JPS606799A - Manufacture of powerful detergent from rice bran as raw material - Google Patents
Manufacture of powerful detergent from rice bran as raw materialInfo
- Publication number
- JPS606799A JPS606799A JP10245583A JP10245583A JPS606799A JP S606799 A JPS606799 A JP S606799A JP 10245583 A JP10245583 A JP 10245583A JP 10245583 A JP10245583 A JP 10245583A JP S606799 A JPS606799 A JP S606799A
- Authority
- JP
- Japan
- Prior art keywords
- raw material
- detergent
- agent
- detergents
- mucin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000003599 detergent Substances 0.000 title claims description 24
- 239000002994 raw material Substances 0.000 title claims description 15
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- 235000007164 Oryza sativa Nutrition 0.000 title description 4
- 235000009566 rice Nutrition 0.000 title description 4
- 240000007594 Oryza sativa Species 0.000 title 1
- 239000003795 chemical substances by application Substances 0.000 claims description 21
- 230000000813 microbial effect Effects 0.000 claims description 6
- 235000020183 skimmed milk Nutrition 0.000 claims description 5
- 244000005700 microbiome Species 0.000 claims description 3
- 150000002632 lipids Chemical class 0.000 claims description 2
- 229920001282 polysaccharide Polymers 0.000 claims 3
- 239000005017 polysaccharide Substances 0.000 claims 3
- 150000004804 polysaccharides Chemical class 0.000 claims 3
- OMDQUFIYNPYJFM-XKDAHURESA-N (2r,3r,4s,5r,6s)-2-(hydroxymethyl)-6-[[(2r,3s,4r,5s,6r)-4,5,6-trihydroxy-3-[(2s,3s,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-2-yl]methoxy]oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O[C@H]2[C@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)[C@H](O)[C@H](O)[C@H](O)O1 OMDQUFIYNPYJFM-XKDAHURESA-N 0.000 claims 1
- 239000004382 Amylase Substances 0.000 claims 1
- 102000013142 Amylases Human genes 0.000 claims 1
- 108010065511 Amylases Proteins 0.000 claims 1
- 229920000926 Galactomannan Polymers 0.000 claims 1
- 229920000715 Mucilage Polymers 0.000 claims 1
- 229920001284 acidic polysaccharide Polymers 0.000 claims 1
- 150000004805 acidic polysaccharides Chemical class 0.000 claims 1
- 239000000853 adhesive Substances 0.000 claims 1
- 235000019418 amylase Nutrition 0.000 claims 1
- 230000007935 neutral effect Effects 0.000 claims 1
- 235000013311 vegetables Nutrition 0.000 claims 1
- 239000003921 oil Substances 0.000 description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 238000004140 cleaning Methods 0.000 description 6
- 239000003925 fat Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 235000013336 milk Nutrition 0.000 description 5
- 239000008267 milk Substances 0.000 description 5
- 210000004080 milk Anatomy 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000000271 synthetic detergent Substances 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000003208 petroleum Substances 0.000 description 4
- 239000000344 soap Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 241000209094 Oryza Species 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 241000251468 Actinopterygii Species 0.000 description 2
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 2
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 2
- 235000013365 dairy product Nutrition 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 235000014593 oils and fats Nutrition 0.000 description 2
- 210000003296 saliva Anatomy 0.000 description 2
- 239000001632 sodium acetate Substances 0.000 description 2
- 235000017281 sodium acetate Nutrition 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000002351 wastewater Substances 0.000 description 2
- 201000004624 Dermatitis Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000003977 dairy farming Methods 0.000 description 1
- 238000004042 decolorization Methods 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000009629 microbiological culture Methods 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000001850 reproductive effect Effects 0.000 description 1
- 238000007788 roughening Methods 0.000 description 1
- 239000013535 sea water Substances 0.000 description 1
- 235000015170 shellfish Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000013042 solid detergent Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
Abstract
(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。(57) [Summary] This bulletin contains application data before electronic filing, so abstract data is not recorded.
