JPS6234401B2 - - Google Patents
Info
- Publication number
- JPS6234401B2 JPS6234401B2 JP57111846A JP11184682A JPS6234401B2 JP S6234401 B2 JPS6234401 B2 JP S6234401B2 JP 57111846 A JP57111846 A JP 57111846A JP 11184682 A JP11184682 A JP 11184682A JP S6234401 B2 JPS6234401 B2 JP S6234401B2
- Authority
- JP
- Japan
- Prior art keywords
- strips
- thin plate
- sheet metal
- strip
- packing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/32—Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/322—Basic shape of the elements
- B01J2219/32203—Sheets
- B01J2219/32224—Sheets characterised by the orientation of the sheet
- B01J2219/32227—Vertical orientation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/322—Basic shape of the elements
- B01J2219/32203—Sheets
- B01J2219/32265—Sheets characterised by the orientation of blocks of sheets
- B01J2219/32268—Sheets characterised by the orientation of blocks of sheets relating to blocks in the same horizontal level
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/322—Basic shape of the elements
- B01J2219/32286—Grids or lattices
- B01J2219/32289—Stretched materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/324—Composition or microstructure of the elements
- B01J2219/32408—Metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/324—Composition or microstructure of the elements
- B01J2219/32483—Plastics
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S261/00—Gas and liquid contact apparatus
- Y10S261/72—Packing elements
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/12—All metal or with adjacent metals
- Y10T428/12361—All metal or with adjacent metals having aperture or cut
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Gas Separation By Absorption (AREA)
Description
【発明の詳細な説明】
本発明は、複数の薄板格子から構成され、各格
子がほぼジグザグ状に曲げられて格子面に対して
傾斜する薄板条片から成り、これらの薄板条片が
曲げ個所で一体につながつてそこに格子の面状交
差個所を形成している、物質交換塔用充填物およ
びその製造方法に関する。DETAILED DESCRIPTION OF THE INVENTION The invention consists of a plurality of sheet metal grids, each grid consisting of sheet metal strips bent in a substantially zigzag manner and inclined with respect to the plane of the grid; The present invention relates to a packing for a mass exchange column, which is integrally connected to form a planar intersection of a lattice therein, and a method for manufacturing the same.
系統的に構成されているこの種の充填物は、精
留および吸収のために使用されかつ液相と気相
(または蒸気相)との間の物質交換に役立ち、物
質交換と同時に熱交換も行なわれる。充填物の目
的は特に、物質および熱交換のためにできるだけ
大きい液面が得られるように液体を分布させるこ
とである。 Systemically constructed packings of this type are used for rectification and absorption and serve for mass exchange between the liquid phase and the gas phase (or vapor phase), and at the same time they also carry out heat exchange. It is done. The purpose of the packing is, inter alia, to distribute the liquid so that as large a liquid surface as possible is obtained for mass and heat exchange.
冒頭に挙げた種類の充填物はドイツ連邦共和国
特許出願公開第2005295号明細書から公知であ
る。この公知の充填物は、互いに交差してあるい
は不規則な位置に設けられた複数の薄板格子対か
ら構成されている。1対の両薄板格子のそれぞれ
はほぼジグザグ状に曲がつた薄板条片から成り、
これらの薄板条片はその曲がり個所において一体
につながつておりかつそこにおいて格子の平面交
差個所を形成している。 A filling of the type mentioned at the outset is known from DE 2005 295 A1. This known packing consists of a plurality of pairs of laminated grids arranged intersecting each other or in irregular positions. Each of the pair of laminar grids consists of a generally zigzag curved sheet metal strip;
These sheet metal strips join together at their bends and form there the plane intersections of the grid.
