JPS60178871A - チアジアゾ−ル誘導体 - Google Patents

チアジアゾ−ル誘導体

Info

Publication number: JPS60178871A
Authority: JP; Japan
Prior art keywords: compound; solution; formula; thiadiazole; salt
Prior art date: 1984-02-23
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP59032971A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0533225B2 (2

Inventor

Hisashi Tanaka

久田中

Tomoo Tanaka

田中　共生

Terumasa Nakagawa

中川　照真

Masahiko Chikuma

正彦千熊

Morio Nakayama

守雄中山

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Daiichi Pharmaceutical Co Ltd

Original Assignee

Daiichi Pharmaceutical Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-02-23

Filing date

1984-02-23

Publication date

1985-09-12

1984-02-23 Application filed by Daiichi Pharmaceutical Co Ltd filed Critical Daiichi Pharmaceutical Co Ltd

1984-02-23 Priority to JP59032971A priority Critical patent/JPS60178871A/ja

1985-09-12 Publication of JPS60178871A publication Critical patent/JPS60178871A/ja

1993-05-19 Publication of JPH0533225B2 publication Critical patent/JPH0533225B2/ja

Status Granted legal-status Critical Current

Links

150000004867 thiadiazoles Chemical class 0.000 title 1
150000004869 1,3,4-thiadiazoles Chemical class 0.000 claims abstract 2
229910052783 alkali metal Inorganic materials 0.000 claims abstract 2
150000001340 alkali metals Chemical class 0.000 claims abstract 2
229910052784 alkaline earth metal Inorganic materials 0.000 claims abstract 2
150000001342 alkaline earth metals Chemical class 0.000 claims abstract 2
125000004435 hydrogen atom Chemical group [H]* 0.000 claims 1
150000001875 compounds Chemical class 0.000 abstract description 24
QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 abstract description 12
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract description 10
239000000243 solution Substances 0.000 abstract description 10
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 9
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract description 6
239000007864 aqueous solution Substances 0.000 abstract description 6
238000006243 chemical reaction Methods 0.000 abstract description 5
229910001385 heavy metal Inorganic materials 0.000 abstract description 5
150000002500 ions Chemical class 0.000 abstract description 5
239000003957 anion exchange resin Substances 0.000 abstract description 4
239000002738 chelating agent Substances 0.000 abstract description 3
235000011118 potassium hydroxide Nutrition 0.000 abstract description 3
238000002360 preparation method Methods 0.000 abstract description 3
-1 etc. Chemical compound 0.000 abstract description 2
150000003839 salts Chemical class 0.000 abstract description 2
235000011121 sodium hydroxide Nutrition 0.000 abstract description 2
125000000542 sulfonic acid group Chemical group 0.000 abstract description 2
239000002253 acid Substances 0.000 abstract 1
KCIDZIIHRGYJAE-YGFYJFDDSA-L dipotassium;[(2r,3r,4s,5r,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl] phosphate Chemical class [K+].[K+].OC[C@H]1O[C@H](OP([O-])([O-])=O)[C@H](O)[C@@H](O)[C@H]1O KCIDZIIHRGYJAE-YGFYJFDDSA-L 0.000 abstract 1
238000010438 heat treatment Methods 0.000 abstract 1
239000000463 material Substances 0.000 abstract 1
239000011347 resin Substances 0.000 description 8
229920005989 resin Polymers 0.000 description 8
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
239000013522 chelant Substances 0.000 description 4
239000000203 mixture Substances 0.000 description 3
239000000047 product Substances 0.000 description 3
XLYOFNOQVPJJNP-ZSJDYOACSA-N Heavy water Chemical compound [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 description 2
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 2
238000001479 atomic absorption spectroscopy Methods 0.000 description 2
239000013078 crystal Substances 0.000 description 2
239000007788 liquid Substances 0.000 description 2
229910021645 metal ion Inorganic materials 0.000 description 2
XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 2
238000010992 reflux Methods 0.000 description 2
229910052709 silver Inorganic materials 0.000 description 2
239000004332 silver Substances 0.000 description 2
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 2
GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 2
239000000126 substance Substances 0.000 description 2
238000005406 washing Methods 0.000 description 2
239000002699 waste material Substances 0.000 description 2
BIGYLAKFCGVRAN-UHFFFAOYSA-N 1,3,4-thiadiazolidine-2,5-dithione Chemical compound S=C1NNC(=S)S1 BIGYLAKFCGVRAN-UHFFFAOYSA-N 0.000 description 1
LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
BWGNESOTFCXPMA-UHFFFAOYSA-N Dihydrogen disulfide Chemical compound SS BWGNESOTFCXPMA-UHFFFAOYSA-N 0.000 description 1
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
238000002835 absorbance Methods 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
238000000862 absorption spectrum Methods 0.000 description 1
239000003929 acidic solution Substances 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
229910001854 alkali hydroxide Inorganic materials 0.000 description 1
150000008044 alkali metal hydroxides Chemical class 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
239000012472 biological sample Substances 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
230000007547 defect Effects 0.000 description 1
238000001035 drying Methods 0.000 description 1
239000008151 electrolyte solution Substances 0.000 description 1
238000000921 elemental analysis Methods 0.000 description 1
230000007613 environmental effect Effects 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
230000005764 inhibitory process Effects 0.000 description 1
238000005342 ion exchange Methods 0.000 description 1
238000005259 measurement Methods 0.000 description 1
238000002844 melting Methods 0.000 description 1
230000008018 melting Effects 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
238000000034 method Methods 0.000 description 1
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
229940072033 potash Drugs 0.000 description 1
229910052700 potassium Inorganic materials 0.000 description 1
239000011591 potassium Substances 0.000 description 1
BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
235000015320 potassium carbonate Nutrition 0.000 description 1
238000004094 preconcentration Methods 0.000 description 1
238000000425 proton nuclear magnetic resonance spectrum Methods 0.000 description 1
239000008213 purified water Substances 0.000 description 1
238000011084 recovery Methods 0.000 description 1
238000001953 recrystallisation Methods 0.000 description 1
239000012266 salt solution Substances 0.000 description 1
229910001961 silver nitrate Inorganic materials 0.000 description 1
235000010265 sodium sulphite Nutrition 0.000 description 1
AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 description 1
235000019345 sodium thiosulphate Nutrition 0.000 description 1
238000001179 sorption measurement Methods 0.000 description 1
230000003595 spectral effect Effects 0.000 description 1
238000001228 spectrum Methods 0.000 description 1
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
229910052717 sulfur Inorganic materials 0.000 description 1
239000011593 sulfur Substances 0.000 description 1
239000006228 supernatant Substances 0.000 description 1
VLLMWSRANPNYQX-UHFFFAOYSA-N thiadiazole Chemical compound C1=CSN=N1.C1=CSN=N1 VLLMWSRANPNYQX-UHFFFAOYSA-N 0.000 description 1
238000001291 vacuum drying Methods 0.000 description 1