Description
【発明の詳細な説明】
本発明は、先に提出した昭和５２年特許願１０８５８２
号審判昭和５６年第２２１０４号、及び昭和５６年特許
願第１７８１８４号に関連するもの＼改良に関するもの
であって、種々な物質に付着した汚れ落しに効果のある
ムチンの粗剤と微生物油脂を原料として作られた脂質性
洗剤の粗剤との２￥ｆｌ剤を組み合せて作る洗剤の製法
に関する。DETAILED DESCRIPTION OF THE INVENTION The present invention is based on patent application no.
Related to Trial No. 22104 of 1982 and Patent Application No. 178184 of 1988 ＼Regarding improvement, the mucin crude agent and microbial oil are effective in removing stains attached to various substances. This invention relates to a method for producing a detergent by combining a crude lipid detergent prepared as a raw material with a 2￥fl agent.
従来より販売されている洗剤は石油を主原料として合成
されたものであって、洗浄力を増強化するためＡＥＳ、
ＬＢＳ製品を冷加混入している。この添加剤は石油か
らアルキベンゼンを合成し、更に、これをスルホン化し
た後に苛性ソーダで中和する過程を経てきているもので
、ＡＢＳ、 ＬＢＳ系高級アルコール系の合成洗剤や現
在の石鹸は共に洗浄力増強剤が添加されているので、使
扇することによシ手の皮膚が荒れたシ湿しんが発生した
シする〇これは合成洗剤が厚い布地の内部まで浸透して
汚汚れを除去する界面活性剤の働きで被讐を受けるもの
である。又、この合成洗剤が湖水や河川に混入すると、
生殖中の植物や魚類などにも多大な被害が発生する欠点
がある。Detergents that have been sold in the past are synthesized using petroleum as the main raw material, and they contain AES, AES, etc. to enhance their cleaning power.
LBS products are mixed in cold. This additive is made by synthesizing alkybenzene from petroleum, sulfonating it, and then neutralizing it with caustic soda, and is used in both ABS and LBS-based higher alcohol-based synthetic detergents and current soaps. Since a detergent enhancer is added, using a fan can cause rough skin on the hands and eczema.This is because the synthetic detergent penetrates deep into thick fabrics and removes dirt. It is attacked by the action of surfactants. Also, if this synthetic detergent gets mixed into lake water or rivers,
The drawback is that it also causes great damage to reproductive plants and fish.
又、染色や塗料などの容易に変色とか、脱色を防止する
色比を施しである洗物でも損傷することがある。この弊
害を防止するためには製品の洗浄効果が低下する。洗浄
効果が強い程被害が犬となる。 前述したように、洗剤
の使用後の排水が河川、湖沼、海水に流れ込むと、長く
残留し環境汚染とか魚貝類に被害を力え、大きな問題に
なっている。 この合成洗剤の原料になっている石油は
、その産出量の９０％を燃料として消費している現況で
あるが、埋蔵量にも限度があシ、いづれ涸渇するので、
洗剤の原料に利用することが停＋）ｉれる時期もあまり
遠くないであろう。In addition, washing clothes that are dyed or painted with a color ratio that prevents discoloration or decolorization may also cause damage. In order to prevent this harmful effect, the cleaning effect of the product is reduced. The stronger the cleaning effect, the more damage will be caused. As mentioned above, when wastewater from detergents flows into rivers, lakes, and seawater, it remains for a long time and causes environmental pollution and damage to fish and shellfish, creating a serious problem. At present, 90% of the petroleum that is produced as a raw material for synthetic detergents is consumed as fuel, but there is a limit to the amount of petroleum that is produced, and it will eventually run out.
It will probably not be long before the use of it as a raw material for detergents ceases.
次に、石鹸の原料は油脂であシ、この資源は食糧事情に
よシ需給のバランスがくづれると価格の変動が激しく、
原料としては資源が不足という欠点がある。Next, the raw material for soap is oil and fat, and this resource is subject to rapid price fluctuations when the supply and demand balance collapses due to food conditions.