このような公知の薄板格子の立体的構成は第1
図から明らかであり、この図は格子網目の拡大斜
視図である。図示した格子網目は、薄板条片3の
ジグザグ状に順次に続く2つの薄片1,2と隣接
の薄板条片6のジグザグ状に続く2つの薄片4,
5とにより形成されている。薄片1,4および
2,5をつないでいる曲げ個所7,8は格子の平
面交差個所を形成している。格子面として平面A
が記入されており、この平面内に格子の平面交差
個所7,8の中心9,10が位置している。薄片
1,2,4,5は、他のすべての薄片のように、
格子面Aに対して角度α傾斜しており、各薄片の
一部が格子面Aの上に位置し、一部が格子面Aの
下に位置している。格子面Aに対して平行な薄板
格子の両区画面はA′およびA″で示されている。
薄板条片3の条片幅はsで示され、厚さはtで示
され、ほぼ菱形の格子網目の大きい方の対角線は
uで示されている。隣接するジグザグ状薄板条片
3,6が交差個所7,8において互いになす角
度、すなわち格子網目の菱形の小さい方の角度は
βで示されている。 The three-dimensional configuration of such a known thin plate lattice is the first
It is clear from the figure, which is an enlarged perspective view of the lattice network. The illustrated lattice network consists of two zigzag-like successive laminae 1, 2 of a sheet metal strip 3, two zigzag-like successive laminae 4 of an adjacent sheet metal strip 6,
5. The bends 7, 8 connecting the lamellas 1, 4 and 2, 5 form plane intersections of the grid. Plane A as a lattice plane
is written, and the centers 9, 10 of the plane intersection points 7, 8 of the grid are located within this plane. Flakes 1, 2, 4, 5, like all other flakes,
It is inclined at an angle α with respect to the lattice plane A, with a portion of each flake located above the lattice plane A and a portion below the lattice plane A. The two sections of the sheet grating parallel to the grating plane A are designated A' and A''.
The strip width of the sheet metal strip 3 is designated s, the thickness is designated t, and the larger diagonal of the approximately diamond-shaped grid network is designated u. The angle that adjacent zigzag-shaped sheet metal strips 3, 6 make with respect to each other at the points of intersection 7, 8, ie the smaller angle of the rhombus of the lattice network, is designated by β.
公知の薄板格子は、エキスパンドメタルの仕方
で製造され、すなわち帯が複数の個所でつながつ
ている平行な条片に切断されて、互いに隣接する
条片をつないでいる切断線部分が同じ長さを持ち
かつこの長さの半分だけ隣接する切断線部分に対
してずらされている。これらの条片を引き離すこ
とにより上述の薄板格子が得られる。 The known sheet metal grid is manufactured in an expanded metal manner, ie the strip is cut into parallel strips that are connected at several points, so that the section lines connecting adjacent strips have the same length. It is held and offset with respect to the adjacent cutting line portion by half this length. By pulling these strips apart, the above-mentioned sheet metal grid is obtained.
冒頭に挙げた種類の充填物の薄板格子は原則と
してエキスパンドメタルと同じやり方で製造され
るが、しかしこの薄板格子は、薄片の幅sがその
厚さtよりはるかに大きく、それに対して通常の
エキスパンドメタルでは格子辺の幅がほぼその厚
さと一致することでこのエキスパンドメタルと異
なつている。 A sheet lattice of fillings of the type mentioned at the outset is produced in principle in the same way as expanded metal, but this sheet lattice is characterized in that the width s of the lamina is much larger than its thickness t, whereas the usual Expanded metal differs from expanded metal in that the width of the lattice sides almost matches its thickness.
冒頭に挙げた充填物は、僅かな材料費で簡単に
大きな充填表面が得られるという利点を持つてい
る。この利点は格子の薄片構造から、すなわち薄
片が、材料費と比して大きい表面を持つ薄板であ
ることから得られる。 The fillings mentioned at the outset have the advantage that large filling surfaces can be easily obtained with low material costs. This advantage results from the laminar structure of the grid, ie because the laminae are thin plates with a large surface area compared to the material cost.
大きい充填物表面の利点は、物質交換のために
次のような場合にしか利用できない。すなわち、
一方では液体が充填物表面全体にわたつて均一に
分布しかつ充填物のすべての薄板条片が全面的に
完全にぬらされるようにし、他方では塔の中を上
昇する気体(または蒸気)が充填物を通過する際
に受ける圧力損失ができるだけ少なく、全気体流
が流れ方向に対して直角に液体上に均一に分布し
て流れかつ気体の部分流が液体との接触なしに充
填物を通つて流れることができないようにしてあ
る場合にしか利用できない。 The advantages of large packing surfaces can only be used for mass exchange in the following cases: That is,
On the one hand, it ensures that the liquid is evenly distributed over the entire packing surface and that all the lamellar strips of the packing are completely wetted, and on the other hand that the gas (or vapor) rising in the column The pressure loss experienced when passing through the material is as low as possible, the entire gas flow flows with a uniform distribution over the liquid at right angles to the flow direction, and a partial flow of the gas passes through the filling without contact with the liquid. It can only be used if it is made so that it cannot flow.
