JPS622577B2 - - Google Patents

Info

Publication number: JPS622577B2
Authority: JP; Japan
Prior art keywords: carbonation; phenate; carbon dioxide; alkali metal; sodium
Prior art date: 1979-07-02
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP8274679A

Other languages

English (en)

Japanese (ja)

Other versions

JPS5610139A (en

Inventor

Rojaa Mooru Yuujin

Chaaresu Makudonarudo Debitsudo

Uirunaa Josefu

Rii Buritsugusu Rojaa

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Dow Chemical Co

Original Assignee

Dow Chemical Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1979-07-02

Filing date

1979-07-02

Publication date

1987-01-20

1979-07-02 Application filed by Dow Chemical Co filed Critical Dow Chemical Co

1979-07-02 Priority to JP8274679A priority Critical patent/JPS5610139A/ja

1981-02-02 Publication of JPS5610139A publication Critical patent/JPS5610139A/ja

1987-01-20 Publication of JPS622577B2 publication Critical patent/JPS622577B2/ja

Status Granted legal-status Critical Current

Links

CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 87
229910002092 carbon dioxide Inorganic materials 0.000 claims description 42
239000001569 carbon dioxide Substances 0.000 claims description 42
238000000034 method Methods 0.000 claims description 40
229910052783 alkali metal Inorganic materials 0.000 claims description 34
150000001340 alkali metals Chemical class 0.000 claims description 28
NESLWCLHZZISNB-UHFFFAOYSA-M sodium phenolate Chemical compound [Na+].[O-]C1=CC=CC=C1 NESLWCLHZZISNB-UHFFFAOYSA-M 0.000 claims description 21
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 13
239000007787 solid Substances 0.000 claims description 8
-1 alkali metal carboxylate Chemical class 0.000 claims description 6
229910052757 nitrogen Inorganic materials 0.000 claims description 6
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 2
238000001694 spray drying Methods 0.000 claims description 2
239000007790 solid phase Substances 0.000 claims 1
238000006243 chemical reaction Methods 0.000 description 36
239000000047 product Substances 0.000 description 28
238000012360 testing method Methods 0.000 description 13
ABBQHOQBGMUPJH-UHFFFAOYSA-M Sodium salicylate Chemical compound [Na+].OC1=CC=CC=C1C([O-])=O ABBQHOQBGMUPJH-UHFFFAOYSA-M 0.000 description 10
239000002245 particle Substances 0.000 description 9
229960004025 sodium salicylate Drugs 0.000 description 9
150000002989 phenols Chemical class 0.000 description 7
239000000843 powder Substances 0.000 description 7
238000002474 experimental method Methods 0.000 description 6
YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 6
238000001816 cooling Methods 0.000 description 5
238000010438 heat treatment Methods 0.000 description 5
238000002156 mixing Methods 0.000 description 5
ZLVSYODPTJZFMK-UHFFFAOYSA-M sodium 4-hydroxybenzoate Chemical compound [Na+].OC1=CC=C(C([O-])=O)C=C1 ZLVSYODPTJZFMK-UHFFFAOYSA-M 0.000 description 5
238000003756 stirring Methods 0.000 description 5
238000012546 transfer Methods 0.000 description 5
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
239000007864 aqueous solution Substances 0.000 description 4
150000001735 carboxylic acids Chemical class 0.000 description 4
239000012530 fluid Substances 0.000 description 4
239000000376 reactant Substances 0.000 description 4
229910052708 sodium Inorganic materials 0.000 description 4
239000011734 sodium Substances 0.000 description 4
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
239000002253 acid Substances 0.000 description 3
238000005054 agglomeration Methods 0.000 description 3
230000002776 aggregation Effects 0.000 description 3
229910002090 carbon oxide Inorganic materials 0.000 description 3
150000007942 carboxylates Chemical class 0.000 description 3
150000001732 carboxylic acid derivatives Chemical class 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
239000011261 inert gas Substances 0.000 description 3
FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 3
229960004889 salicylic acid Drugs 0.000 description 3
150000003839 salts Chemical class 0.000 description 3
239000002904 solvent Substances 0.000 description 3
239000007858 starting material Substances 0.000 description 3
125000001424 substituent group Chemical group 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
238000004458 analytical method Methods 0.000 description 2
239000006227 byproduct Substances 0.000 description 2
230000000052 comparative effect Effects 0.000 description 2
238000007796 conventional method Methods 0.000 description 2
125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
239000012535 impurity Substances 0.000 description 2
229910052751 metal Inorganic materials 0.000 description 2
239000002184 metal Substances 0.000 description 2
239000000203 mixture Substances 0.000 description 2
230000020477 pH reduction Effects 0.000 description 2
239000000243 solution Substances 0.000 description 2
229910001220 stainless steel Inorganic materials 0.000 description 2
239000010935 stainless steel Substances 0.000 description 2
VGVRPFIJEJYOFN-UHFFFAOYSA-N 2,3,4,6-tetrachlorophenol Chemical class OC1=C(Cl)C=C(Cl)C(Cl)=C1Cl VGVRPFIJEJYOFN-UHFFFAOYSA-N 0.000 description 1
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
230000004913 activation Effects 0.000 description 1
150000008044 alkali metal hydroxides Chemical class 0.000 description 1
125000000217 alkyl group Chemical group 0.000 description 1
125000003277 amino group Chemical group 0.000 description 1
239000008346 aqueous phase Substances 0.000 description 1
150000001601 aromatic carbocyclic compounds Chemical class 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
238000010923 batch production Methods 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
239000000470 constituent Substances 0.000 description 1
238000011109 contamination Methods 0.000 description 1
238000010924 continuous production Methods 0.000 description 1
239000000498 cooling water Substances 0.000 description 1
150000001896 cresols Chemical class 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
229910001873 dinitrogen Inorganic materials 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
235000013312 flour Nutrition 0.000 description 1
239000007789 gas Substances 0.000 description 1
238000005469 granulation Methods 0.000 description 1
230000003179 granulation Effects 0.000 description 1
230000005484 gravity Effects 0.000 description 1
125000005843 halogen group Chemical group 0.000 description 1
239000012442 inert solvent Substances 0.000 description 1
229910052500 inorganic mineral Inorganic materials 0.000 description 1
229910052742 iron Inorganic materials 0.000 description 1
238000004811 liquid chromatography Methods 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000000463 material Substances 0.000 description 1
239000011707 mineral Substances 0.000 description 1
125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 1
150000002894 organic compounds Chemical class 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
159000000001 potassium salts Chemical class 0.000 description 1
238000012545 processing Methods 0.000 description 1
238000010926 purge Methods 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
230000009257 reactivity Effects 0.000 description 1
238000011084 recovery Methods 0.000 description 1
238000012552 review Methods 0.000 description 1
159000000000 sodium salts Chemical class 0.000 description 1
238000000859 sublimation Methods 0.000 description 1
230000008022 sublimation Effects 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000013589 supplement Substances 0.000 description 1
239000000725 suspension Substances 0.000 description 1
230000000007 visual effect Effects 0.000 description 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