The disadvantage is that there are insufficient resources as raw materials.
この発明は、以上述べたような従来の欠点を排除するも
のである。The present invention eliminates the drawbacks of the prior art as described above.
先に提出した昭和５６年特許願第１７８１８４号のクリ
ーニング用洗剤組成物の製法では、一般の汚れ物の洗濯
に使用する製法に関するものであるが、本発明は油１１
斤性汚れにも一般汚れにも効果ある洗剤で、種々の物質
に付着した汚れを取り去るために改良したもので、２剤
を組み合せてそれぞれの用途に応じ粉末果粒、溶液体、
固形などの洗剤を製造するもので、この動機となったの
は、通常では繊維製品などに付着したシミ汚れを除去す
るには、ギの汚染の状態を判別するため、汚ねの一部分
を純水で浸してシミの状態とその変化をよく調べて処理
する。たまた首、氷で浸すところを人間の唾液を代用し
たところ、汚れが良く分解されて除去され、生地にも異
状がなかった。The method for manufacturing a cleaning detergent composition disclosed in Patent Application No. 178184 filed earlier in 1984 is related to a manufacturing method for use in washing general soiled items, but the present invention relates to a method for manufacturing a cleaning detergent composition for general use in washing dirty items.
It is a detergent that is effective for both crumbly stains and general stains, and has been improved to remove stains attached to various substances.The two agents can be combined to produce powder, solution, or powder depending on the application.
The company manufactures detergents such as solid detergents, and the reason for this was that normally, in order to remove stains from textiles, etc., a portion of the stain must be purified to determine the state of contamination. Soak it in water, carefully examine the condition of the stain and its changes, and then treat it. When we substituted human saliva for the neck, which was soaked in ice, the dirt was well broken down and removed, and there was no problem with the fabric.
この効果は唾液の含有する主成分ムチンの化学作用であ
る事が判明し、原料の研死分析実験の結果、米糠がムチ
ン生成分を大量に含有することを知り、ムチンを米糠か
ら抽出し洗剤の原料とする本発明をしたものである。It was discovered that this effect was due to the chemical action of mucin, the main component contained in saliva, and as a result of a grinding analysis experiment of raw materials, it was learned that rice bran contains a large amount of mucin-forming components, so mucin was extracted from rice bran and used in detergents. The present invention uses it as a raw material.
米糠の約３倍数の水を混入し、この量の１％の酢酸ナト
リュウムを入れ室温下の状態にて、ミキサーによ９２〜
３時間位にて抽出する。Mix about 3 times as much water as rice bran, add this amount of 1% sodium acetate, and mix in a mixer at room temperature.
Extract in about 3 hours.
不溶解部については１０．００Ｏｒ、ｐ、ｍで約２０分
間位遠心分離器で処理することによシ、はソ透明となっ
た抽出液を得ることができる。For the undissolved portion, a transparent extract can be obtained by processing it in a centrifuge at 10.00 Or, p, m for about 20 minutes.
この抽出液の全量の３倍量の、エナールアルコール１％
含有を温度４°Ｃ位の状態で添加し、これを攪拌した後
、数時間放置して、又、遠心分離機にて処理する事によ
り沈澱させる。この沈澱したものに約１０倍量の水（１
％酢酸ナトリュウム含有）にてＭｍさせて再度攪拌、し
て溶解せしめ、少量の不溶部分を遠心分離器で除去する
。Enal alcohol 1% in 3 times the total amount of this extract
The mixture is added at a temperature of about 4°C, stirred, left to stand for several hours, and precipitated by treatment with a centrifuge. About 10 times the amount of water (1
% sodium acetate), stir again to dissolve, and a small amount of insoluble portion is removed using a centrifuge.
