JPS5943201B2 - How to collect liquid crystal - Google Patents
How to collect liquid crystalInfo
- Publication number
- JPS5943201B2 JPS5943201B2 JP14627080A JP14627080A JPS5943201B2 JP S5943201 B2 JPS5943201 B2 JP S5943201B2 JP 14627080 A JP14627080 A JP 14627080A JP 14627080 A JP14627080 A JP 14627080A JP S5943201 B2 JPS5943201 B2 JP S5943201B2
- Authority
- JP
- Japan
- Prior art keywords
- liquid crystal
- cell
- injection hole
- holder
- absorbed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000004973 liquid crystal related substance Substances 0.000 title claims description 47
- 238000002347 injection Methods 0.000 claims description 21
- 239000007924 injection Substances 0.000 claims description 21
- 239000000835 fiber Substances 0.000 claims description 14
- 210000004027 cell Anatomy 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 10
- 239000010453 quartz Substances 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 210000002858 crystal cell Anatomy 0.000 claims description 5
- 239000003960 organic solvent Substances 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 2
- 238000011084 recovery Methods 0.000 claims 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 12
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000565 sealant Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 238000009849 vacuum degassing Methods 0.000 description 2
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 239000004917 carbon fiber Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- KYKAJFCTULSVSH-UHFFFAOYSA-N chloro(fluoro)methane Chemical compound F[C]Cl KYKAJFCTULSVSH-UHFFFAOYSA-N 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 239000003365 glass fiber Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Liquid Crystal (AREA)
- Extraction Or Liquid Replacement (AREA)
- Liquid Crystal Substances (AREA)
Description
【発明の詳細な説明】
本発明は液晶セルの製造工程、特に液晶を注入する際に
セルの注入孔周辺に付着した余分の液晶を回収する方法
に関する。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a process for manufacturing a liquid crystal cell, and more particularly to a method for recovering excess liquid crystal deposited around an injection hole of a cell during injection of liquid crystal.
液晶セルは通常、一対の電極板を所定の間隔に対向配置
し、周辺をシール剤によりシールし、シール部の1ケ所
又は2ケ所に設けられた注入孔より液晶を注入後、注入
孔を封止することによつて作成される。Usually, a liquid crystal cell has a pair of electrode plates arranged facing each other at a predetermined distance, the periphery is sealed with a sealant, liquid crystal is injected through an injection hole provided at one or two places in the sealing part, and then the injection hole is sealed. created by stopping.
液晶を注入する方法としては、セルと液晶を真空脱気可
能な容器に入れ、真空脱気を行なつた後、セルの注入孔
に液晶を接触させ、その後常圧の不活性ガスを容器にパ
ージさせることにより注入を行なう方法と、2つの注入
孔の一方に液晶を接触させ、他方より吸引することによ
つて注入する方法がある。The method for injecting liquid crystal is to place the cell and liquid crystal in a container that can be vacuum degassed, and after vacuum degassing, bring the liquid crystal into contact with the injection hole of the cell, and then fill the container with inert gas at normal pressure. There is a method of injecting by purging, and a method of injecting by bringing liquid crystal into contact with one of two injection holes and suctioning from the other.
いずれの注入方法においても注入の際の泡の混入を防ぐ
ため過剰の液晶に接触させる必要があり、注入孔周辺に
余分な液晶が付着してしまう。従来は、この注入孔周辺
に付着した余分の液晶をふきとつていたが、この余分に
付着した液晶の量は実際にセルに注入される量の1〜2
倍あり、極めて無駄が多い上に、安全衛生面、公害面に
おいても多くの欠点があつた。In either injection method, in order to prevent bubbles from entering during injection, it is necessary to contact excess liquid crystal, resulting in excess liquid crystal adhering to the vicinity of the injection hole. Conventionally, the excess liquid crystal that adhered around this injection hole was wiped off, but the amount of excess liquid crystal that adhered was 1 to 2 times the amount that was actually injected into the cell.
Not only was it twice as expensive, it was extremely wasteful, but it also had many drawbacks in terms of safety, health, and pollution.
本発明は、上記問題点に鑑みなされたもので、液晶を注
入する際にセル注入孔周辺に付着した余分の液晶を回収
する方法を提供するものである。The present invention has been made in view of the above problems, and provides a method for recovering excess liquid crystal that adheres around the cell injection hole when liquid crystal is injected.
即ち、本発明は液晶セルに液晶を注入する際に、セルの
注入孔周辺に付着した余分の液晶を保持体に接触させ、
該保持体に吸収された液晶を有機溶剤を用いて抽出し、
次いで溶剤と液晶を分離することを特徴とする。本発明
にあつては、液晶を注入した際に注入孔周辺に付着した
余分の液晶に対し保持体を接触させると毛細管現象によ
り、液晶が保持体に吸収される。That is, in the present invention, when injecting liquid crystal into a liquid crystal cell, excess liquid crystal attached around the injection hole of the cell is brought into contact with a holder,
Extracting the liquid crystal absorbed by the holder using an organic solvent,
The method is characterized in that the solvent and liquid crystal are then separated. In the present invention, when the holder is brought into contact with excess liquid crystal that has adhered around the injection hole when liquid crystal is injected, the liquid crystal is absorbed into the holder due to capillary action.
