation

Country Status (1)

Country Link
JP (1) JPS58187155A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4642241A (en) * 1984-12-27 1987-02-10 Director Of National Food Research Institute Method for the preparation of textured soybean draff
JPH03224459A (en) * 1990-01-30 1991-10-03 Orient Moken:Kk Production of fiber food
JP2010233497A (en) * 2009-03-31 2010-10-21 Institute Of National Colleges Of Technology Japan Extract from Okara

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4642241A (en) * 1984-12-27 1987-02-10 Director Of National Food Research Institute Method for the preparation of textured soybean draff
JPH03224459A (en) * 1990-01-30 1991-10-03 Orient Moken:Kk Production of fiber food
JP2010233497A (en) * 2009-03-31 2010-10-21 Institute Of National Colleges Of Technology Japan Extract from Okara

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