次に、簿渇色上溝液にエタノールを６０〜７０％を加え
、これを数時間放置後、遠心分離器にかけて沈澱したも
のを集める。この操作を数回繰シ返す。Next, 60 to 70% ethanol is added to the dry liquid, left to stand for several hours, and then centrifuged to collect the precipitate. Repeat this operation several times.
その後、淡水に溶解し、これを凍結、乾燥させてから粉
末にし洗剤を作るのである。It is then dissolved in fresh water, frozen, dried, and powdered to make detergent.
本発明は、この方法によって作られた材料を素剤として
、これに別途の方法にて作製した。In the present invention, the material produced by this method was used as a base material and was produced by a separate method.
それは、微生物油脂を原料に作られた素剤の２剤を組み
合せて作る、架剤の改良とも言うべきものである。It can be said to be an improved cross-agent made by combining two base agents made from microbial fats and oils.
一般的な汚れ落しに使用するものと、油性による汚れに
使用するもの＼２剤を、従来の洗剤の有する欠点を排除
した方法によシ混合して作られた素剤である。This is a base agent made by mixing two agents, one used for general stain removal and one used for oily stains, in a method that eliminates the drawbacks of conventional detergents.
次に、微生物油脂の製法については、脱脂乳を微生物培
養の液に用いるものである。とれを素材とすることは、
牛乳の増産の一役となるのと、洗剤の原料に使用する油
脂の不足を補うためでもある。 牛乳からは種々の乳製
品が加工される。その際の脂肪を採集した脱脂乳を使用
するものである。その製法は脱脂乳に酵母を混入し発酵
槽に入れ、２５°Ｃ位で２０〜２５時間で発酵槽の中の
脱脂乳に酵母によシ微生物を発酵培養して微生物油脂を
作シ、その油脂に苛性ソーダを中オロ、させて、石鹸粗
剤を作る。該粗剤、は油性汚れを除去するのに優れた性
質がある。これにムチン粗剤を組み合せた事によシ、こ
の２剤の主成分は互いに助は融和の状態となって、一段
と洗浄力の効果を向上発揮することになる。この開発に
よって、在来の洗剤の如く被洗物を損−傷したシ、その
他、前記のような障害を発生する欠点を無くすると共に
、未熟練者でも安心して使用可能となるものである。Next, regarding the method for producing microbial fats and oils, skim milk is used as a microbial culture solution. Using tore as a material means that
This is to help increase milk production and to compensate for the shortage of oils and fats used as raw materials for detergents. Various dairy products are processed from milk. Skimmed milk from which the fat is collected is used. The manufacturing method is to mix yeast into skim milk and put it in a fermenter, and ferment and culture microorganisms with yeast in the skim milk in the fermenter at about 25°C for 20 to 25 hours to produce microbial oil. A soap coarsening agent is made by stirring caustic soda into fats and oils. The roughening agent has excellent properties for removing oily stains. By combining this with the mucin coarsening agent, the main components of these two agents are compatible with each other, and the cleaning power is further improved. This development eliminates the drawbacks of conventional detergents that cause damage to the items to be washed and other problems mentioned above, and allows even unskilled people to use the detergent with peace of mind.
以上の２剤を同量ずつ組み合わせ加ニレ、用途に応じて
使用上便利に溶液状、粉末、果粒状、固形、噴霧容器入
れ等とし製品化するものである。The above two agents are combined in equal amounts to produce a product in the form of a solution, powder, granule, solid, spray container, etc., depending on the purpose.
この発明は、素ムチン粗剤と微生物油脂を原料に作られ
た素剤の２剤を絹み合せた洗剤の改良であって、粗剤は
それぞれ単独でも特徴のある洗剤で、素ムチンは、たん
ばく質性の汚れ除去に効果があり、微生物は油脂系汚れ
除去に効果がある石鹸の原料ともなる素材である。This invention is an improvement to a detergent that combines two agents: a raw mucin coarse agent and a base agent made from microbial fats and oils.Each coarse agent has its own characteristics, and the raw mucin It is effective in removing proteinaceous stains, and microorganisms are also a raw material for soap, which is effective in removing oil-based stains.
