JPS598614A - 有機溶剤を分散媒とするシリカゾルの製造方法 - Google Patents

有機溶剤を分散媒とするシリカゾルの製造方法

Info

Publication number: JPS598614A
Authority: JP; Japan
Prior art keywords: organic solvent; water; silica sol; dispersion medium; silica
Prior art date: 1982-06-30
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP11429482A

Other languages

English (en)

Japanese (ja)

Other versions

JPH021087B2 (fr

Inventor

Yusaku Arima

悠策有馬

Jun Yuki

結城　諄

Hiroyasu Nishida

広泰西田

Takashi Harada

孝原田

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

SHOKUBAI KASEI KOGYO KK

JGC Catalysts and Chemicals Ltd

Original Assignee

SHOKUBAI KASEI KOGYO KK

Catalysts and Chemicals Industries Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1982-06-30

Filing date

1982-06-30

Publication date

1984-01-17

1982-06-30 Application filed by SHOKUBAI KASEI KOGYO KK, Catalysts and Chemicals Industries Co Ltd filed Critical SHOKUBAI KASEI KOGYO KK

1982-06-30 Priority to JP11429482A priority Critical patent/JPS598614A/ja

1984-01-17 Publication of JPS598614A publication Critical patent/JPS598614A/ja

1990-01-10 Publication of JPH021087B2 publication Critical patent/JPH021087B2/ja

Status Granted legal-status Critical Current

Links

239000003960 organic solvent Substances 0.000 title claims abstract description 41
RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 title claims abstract description 31
239000002612 dispersion medium Substances 0.000 title claims abstract description 23
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 32
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 29
238000000034 method Methods 0.000 claims abstract description 24
239000000377 silicon dioxide Substances 0.000 claims abstract description 13
238000002156 mixing Methods 0.000 claims abstract description 12
239000002245 particle Substances 0.000 claims abstract description 8
239000000203 mixture Substances 0.000 claims abstract description 6
238000000108 ultra-filtration Methods 0.000 claims description 14
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
239000012528 membrane Substances 0.000 claims description 12
238000004519 manufacturing process Methods 0.000 claims description 4
150000002148 esters Chemical class 0.000 claims description 2
150000002576 ketones Chemical class 0.000 claims description 2
239000011148 porous material Substances 0.000 claims description 2
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
230000018044 dehydration Effects 0.000 claims 1
238000006297 dehydration reaction Methods 0.000 claims 1
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract description 12
238000001914 filtration Methods 0.000 abstract description 5
239000002904 solvent Substances 0.000 abstract description 4
239000012141 concentrate Substances 0.000 abstract description 3
229910052681 coesite Inorganic materials 0.000 abstract 1
229910052906 cristobalite Inorganic materials 0.000 abstract 1
235000012239 silicon dioxide Nutrition 0.000 abstract 1
229910052682 stishovite Inorganic materials 0.000 abstract 1
229910052905 tridymite Inorganic materials 0.000 abstract 1
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
230000000052 comparative effect Effects 0.000 description 6
235000019441 ethanol Nutrition 0.000 description 6
239000002131 composite material Substances 0.000 description 4
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
239000013040 bath agent Substances 0.000 description 3
238000009835 boiling Methods 0.000 description 3
238000001704 evaporation Methods 0.000 description 3
230000008020 evaporation Effects 0.000 description 3
239000011368 organic material Substances 0.000 description 3
239000003495 polar organic solvent Substances 0.000 description 3
239000000126 substance Substances 0.000 description 3
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 2
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 2
239000006185 dispersion Substances 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
239000007788 liquid Substances 0.000 description 2
239000005416 organic matter Substances 0.000 description 2
235000019353 potassium silicate Nutrition 0.000 description 2
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 2
POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 1
241001474374 Blennius Species 0.000 description 1
239000000853 adhesive Substances 0.000 description 1
230000001070 adhesive effect Effects 0.000 description 1
238000005054 agglomeration Methods 0.000 description 1
230000002776 aggregation Effects 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
238000011109 contamination Methods 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
238000001816 cooling Methods 0.000 description 1
238000000502 dialysis Methods 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000000694 effects Effects 0.000 description 1
150000002170 ethers Chemical class 0.000 description 1
-1 ethyl methyl ketone Chemical compound 0.000 description 1
238000000605 extraction Methods 0.000 description 1
239000012510 hollow fiber Substances 0.000 description 1
125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
239000011147 inorganic material Substances 0.000 description 1
229910052809 inorganic oxide Inorganic materials 0.000 description 1
238000005342 ion exchange Methods 0.000 description 1
239000012452 mother liquor Substances 0.000 description 1
230000003472 neutralizing effect Effects 0.000 description 1
239000003973 paint Substances 0.000 description 1
238000001935 peptisation Methods 0.000 description 1
239000003208 petroleum Substances 0.000 description 1
239000002994 raw material Substances 0.000 description 1
229920005989 resin Polymers 0.000 description 1
239000011347 resin Substances 0.000 description 1
239000011734 sodium Substances 0.000 description 1
159000000000 sodium salts Chemical class 0.000 description 1
239000007921 spray Substances 0.000 description 1
239000007858 starting material Substances 0.000 description 1
229920003002 synthetic resin Polymers 0.000 description 1
239000000057 synthetic resin Substances 0.000 description 1