液体の横分布のためには、充填物自体がその構
造により液体を流れ方向に対して直角に分布させ
ることが必要である。すなわち、液体を充填物横
断面にわたつて均一に分布させて供給することは
実際上不可能である。このことが大きい費用をか
けてできたとしても、これだけではまだ充分でな
い。なぜならば、充填物の構造が液体の永続的な
横分布によつてこのような細流形成を回避できな
い場合に、液体が充填物の内部で再び合流して細
流を形成することがあるからである。さらに液体
分布は気体流の助力なしに行なわれるようにして
ある。なぜならば、もしそうでなければ気体荷重
による好ましくない影響が生ずるからである。さ
らに最適な物質交換のために、液体表面が絶えず
更新され、すなわち充填物表面上を流れる液膜が
できるだけ高い程度の乱流を持つようにしなけれ
ばならない。 For lateral distribution of the liquid, it is necessary that the packing itself, by its structure, distributes the liquid at right angles to the flow direction. That is, it is practically impossible to supply liquid in a uniformly distributed manner over the cross-section of the packing. Even if this can be done at great expense, it is still not enough. This is because the liquid may recombine inside the filling to form a rivulet if the structure of the filling cannot avoid such rivulet formation with a permanent lateral distribution of the liquid. . Furthermore, the liquid distribution is arranged to take place without the aid of a gas flow. This is because if this were not the case, undesirable effects due to gas loading would occur. Furthermore, for optimal mass exchange, it must be ensured that the liquid surface is constantly renewed, ie the liquid film flowing over the packing surface has as high a degree of turbulence as possible.
本発明の基礎になつている実験の結果は次の通
りである。すなわち、公知の薄板格子の薄板条片
が流れ方向に対して直角に設けられるならば、塔
内を上昇する気体が充填物を通過する際に受ける
圧力損失は、薄板格子が大きな間隙なしに互いに
並んで配置される場合、非常に大きい。ドイツ連
邦共和国特許出願公開第2005295号明細書から公
知の充填物においては、明らかにこの理由から薄
板格子が規則的に互いに接して設けられるのでは
なくて対にして互いに直角方向に不規則な位置に
設けられている。このことは一方では充填物の小
さい比表面積(充填物体積当りの充填物表面積)
しか得られず、他方では気体のかなりの部分が液
体上の代りに格子対間の間隙を通つて流れるとい
う欠点を持つ。さらに、薄板条片を流れ方向に対
して直角に設ける場合は、液体の少なからざる部
分が薄片特に薄板条片の端部からしたたり落ち、
物質交換に使われないままになつている。薄板条
片が流れ方向に設けられる場合は、上述した欠点
は回避されるが、しかしその場合は液体がジグザ
グ状に延びている薄板条片に沿つて下方へ流れて
行き、薄片の全表面を完全にかつ均一にぬらすた
めに必要な液体の横分布も液体の混合および表面
更新に必要な乱流も得られない。 The results of the experiments that form the basis of the present invention are as follows. That is, if the thin plate strips of the known thin plate grid are arranged at right angles to the flow direction, the pressure drop experienced by the gas rising in the column as it passes through the packing is such that the thin plate grids are connected to each other without large gaps. Very large when placed side by side. Apparently for this reason, in the packing known from DE 2005 295 A1, the laminar grids are not arranged regularly adjacent to each other, but are arranged in pairs at irregular positions at right angles to one another. It is set in. This means, on the one hand, that the specific surface area of the filling is small (filling surface area per filling volume).
On the other hand, it has the disadvantage that a significant portion of the gas flows through the gaps between the grid pairs instead of over the liquid. Furthermore, if the lamellar strips are arranged at right angles to the flow direction, a significant portion of the liquid will drip off the lamellas, especially from the ends of the lamellar strips;
It remains unused for material exchange. The above-mentioned disadvantages are avoided if the lamella strips are arranged in the flow direction, but then the liquid flows downwards along the zigzag-like lamella strips and covers the entire surface of the lamina. Neither the lateral distribution of liquid necessary for complete and uniform wetting nor the turbulence necessary for liquid mixing and surface renewal is obtained.
本発明の課題は、液相を流れ方向に対して直角
に均一に分布させて液相において高い程度の乱流
を発生させかつ気体または蒸気流の圧力損失が充
填物の比表面積の大きい場合にもできるだけ少な
いような冒頭に挙げた種類の簡単にかつ安価に製
造可能な充填物を提供することにある。 The problem of the present invention is to uniformly distribute the liquid phase at right angles to the flow direction, generate a high degree of turbulence in the liquid phase, and reduce the pressure loss of the gas or vapor flow when the specific surface area of the filling is large. The object of the present invention is to provide a filling of the type mentioned at the outset which can be produced simply and inexpensively, with as little as possible.