JP8274679A 1979-07-02 1979-07-02 Carbonation of alkali metal phenates Granted JPS5610139A (en)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP8274679A JPS5610139A (en)	1979-07-02	1979-07-02	Carbonation of alkali metal phenates

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP8274679A JPS5610139A (en)	1979-07-02	1979-07-02	Carbonation of alkali metal phenates

Publications (2)

Publication Number	Publication Date
JPS5610139A JPS5610139A (en)	1981-02-02
JPS622577B2 true JPS622577B2 (de)	1987-01-20

Family

ID=13782983

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP8274679A Granted JPS5610139A (en)	1979-07-02	1979-07-02	Carbonation of alkali metal phenates

Country Status (1)

Country	Link
JP (1)	JPS5610139A (de)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4376867A (en) *	1981-07-07	1983-03-15	Gert Jansen	Chemical process
IL69282A (en) *	1982-09-02	1988-06-30	Euro Celtique Sa	Method for the carboxylation of potassium phenoxide with carbon dioxide

1979
- 1979-07-02 JP JP8274679A patent/JPS5610139A/ja active Granted

Also Published As

Publication number	Publication date
JPS5610139A (en)	1981-02-02

Publication	Publication Date	Title
US2823230A (en)	1958-02-11	Process for preparing terephthalic acid
US2891992A (en)	1959-06-23	Process for the rearrangement of salts of aromatic or heterocyclic carboxylic acids
JPS622577B2 (de)	1987-01-20
US2580931A (en)	1952-01-01	Production of sebacic acid
CA1226874A (en)	1987-09-15	Carboxylation of metal aryloxides
US4171453A (en)	1979-10-16	Carbonation of alkali metal phenates
US2948750A (en)	1960-08-09	Process for the introduction of carboxyl groups into aromatic hydrocarbons
JPS58172347A (ja)	1983-10-11	芳香族ヒドロキシカルボン酸類の製造方法
CA1126290A (en)	1982-06-22	Carbonation of alkali metal phenates
JPH03130243A (ja)	1991-06-04	グリコールエーテルの調製方法
US3816521A (en)	1974-06-11	Process for the production of p-hydroxy benzoic acid
US4529817A (en)	1985-07-16	Process for preparing aromatic hydroxycarboxylic acids
GB2053186A (en)	1981-02-04	Carbonation of alkali metal phenates
US3089905A (en)	1963-05-14	Process for the production of 4-hydroxyisophthalic acid
US5859149A (en)	1999-01-12	Production of solid polyaspartate salt
RU2029759C1 (ru)	1995-02-27	Способ получения солей насыщенных карбоновых кислот или их смесей
US3746752A (en)	1973-07-17	Process for preparation of aromatic carboxylates
US4230885A (en)	1980-10-28	Conversion of aromatic carboxylates to terephthalate
US2823228A (en)	1958-02-11	Process for the transformation of di-
US5001245A (en)	1991-03-19	Process for producing metallic salt of ethercarboxylic acid
US3955961A (en)	1976-05-11	Carboxylate metals process
US3359310A (en)	1967-12-19	Process for producing potassium malonate
US2703812A (en)	1955-03-08	Carbonation of resorcinol
JPS594427B2 (ja)	1984-01-30	Ｓ−メチルｎ−〔（メチル−カルバモイル）オキシ〕チオアセトイミデ−トの製造法
EP1232136B1 (de)	2005-10-19	Alkyl-carboxylat-salze als lösungsmittel für henkel-verwandte prozesse