Landscapes

Silicon Compounds (AREA)
Pigments, Carbon Blacks, Or Wood Stains (AREA)

JP11429482A 1982-06-30 1982-06-30 有機溶剤を分散媒とするシリカゾルの製造方法 Granted JPS598614A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP11429482A JPS598614A (ja)	1982-06-30	1982-06-30	有機溶剤を分散媒とするシリカゾルの製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP11429482A JPS598614A (ja)	1982-06-30	1982-06-30	有機溶剤を分散媒とするシリカゾルの製造方法

Publications (2)

Publication Number	Publication Date
JPS598614A true JPS598614A (ja)	1984-01-17
JPH021087B2 JPH021087B2 (fr)	1990-01-10

Family

ID=14634253

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP11429482A Granted JPS598614A (ja)	1982-06-30	1982-06-30	有機溶剤を分散媒とするシリカゾルの製造方法

Country Status (1)

Country	Link
JP (1)	JPS598614A (fr)

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4772660A (en) *	1985-10-18	1988-09-20	Sumitomo Chemical Company, Limited	Oxide sol using reactive monomer as dispersion medium
FR2684367A1 (fr) *	1991-12-02	1993-06-04	Hoechst France	Procede d'obtention d'un sol de silice disperse dans un alcanol inferieur et application de l'organosol ainsi obtenu, notamment a la preparation de compositions de revetement de surface de verre organique.
EP0699626A1 (fr)	1994-08-05	1996-03-06	Nissan Chemical Industries Ltd.	Méthode de préparation d'un sol de silice dans le propanol
JP2001213617A (ja) *	2000-01-28	2001-08-07	Jsr Corp	疎水化コロイダルシリカの製造方法
EP1754685A2 (fr)	2005-08-02	2007-02-21	Nissan Chemical Industries, Ltd.	Organosol de silice et son procédé de préparation
WO2009101974A1 (fr)	2008-02-12	2009-08-20	Nissan Chemical Industries, Ltd.	Particules de silice colloïdale, leur procédé de production et sol de silice dans un solvant organique, sol de silice dans un composé polymérisable et sol de silice dans de l'anhydride dicarboxylique obtenu à partir de celui-ci
JP2015034106A (ja) *	2013-08-08	2015-02-19	信越化学工業株式会社	オルガノゾル及びその製造方法
US9272916B2 (en)	2007-11-30	2016-03-01	Jgc Catalysts And Chemicals Ltd.	Non-spherical silica sol, process for producing the same, and composition for polishing
JP2019151498A (ja) *	2018-02-28	2019-09-12	株式会社ダイセル	ナノダイヤモンド有機溶媒分散体の製造方法
CN113636562A (zh) *	2021-09-02	2021-11-12	上海新安纳电子科技有限公司	一种二氧化硅分散液及其制备方法和应用

1982
- 1982-06-30 JP JP11429482A patent/JPS598614A/ja active Granted

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4772660A (en) *	1985-10-18	1988-09-20	Sumitomo Chemical Company, Limited	Oxide sol using reactive monomer as dispersion medium
FR2684367A1 (fr) *	1991-12-02	1993-06-04	Hoechst France	Procede d'obtention d'un sol de silice disperse dans un alcanol inferieur et application de l'organosol ainsi obtenu, notamment a la preparation de compositions de revetement de surface de verre organique.
EP0699626A1 (fr)	1994-08-05	1996-03-06	Nissan Chemical Industries Ltd.	Méthode de préparation d'un sol de silice dans le propanol
US5902226A (en) *	1994-08-05	1999-05-11	Nissan Chemical Industries, Ltd.	Method of preparing a propanol sol of silica
JP2001213617A (ja) *	2000-01-28	2001-08-07	Jsr Corp	疎水化コロイダルシリカの製造方法
EP1754685A2 (fr)	2005-08-02	2007-02-21	Nissan Chemical Industries, Ltd.	Organosol de silice et son procédé de préparation
JP2007063117A (ja) *	2005-08-02	2007-03-15	Nissan Chem Ind Ltd	有機溶媒分散シリカゾル及びその製造方法
US9272916B2 (en)	2007-11-30	2016-03-01	Jgc Catalysts And Chemicals Ltd.	Non-spherical silica sol, process for producing the same, and composition for polishing
US10160894B2 (en)	2007-11-30	2018-12-25	Jgc Catalysts And Chemicals Ltd.	Non-spherical silica sol, process for producing the same, and composition for polishing
US9527749B2 (en)	2008-02-12	2016-12-27	Nissan Chemical Industries, Ltd.	Colloidal silica particles, process for producing the same, and organic solvent-dispersed silica sol, polymerizable compound-dispersed silica sol, and dicarboxylic anhydride-dispersed silica sol each obtained from the same
US9284197B2 (en)	2008-02-12	2016-03-15	Nissan Chemical Industries, Ltd.	Colloidal silica particles, process for producing the same, and organic solvent-dispersed silica sol, polymerizable compound-dispersed silica sol, and dicarboxylic anhydride-dispersed silica sol each obtained from the same
US9376322B2 (en)	2008-02-12	2016-06-28	Nissan Chemical Industries, Ltd.	Process for producing colloidal silica particles
WO2009101974A1 (fr)	2008-02-12	2009-08-20	Nissan Chemical Industries, Ltd.	Particules de silice colloïdale, leur procédé de production et sol de silice dans un solvant organique, sol de silice dans un composé polymérisable et sol de silice dans de l'anhydride dicarboxylique obtenu à partir de celui-ci
JP2015034106A (ja) *	2013-08-08	2015-02-19	信越化学工業株式会社	オルガノゾル及びその製造方法
JP2019151498A (ja) *	2018-02-28	2019-09-12	株式会社ダイセル	ナノダイヤモンド有機溶媒分散体の製造方法
CN113636562A (zh) *	2021-09-02	2021-11-12	上海新安纳电子科技有限公司	一种二氧化硅分散液及其制备方法和应用