この課題を解決するため本発明によれば、流れ
方向に延びる薄板条片が、交差個所に流れ案内部
を持ち、この流れ案内部により、薄板条片上を流
下する液相の流れ方向が変化して、液相の一部が
交差個所を経て隣接する薄板条片へ偏向される。
流れ案内部は、各交差個所の両側において薄板条
片外側範囲に設けられる切欠きの縁または各交差
個所の両側において薄板条片に設けられる隆起あ
るいは凹所により形成される。 In order to solve this problem, according to the present invention, the thin plate strips extending in the flow direction have a flow guide section at the intersection point, and the flow guide section changes the flow direction of the liquid phase flowing down on the thin plate strips. A portion of the liquid phase is then deflected through the intersection to the adjacent sheet metal strip.
The flow guides are formed by edges of recesses provided in the outer region of the sheet metal strip on both sides of each crossing point or by elevations or depressions provided in the sheet metal strip on both sides of each crossing point.
こうして本発明により薄板条片が流れ方向に延
びていることにより、高い充填物密度でも気体流
または蒸気流の圧力損失を少なくすることができ
る。また交差個所にある案内部により、薄板条片
上を流下する液相の一部を隣接する薄板条片へ偏
向させることにより、流れ方向に対して直角な方
向への液相の均一な分布および液膜における大き
な乱流が得られ、その結果最適な物質交換が行な
われる。この乱流は、隣接し合う薄板条片上を流
下する液相の一部が案内部のため交差個所で偏向
されて、互いに交差することにより生ずる。 Due to the inventive sheet metal strips extending in the direction of flow, pressure losses in the gas or steam flow can thus be reduced even at high packing densities. In addition, guides at the intersections deflect part of the liquid phase flowing down on the thin plate strips to the adjacent thin plate strips, resulting in a uniform distribution of the liquid phase in the direction perpendicular to the flow direction and High turbulence in the membrane is obtained, resulting in optimal mass exchange. This turbulence is caused by the fact that parts of the liquid phase flowing down on adjacent sheet metal strips are deflected by the guides at the crossing points and cross each other.
本発明の実施例を図面により以下に詳細に説明
する。 Embodiments of the invention will be described in detail below with reference to the drawings.
以下に詳細に説明する充填物はすべて直接互い
に積み重ねられた複数の薄板格子から構成されて
いる。 The packings described in detail below all consist of a plurality of laminated grids stacked directly on top of each other.
第2図、第3図および第4図、第5図に示した
充填物11および12の薄板格子はすべて同じに
構成されかつほぼジグザグ状に曲げられた薄板条
片13ないし17から成り、これらの薄板条片は
曲げ個所18において一体につながつておりかつ
そこにおいて格子の平面交差個所を形成してい
る。各格子の隣接するジグザグ状薄板条片13な
いし17は各交差個所18の両側において外縁に
3角形の切欠き20,21(第2図および第6
図)を持つているので、交差個所に隣接している
薄片の部分は交差個所の方へ先細になつている。
切欠き20,21は、薄板条片がジグザグ状に延
びている方向において薄板条片の幅sより長くか
つこの薄板条片に対して直角方向において条片幅
sの半分より深い。第2図においては、切欠き3
角形の底辺および高さに相当する切欠きの長さお
よび深さがそれぞれgおよびhで示されている。
切欠きの深さhは幅sの半分より大きいから、最
も狭い個所における交差面の幅kは薄板条片の幅
sより小さい。 The sheet metal grids of the packings 11 and 12 shown in FIGS. 2, 3 and 4 and 5 are all constructed identically and consist of approximately zigzag-shaped sheet metal strips 13 to 17, which The sheet metal strips are joined together at the bending points 18 and form there the plane intersections of the grid. Adjacent zigzag-shaped sheet metal strips 13 to 17 of each grid have triangular cutouts 20, 21 (FIGS. 2 and 6) in their outer edges on both sides of each intersection point 18.
), so that the portion of the lamina adjacent to the intersection tapers toward the intersection.
The recesses 20, 21 are longer than the width s of the sheet metal strip in the zigzag direction of the sheet metal strip and deeper than half the strip width s in the direction perpendicular to this sheet metal strip. In Figure 2, notch 3
The length and depth of the cutout corresponding to the base and height of the square are designated g and h, respectively.