保持体に吸収された液晶は、例えばベンゼン、メタノー
ル、アセトン、エタノール、トルエン、フロン等の溶解
度の高い有機溶剤を用いて抽出する。抽出された液晶は
有機溶剤を真空脱気することにより分離回収され、再び
利用される。本発明において保持体としては、毛細管効
果のあるものであればよく、例えば、石英ファイバー、
ガラス繊維、炭素繊維、金属繊維、石綿繊維、スラグ繊
維、有機ファイバー等の繊維又はこれらを加工したヤー
ン、テープマット、クロス或はスポンジ等が例示される
が、特に液晶に対し汚染がなく、任意の形状が得られ、
毛細管効果の優れた石英ファイバーのヤーンが望ましい
。実施例
第1図に示す様にセル1の注入孔2を液晶3に接触させ
て真空注入した。The liquid crystal absorbed by the carrier is extracted using a highly soluble organic solvent such as benzene, methanol, acetone, ethanol, toluene, and chlorofluorocarbon. The extracted liquid crystal is separated and recovered by vacuum degassing of the organic solvent, and is reused. In the present invention, the holder may be anything that has a capillary effect, such as quartz fiber,
Examples include fibers such as glass fibers, carbon fibers, metal fibers, asbestos fibers, slag fibers, and organic fibers, or yarns processed from these fibers, tape mats, cloths, sponges, etc., but in particular, any material that does not contaminate liquid crystals may be used. The shape is obtained,
A quartz fiber yarn with good capillary effect is preferred. EXAMPLE As shown in FIG. 1, the injection hole 2 of the cell 1 was brought into contact with the liquid crystal 3, and vacuum injection was carried out.
この際セル1の注入孔2の周辺部に付着した余分の液晶
4を石英フアイバ一のヤーン5に吸収させ(第2図)注
入孔2周辺の余分の液晶を除去し(第3図)、注入孔2
を封止剤6で封止して液晶セルを得た。この製造工程に
おいて、石英フアイバ一のヤーン5に吸収された液晶の
量は過剰液晶の約70%であつた。At this time, the excess liquid crystal 4 attached to the periphery of the injection hole 2 of the cell 1 is absorbed by the yarn 5 of the quartz fiber (Fig. 2), and the excess liquid crystal around the injection hole 2 is removed (Fig. 3). Injection hole 2
was sealed with sealant 6 to obtain a liquid crystal cell. In this manufacturing process, the amount of liquid crystal absorbed into the quartz fiber yarns 5 was approximately 70% of the excess liquid crystal.
石英フアイバ一のヤーン中に吸収された液晶をベンゼン
を用いて抽出し、次いでベンゼンと液晶は真空ロータリ
ーエバポレーターを用いてベンゼンを脱気することによ
り分離し、過剰液晶の約60%が回収された。以上説明
した様に、本発明によれば、セルの注入孔周辺に付着し
た余分の液晶は、従来ふきとつていたのに換えて、保持
体に吸収させることにより、液晶の回収が可能となり、
液晶の無駄が著るしく低減された。The liquid crystals absorbed into the quartz fiber yarn were extracted using benzene, and then the benzene and liquid crystals were separated by degassing the benzene using a vacuum rotary evaporator, and approximately 60% of the excess liquid crystals were recovered. . As explained above, according to the present invention, excess liquid crystal attached around the injection hole of the cell can be recovered by absorbing it into the holder instead of wiping it off in the conventional method. ,
Liquid crystal waste has been significantly reduced.
又、繊維状の保持体を用いれば基板間の凹部に付着した
液晶も完全に吸い取りができる等の効果がある。Furthermore, if a fibrous holder is used, liquid crystal deposited in the recesses between the substrates can be completely absorbed.
第1図〜第4図は製造工程を示す側面図である。
1・・・・・・セル、2・・・・・・注入孔、3・・・
・・・液晶、4・・・・・・余分な液晶、5・・・・・
・保持体、6・・・・・・封止剤。1 to 4 are side views showing the manufacturing process. 1...Cell, 2...Injection hole, 3...
...LCD, 4...Extra liquid crystal, 5...
- Holding body, 6...Sealing agent.
Claims (1)
に付着した余分の液晶を保持体に接触させ、該保持体に
吸収された液晶を有機溶剤を用いて抽出し、次いで溶剤
と液晶を分離することを特徴とする液晶の回収方法。 2 保持体が繊維もしくは繊維を加工したものであるこ
とを特徴とする特許請求の範囲第1項記載の液晶の回収
方法。 3 保持体が石英ファイバーのヤーンであることを特徴
とする特許請求の範囲第2項記載の液晶の回収方法。[Claims] 1. When injecting liquid crystal into a liquid crystal cell, excess liquid crystal attached around the injection hole of the cell is brought into contact with a holder, and the liquid crystal absorbed by the holder is extracted using an organic solvent. and then separating the solvent and the liquid crystal. 2. The liquid crystal recovery method according to claim 1, wherein the holding body is made of fiber or processed fiber. 3. The liquid crystal recovery method according to claim 2, wherein the holding body is a quartz fiber yarn.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14627080A JPS5943201B2 (en) | 1980-10-21 | 1980-10-21 | How to collect liquid crystal |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14627080A JPS5943201B2 (en) | 1980-10-21 | 1980-10-21 | How to collect liquid crystal |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5771603A JPS5771603A (en) | 1982-05-04 |
| JPS5943201B2 true JPS5943201B2 (en) | 1984-10-20 |
Family
ID=15403933
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP14627080A Expired JPS5943201B2 (en) | 1980-10-21 | 1980-10-21 | How to collect liquid crystal |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5943201B2 (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI458570B (en) | 2011-12-07 | 2014-11-01 | Ind Tech Res Inst | Method of reusing micro-encapsulated cholesteric liquid crystal |
| TWI443181B (en) | 2011-12-07 | 2014-07-01 | Ind Tech Res Inst | Method for recovering cholesterol liquid crystal |
-
1980
- 1980-10-21 JP JP14627080A patent/JPS5943201B2/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5771603A (en) | 1982-05-04 |
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