JPS59101476A - エポキシ化合物の精製方法 - Google Patents

エポキシ化合物の精製方法

Info

Publication number: JPS59101476A
Authority: JP; Japan
Prior art keywords: epoxy compound; acetic acid; condenser; condensed; evaporator
Prior art date: 1982-11-30
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP21022782A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0324475B2 (cs

Inventor

Shinji Hattori

服部　信司

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Daicel Corp

Original Assignee

Daicel Chemical Industries Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1982-11-30

Filing date

1982-11-30

Publication date

1984-06-12

1982-11-30 Application filed by Daicel Chemical Industries Ltd filed Critical Daicel Chemical Industries Ltd

1982-11-30 Priority to JP21022782A priority Critical patent/JPS59101476A/ja

1984-06-12 Publication of JPS59101476A publication Critical patent/JPS59101476A/ja

1991-04-03 Publication of JPH0324475B2 publication Critical patent/JPH0324475B2/ja

Status Granted legal-status Critical Current

Links

150000001875 compounds Chemical class 0.000 title claims abstract description 39
239000004593 Epoxy Substances 0.000 title claims abstract description 37
238000000746 purification Methods 0.000 title description 5
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 120
238000000034 method Methods 0.000 claims abstract description 31
239000007788 liquid Substances 0.000 claims abstract description 28
239000010409 thin film Substances 0.000 claims abstract description 10
KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 claims description 22
238000006735 epoxidation reaction Methods 0.000 claims description 6
238000001704 evaporation Methods 0.000 abstract description 14
238000009835 boiling Methods 0.000 abstract description 13
230000008020 evaporation Effects 0.000 abstract description 12
238000009833 condensation Methods 0.000 abstract description 6
230000005494 condensation Effects 0.000 abstract description 6
238000003809 water extraction Methods 0.000 abstract description 3
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 15
238000006243 chemical reaction Methods 0.000 description 14
239000000243 solution Substances 0.000 description 13
238000004821 distillation Methods 0.000 description 11
XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 10
RBHIUNHSNSQJNG-UHFFFAOYSA-N 6-methyl-3-(2-methyloxiran-2-yl)-7-oxabicyclo[4.1.0]heptane Chemical compound C1CC2(C)OC2CC1C1(C)CO1 RBHIUNHSNSQJNG-UHFFFAOYSA-N 0.000 description 8
239000000203 mixture Substances 0.000 description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 4
239000006227 byproduct Substances 0.000 description 4
238000010438 heat treatment Methods 0.000 description 3
150000002894 organic compounds Chemical class 0.000 description 3
230000001590 oxidative effect Effects 0.000 description 3
238000000926 separation method Methods 0.000 description 3
239000002904 solvent Substances 0.000 description 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
AWMVMTVKBNGEAK-UHFFFAOYSA-N Styrene oxide Chemical compound C1OC1C1=CC=CC=C1 AWMVMTVKBNGEAK-UHFFFAOYSA-N 0.000 description 2
230000000052 comparative effect Effects 0.000 description 2
239000012045 crude solution Substances 0.000 description 2
229940087305 limonene Drugs 0.000 description 2
235000001510 limonene Nutrition 0.000 description 2
238000004064 recycling Methods 0.000 description 2
238000007790 scraping Methods 0.000 description 2
OECTYKWYRCHAKR-UHFFFAOYSA-N 4-vinylcyclohexene dioxide Chemical compound C1OC1C1CC2OC2CC1 OECTYKWYRCHAKR-UHFFFAOYSA-N 0.000 description 1
XAYDWGMOPRHLEP-UHFFFAOYSA-N 6-ethenyl-7-oxabicyclo[4.1.0]heptane Chemical compound C1CCCC2OC21C=C XAYDWGMOPRHLEP-UHFFFAOYSA-N 0.000 description 1
XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 1
229910000831 Steel Inorganic materials 0.000 description 1
KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 1
239000002253 acid Substances 0.000 description 1
230000001476 alcoholic effect Effects 0.000 description 1
238000000998 batch distillation Methods 0.000 description 1
238000001944 continuous distillation Methods 0.000 description 1
230000008094 contradictory effect Effects 0.000 description 1
239000000498 cooling water Substances 0.000 description 1
230000006837 decompression Effects 0.000 description 1
230000007423 decrease Effects 0.000 description 1
NKDDWNXOKDWJAK-UHFFFAOYSA-N dimethoxymethane Chemical compound COCOC NKDDWNXOKDWJAK-UHFFFAOYSA-N 0.000 description 1
238000007700 distillative separation Methods 0.000 description 1
238000005194 fractionation Methods 0.000 description 1
239000011521 glass Substances 0.000 description 1
239000007791 liquid phase Substances 0.000 description 1
239000012071 phase Substances 0.000 description 1
239000000047 product Substances 0.000 description 1
230000001737 promoting effect Effects 0.000 description 1
238000010992 reflux Methods 0.000 description 1
230000000630 rising effect Effects 0.000 description 1
229910001220 stainless steel Inorganic materials 0.000 description 1
239000010935 stainless steel Substances 0.000 description 1
239000010959 steel Substances 0.000 description 1

Landscapes

Epoxy Compounds (AREA)

JP21022782A 1982-11-30 1982-11-30 エポキシ化合物の精製方法 Granted JPS59101476A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP21022782A JPS59101476A (ja)	1982-11-30	1982-11-30	エポキシ化合物の精製方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP21022782A JPS59101476A (ja)	1982-11-30	1982-11-30	エポキシ化合物の精製方法

Publications (2)

Publication Number	Publication Date
JPS59101476A true JPS59101476A (ja)	1984-06-12
JPH0324475B2 JPH0324475B2 (cs)	1991-04-03

Family

ID=16585887

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP21022782A Granted JPS59101476A (ja)	1982-11-30	1982-11-30	エポキシ化合物の精製方法

Country Status (1)

Country	Link
JP (1)	JPS59101476A (cs)

1982
- 1982-11-30 JP JP21022782A patent/JPS59101476A/ja active Granted

Also Published As

Publication number	Publication date
JPH0324475B2 (cs)	1991-04-03

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