Since the depth h of the cutout is greater than half the width s, the width k of the intersection plane at its narrowest point is less than the width s of the sheet metal strip.
例えば第2図、第3図および第4図、第5図に
示したように、薄板格子を別のやり方で規則正し
く互いに積み重ねることができ、その際積み重ね
のやり方に応じて充填度の異なる充填物すなわち
比表面積の異なる充填物が得られる。第2図、第
3図および第4図、第5図においてはそれぞれ第
1の格子の薄片がaで示され、第2の格子の薄片
がbで示され、以下同様に示されている。格子面
は文字A,B等々で示されている。 As shown for example in FIGS. 2, 3 and 4, 5, the sheet metal grids can be stacked one on top of the other in an orderly manner in another way, with fillings having different degrees of filling depending on the stacking method. In other words, fillers with different specific surface areas can be obtained. In FIGS. 2, 3 and 4 and 5, the first lattice lamina is designated a, the second lattice lamina b, and so on. The lattice planes are indicated by letters A, B, etc.
両方の充填物11および12においては、第
1、第3、第5等々の格子a,c,…の薄片が同
じ向きに格子面へ傾斜し、第2、第4、第6等々
の格子b,d,f,…の薄片は逆向きに格子面へ
傾斜している。これは、格子を積み重ねて充填物
11または12を作る際第2、第4等々の格子を
それぞれ格子面において第1、第3等々の格子に
対して180゜回転させることによつて、正確に同
じに構成された格子を用いて実現される。 In both packings 11 and 12, the flakes of the first, third, fifth, etc. gratings a, c, ... are inclined in the same direction to the grating plane, and the second, fourth, sixth, etc. gratings b , d, f, ... are tilted in the opposite direction toward the lattice plane. This can be done precisely by rotating the second, fourth, etc. grids by 180° relative to the first, third, etc. in the grid plane, respectively, when stacking the grids to form the packing 11 or 12. This is realized using identically constructed grids.
充填物11においては、第1、第3、第5等々
の格子a,c,e,…の交差個所の中心が格子面
に対して垂直な共通の一列線上に位置し、第2、
第4、第6等々の格子b,d,f,…の交差個所
の中心が、第1、第3、第5等々の格子a,c,
e,…の網目の中心を通つて延びかつ格子面に対
して垂直な共通の一列線上に位置している。それ
によつて非常に密な充填物、すなわち非常に高い
比表面積の充填物が得られる。この場合格子面に
対して平行な各格子の区画面が、隣接する両格子
の格子面と合致するので、それぞれ3つの順次に
続く格子の全厚さは個々の格子の厚さの2倍にし
か相当しない。 In the filling 11, the centers of the intersections of the first, third, fifth, etc. lattices a, c, e, ... are located on a common line perpendicular to the lattice plane, and the second,
The center of the intersection of the fourth, sixth, etc. lattices b, d, f, ... is the center of the intersection of the first, third, fifth, etc. lattices a, c, etc.
e, ... extending through the center of the mesh and located on a common line perpendicular to the lattice plane. Very dense packings, ie packings with a very high specific surface area, are thereby obtained. In this case, the division plane of each grating parallel to the grating plane coincides with the grating plane of both adjacent gratings, so that the total thickness of each of the three successive gratings is twice the thickness of the individual grating. Only equivalent.
充填物12においては、すべての格子a,b,
c,…の交差個所の中心が共通の一列線上に位置
しており、この充填物は充填物11より小さい比
表面積を有するが、しかしその代りに気相の圧力
損失は少し小さい。 In the packing 12, all the lattices a, b,
The center of the intersection of c, .