この２種類の粗剤を組み合せて作る事によって、あらゆ
る物に付着した汚れの除去に効果があり、その上、毒性
は皆無で公害発生の原因となった現在の合成洗剤のよう
な問題を発生しない。By combining these two types of coarsening agents, it is effective in removing dirt from all kinds of objects, and it is completely non-toxic and does not cause problems like the current synthetic detergents that cause pollution. do not.
使用済みの排水を多く放出しても心配のない特徴がある
。 この発明は前記の如く、粗剤を組み合せて製造され
ていることによって、被洗物の撰別する工程の必要はい
らない、いづれの汚れ除去にも安心して使用可能である
のと、微生物油脂の素材はこれまで食糧油脂を原料にす
るので、原料資源が不足勝ちとなるため牛乳を原料に開
発したもので、近年牛乳の価格が低落している（牛乳生
産量が増大のため）酪農家の赤字経営の改善策ともなる
。 この発明によって、酪農経営の向上に役立つと共に
、洗剤を排水路に放水による被害の発生を阻止し、国民
生活に役立つ発明を提供するものである。It has the feature that there is no need to worry even if a large amount of used wastewater is discharged. As mentioned above, this invention is manufactured by combining coarsening agents, so there is no need for a process of sorting the items to be washed, and it can be safely used for removing any kind of dirt. Up until now, the material has been made from food oils and fats, but because of the shortage of raw material resources, it was developed using milk as a raw material.In recent years, the price of milk has fallen (due to an increase in milk production), so dairy farmers are It also serves as a measure to improve deficit management. This invention not only helps improve dairy farming management, but also prevents damage caused by spraying detergent into drains, thereby providing an invention that is useful for people's lives.
特許出願人 北 畠 三 之 丞Patent applicant Sanjo Kitabatake
Claims (1)
し、これに約６０ｑ６の中性植物多糖としてのグリコマ
ンナン、及びガラクトマンナン約２０％〜２５チとの多
糖ベントグリカン、及び酸性多糖、ないし、とれら多糖
とアミラーゼと複合体からなるものによシ抽出したムチ
ン粗剤を作シ、これに微生物油脂を原料にして作られた
油脂性洗剤の粗剤とを組み合せて作ることを特徴とした
洗剤の製法。 ２、脱脂牛乳の中に油脂性微生物を培養し、出来た微生
物油脂を原料に脂質洗剤の粗剤を作シ、これにムチン粗
剤とを組み合せて作る特許請求の範囲第１項に記載の洗
剤の製法。[Claims] 1. O'° bran containing the main component of vegetable mucilage is used as a raw material, and glycomannan as a neutral plant polysaccharide of about 60q6 and galactomannan about 20% to 25% are added to this. A mucin crude agent is extracted from polysaccharide bentoglycan, acidic polysaccharide, or a complex of these polysaccharides and amylase. A detergent manufacturing method characterized by combining detergents with detergents. 2.Cultivating oil-based microorganisms in skimmed milk, producing a rough agent for lipid detergent using the resulting microbial oil as a raw material, and combining this with a rough agent for mucin according to claim 1. Detergent manufacturing method.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10245583A JPS606799A (en) | 1983-06-07 | 1983-06-07 | Manufacture of powerful detergent from rice bran as raw material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10245583A JPS606799A (en) | 1983-06-07 | 1983-06-07 | Manufacture of powerful detergent from rice bran as raw material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS606799A true JPS606799A (en) | 1985-01-14 |
Family
ID=14327939
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10245583A Pending JPS606799A (en) | 1983-06-07 | 1983-06-07 | Manufacture of powerful detergent from rice bran as raw material |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS606799A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8119583B2 (en) * | 2008-04-09 | 2012-02-21 | Solazyme, Inc. | Soaps produced from oil-bearing microbial biomass and oils |
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