Landscapes

Nitrogen- Or Sulfur-Containing Heterocyclic Ring Compounds With Rings Of Six Or More Members (AREA)

JP59032971A 1984-02-23 1984-02-23 チアジアゾ−ル誘導体 Granted JPS60178871A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP59032971A JPS60178871A (ja)	1984-02-23	1984-02-23	チアジアゾ−ル誘導体

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP59032971A JPS60178871A (ja)	1984-02-23	1984-02-23	チアジアゾ−ル誘導体

Publications (2)

Publication Number	Publication Date
JPS60178871A true JPS60178871A (ja)	1985-09-12
JPH0533225B2 JPH0533225B2 (2)	1993-05-19

Family

ID=12373783

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP59032971A Granted JPS60178871A (ja)	1984-02-23	1984-02-23	チアジアゾ−ル誘導体

Country Status (1)

Country	Link
JP (1)	JPS60178871A (2)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN104610483A (zh) *	2015-02-05	2015-05-13	浙江工商大学	对Hg(II)具有选择性吸附的螯合功能树脂的制备法

1984
- 1984-02-23 JP JP59032971A patent/JPS60178871A/ja active Granted

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
CHEMICAL ABSTRACTS=1966 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN104610483A (zh) *	2015-02-05	2015-05-13	浙江工商大学	对Hg(II)具有选择性吸附的螯合功能树脂的制备法

Also Published As

Publication number	Publication date
JPH0533225B2 (2)	1993-05-19

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