Also Published As

Publication number	Publication date
JPH021087B2 (fr)	1990-01-10

Publication	Publication Date	Title
DE2925969C2 (fr)	1987-12-03
DE60107049T2 (de)	2005-10-20	Verfahren zur herstellung von hydrophober kolloidaler kieselsäure
DE69915224T2 (de)	2005-01-13	Kieselsäure-Magnesiumfluoridhydrat-Komposit enthaltende Sole und Verfahren zu deren Herstellung
DE69304695T2 (de)	1997-03-20	Verfahren zur herstellung anorganischer gele
EP0716641B1 (fr)	1998-01-14	Aerogels hydrophobes d'acide silicique
DE19648798C2 (de)	1998-11-19	Verfahren zur Herstellung von organisch modifizierten Aerogelen durch Oberflächenmodifikation des wäßrigen Gels (ohne vorherigen Lösungsmitteltausch) und anschließender Trocknung
DE69721517T2 (de)	2004-03-18	Russ, verfahren zu seiner herstellung und waessrige dispersion und diesen russ enthaltende wasserfarbe
Tweddle et al.	1983	Polysulfone ultrafiltration membranes
EP1603663B1 (fr)	2010-05-26	Membrane de nanofiltration ceramique destinee a etre employee dans des solvants organiques et procede de fabrication
EP0098946B1 (fr)	1985-12-04	Organopolysiloxanes ayant des groupements sulfonates, procédé de préparation et leur emploi
DE2758415A1 (de)	1979-07-12	Kieselsaeureheteropolykondensate, verfahren zu deren herstellung und deren verwendung als membranen und adsorbentien
EP0859740A1 (fr)	1998-08-26	Procede de preparation d'aerogels modifies de maniere organique, selon lequel les sels formes sont precipites
JPS598614A (ja)	1984-01-17	有機溶剤を分散媒とするシリカゾルの製造方法
DE2048861A1 (de)	1971-04-22	Herstellungsverfahren von Benzvhden sorbit
EP1905741A1 (fr)	2008-04-02	Procédé destiné à la fabrication de sols en gravier riches en matières solides
WO1997018161A1 (fr)	1997-05-22	Procede de preparation d'aerogels modifies de maniere organique a l'aide d'alcools, selon lequel les sels formes sont precipites
DE102015207944A1 (de)	2016-11-03	Verfahren zur Herstellung organisch modifizierter Aerogele
US3738957A (en)	1973-06-12	Coacervates of polyvinyl alcohol and colloidal silica
EP0582811A1 (fr)	1994-02-16	Polysiloxanes façonnés ayant des groupes sulphonate, procédé de préparation et leur application
US4173491A (en)	1979-11-06	Pigmented microporous silica microspheres by spray processes
EP0207269B1 (fr)	1992-07-15	Organopolysiloxanes contenant des groupes phénylsulphonates, procédé de préparation et emploi
EP0812803B1 (fr)	2000-08-30	Préparation de dispersions d'un sol de silice à faible teneur en sel, dans des alcools à bas point d'ébullition
US3948799A (en)	1976-04-06	Process for preparing silica organosols
JPH05246707A (ja)	1993-09-24	低級アルカノールに分散したシリカゾルを製造する方法
DE1160413B (de)	1964-01-02	Verfahren zur Herstellung eines bestaendigen alkalischen Kieselsaeuresols