JPS59210041A - 酢酸の回収法 - Google Patents

酢酸の回収法

Info

Publication number: JPS59210041A
Authority: JP; Japan
Prior art keywords: acetic acid; acid; organic; tertiary amine; extraction
Prior art date: 1983-05-13
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP8471283A

Other languages

English (en)

Japanese (ja)

Other versions

JPS6352022B2 (de

Inventor

Kunio Koga

国夫古賀

Mutsumi Samejima

睦鮫島

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Daicel Corp

Original Assignee

Daicel Chemical Industries Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-05-13

Filing date

1983-05-13

Publication date

1984-11-28

1983-05-13 Application filed by Daicel Chemical Industries Ltd filed Critical Daicel Chemical Industries Ltd

1983-05-13 Priority to JP8471283A priority Critical patent/JPS59210041A/ja

1984-05-11 Priority to GB08412069A priority patent/GB2139624A/en

1984-05-14 Priority to FR8407442A priority patent/FR2546882B1/fr

1984-11-28 Publication of JPS59210041A publication Critical patent/JPS59210041A/ja

1988-10-17 Publication of JPS6352022B2 publication Critical patent/JPS6352022B2/ja

Status Granted legal-status Critical Current

Links

QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 title claims abstract description 132
238000000034 method Methods 0.000 title claims abstract description 14
238000000605 extraction Methods 0.000 claims abstract description 23
150000007522 mineralic acids Chemical class 0.000 claims abstract description 21
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 16
239000008346 aqueous phase Substances 0.000 claims abstract description 16
150000003512 tertiary amines Chemical class 0.000 claims abstract description 13
239000007864 aqueous solution Substances 0.000 claims abstract description 10
239000003085 diluting agent Substances 0.000 claims abstract description 8
239000000203 mixture Substances 0.000 claims abstract description 6
239000000284 extract Substances 0.000 claims description 9
239000003795 chemical substances by application Substances 0.000 abstract description 7
150000001412 amines Chemical class 0.000 description 10
239000002253 acid Substances 0.000 description 9
238000005192 partition Methods 0.000 description 9
239000002904 solvent Substances 0.000 description 8
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
MEBONNVPKOBPEA-UHFFFAOYSA-N 1,1,2-trimethylcyclohexane Chemical compound CC1CCCCC1(C)C MEBONNVPKOBPEA-UHFFFAOYSA-N 0.000 description 4
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
230000003247 decreasing effect Effects 0.000 description 4
230000007423 decrease Effects 0.000 description 3
239000012074 organic phase Substances 0.000 description 3
239000003960 organic solvent Substances 0.000 description 3
-1 sulfuric acid Chemical class 0.000 description 3
239000003513 alkali Substances 0.000 description 2
229910000147 aluminium phosphate Inorganic materials 0.000 description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
230000000052 comparative effect Effects 0.000 description 2
230000000694 effects Effects 0.000 description 2
239000007788 liquid Substances 0.000 description 2
238000006386 neutralization reaction Methods 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
239000001301 oxygen Substances 0.000 description 2
238000011084 recovery Methods 0.000 description 2
150000003839 salts Chemical class 0.000 description 2
235000011121 sodium hydroxide Nutrition 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
XPZBNIUWMDJFPW-UHFFFAOYSA-N 2,2,3-trimethylcyclohexan-1-one Chemical compound CC1CCCC(=O)C1(C)C XPZBNIUWMDJFPW-UHFFFAOYSA-N 0.000 description 1
VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
238000009825 accumulation Methods 0.000 description 1
239000002585 base Substances 0.000 description 1
238000009835 boiling Methods 0.000 description 1
238000004581 coalescence Methods 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000004821 distillation Methods 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
239000011521 glass Substances 0.000 description 1
239000012046 mixed solvent Substances 0.000 description 1
XTAZYLNFDRKIHJ-UHFFFAOYSA-N n,n-dioctyloctan-1-amine Chemical compound CCCCCCCCN(CCCCCCCC)CCCCCCCC XTAZYLNFDRKIHJ-UHFFFAOYSA-N 0.000 description 1
239000012071 phase Substances 0.000 description 1
239000001632 sodium acetate Substances 0.000 description 1
235000017281 sodium acetate Nutrition 0.000 description 1
239000000243 solution Substances 0.000 description 1
238000003756 stirring Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Oil, Petroleum & Natural Gas (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Extraction Or Liquid Replacement (AREA)

JP8471283A 1983-05-13 1983-05-13 酢酸の回収法 Granted JPS59210041A (ja)

Priority Applications (3)

Application Number	Priority Date	Filing Date	Title
JP8471283A JPS59210041A (ja)	1983-05-13	1983-05-13	酢酸の回収法
GB08412069A GB2139624A (en)	1983-05-13	1984-05-11	Process for recovering acetic acid
FR8407442A FR2546882B1 (fr)	1983-05-13	1984-05-14	Procede de recuperation d'acide acetique

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP8471283A JPS59210041A (ja)	1983-05-13	1983-05-13	酢酸の回収法

Publications (2)

Publication Number	Publication Date
JPS59210041A true JPS59210041A (ja)	1984-11-28
JPS6352022B2 JPS6352022B2 (de)	1988-10-17

Family

ID=13838272

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP8471283A Granted JPS59210041A (ja)	1983-05-13	1983-05-13	酢酸の回収法

Country Status (3)

Country	Link
JP (1)	JPS59210041A (de)
FR (1)	FR2546882B1 (de)
GB (1)	GB2139624A (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2011517445A (ja) *	2008-03-20	2011-06-09	テートアンドライルテクノロジーリミテッド	第三級アミド溶媒からの酸の除去

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DK170019B1 (da) *	1993-03-12	1995-05-01	Topsoe Haldor As	Fremgangsmåde til genvinding af brugt fluoreret sulfonsyrekatalysator fra en alkyleringsproces

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR866969A (fr) *	1940-05-23	1941-09-20	Le Gouvernement De La Province	Procédé pour la concentration ou l'extraction de l'acide acétique
US2581452A (en) *	1947-03-29	1952-01-08	Kellogg M W Co	Dehydration of organic acids
US4353784A (en) *	1981-09-21	1982-10-12	Daicel Chemical Industries, Ltd.	Method of recovery of acetic acid
JPS597131A (ja) *	1982-07-06	1984-01-14	Daicel Chem Ind Ltd	酢酸の回収法

1983
- 1983-05-13 JP JP8471283A patent/JPS59210041A/ja active Granted
1984
- 1984-05-11 GB GB08412069A patent/GB2139624A/en not_active Withdrawn
- 1984-05-14 FR FR8407442A patent/FR2546882B1/fr not_active Expired

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2011517445A (ja) *	2008-03-20	2011-06-09	テートアンドライルテクノロジーリミテッド	第三級アミド溶媒からの酸の除去

Also Published As

Publication number	Publication date
FR2546882A1 (fr)	1984-12-07
JPS6352022B2 (de)	1988-10-17
GB2139624A (en)	1984-11-14
GB8412069D0 (en)	1984-06-20
FR2546882B1 (fr)	1987-07-17

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