充填物は、ジグザグ状に曲げられた薄板条片1
3ないし17が塔の軸線方向に、すなわち液体ま
たは気体が充填物に供給される方向に延びるよう
に塔の中へ挿入される。第2図および第4図にお
いては、液体の流れ方向が矢印22で示され、気
体の流れ方向が矢印22′で示されている。供給
される液体は、第2図に矢印23で示したよう
に、薄板条片13ないし17上を通つて下方へ流
れて行く。第6図に示したように、薄板条片17
上を通つて交差個所18のうちの1つへ流下する
液体23は、先細になつている薄片形状のため
に、交差個所18を横切つて隣接の薄板条片16
へ流れるように導かれる。それによつて液体の最
適な横分布が得られ、隣接の薄板条片16が液体
を導くが(図示せず)、交差個所における両液体
流の最適な混合および表面更新が行なわれる。第
6図に示したように、液体の一部は交差個所の通
過直後に上側の薄片面から切欠き20を区画する
縁24を曲つて下側の薄片面に向かつて流れて行
く。それによつて、液体が両方の薄片面にわたり
かつ両方の薄片面上を流下する液体が交差個所に
おいて常に再び混合されるので、物質交換のため
に非常に大きくかつ絶えず更新される液面が得ら
れることが保証される。 The filling consists of zigzag bent thin plate strips 1
3 to 17 are inserted into the column in such a way that they extend in the axial direction of the column, ie in the direction in which liquid or gas is fed to the packing. In FIGS. 2 and 4, the direction of liquid flow is indicated by arrow 22, and the direction of gas flow is indicated by arrow 22'. The liquid supplied flows downwardly over the sheet metal strips 13 to 17, as indicated by the arrow 23 in FIG. As shown in FIG.
Due to the tapered lamina shape, the liquid 23 flowing down through the top into one of the intersection points 18 flows across the intersection 18 and into the adjacent laminate strip 16.
be guided in a flowing manner. This results in an optimal lateral distribution of the liquid, with the adjoining sheet metal strips 16 conducting the liquid (not shown), and optimal mixing and surface renewal of the two liquid streams at the point of intersection. Immediately after passing the intersection, a portion of the liquid flows from the upper lamella surface around the edge 24 defining the notch 20 toward the lower lamina surface, as shown in FIG. This results in a very large and constantly renewed liquid surface for mass exchange, since the liquid flows over both lamina sides and the liquid flowing down on both lamina sides is always remixed at the point of intersection. This is guaranteed.
一方では切欠き20,21により生ずる交差個
所18における薄板条片13ないし17の狭隘部
により個々の薄板格子における液体の最適な横分
布が得られ、他方では充填物のすべての薄板格子
を直接互いに積み重ねることにより、個々の格子
間に、したがつて格子面に対して直角方向に僅か
ではあるが或る程度の液体の横分布が得られかつ
隣接の格子の液体流間に相互作用が得られる。こ
の場合、特に充填物11においては或る程度の乱
流も生ずる。なぜならば第2図において矢印23
により示された液体流が隣接する格子の互いに接
触する薄片に向かつて互いに或る角度をなして流
れるからである。 On the one hand, the narrowing of the sheet metal strips 13 to 17 at the intersection point 18 caused by the recesses 20, 21 results in an optimal lateral distribution of the liquid in the individual sheet metal grids, and on the other hand, all the sheet metal grids of the filling are connected directly to one another. Stacking provides a slight but certain lateral distribution of liquid between the individual grids and thus perpendicular to the plane of the grid and interaction between the liquid streams of adjacent grids. . In this case, a certain degree of turbulence also occurs, especially in the packing 11. This is because arrow 23 in Figure 2
This is because the liquid streams represented by are directed toward mutually contacting laminae of adjacent grids at an angle to each other.
充填物11,12により気相または蒸気相にお
いて乱流および良好な横分布が得られる。これは
特に、隣接する格子の薄片は互いに傾斜しており
かつ充填物11においてはさらに薄片が隣接の格
子の網目に突出しているからである。 The packings 11, 12 provide turbulent flow and good lateral distribution in the gas or vapor phase. This is particularly because the lamina of adjacent lattices are inclined with respect to each other and in the filling 11 the lamina furthermore protrude into the mesh of the adjacent lattice.
充填物11は特に、非常に高い比表面積を持ち
かつそれにもかかわらず気相において僅かな圧力
損失しか引き起こさないという理由から、精留お
よび吸収の通常の使用に特に有利であることが判
明した。それに対して、極めて低い圧力のもとで
作業しなければならない特別の使用目的のために
は充填物12の方が適している。 Packing 11 has proven to be particularly advantageous for customary applications in rectification and absorption, in particular because it has a very high specific surface area and nevertheless causes only low pressure losses in the gas phase. On the other hand, the filling 12 is more suitable for special applications in which it is necessary to work under extremely low pressures.
これに関して、液体の上述の横分布は、薄板格
子内および薄板格子間において気体流に関係なし
に行なわれ、したがつてこの横分布は気体流が僅
かしかない場合にも常に最適に保証されることを
指摘しなければならない。 In this regard, the above-mentioned lateral distribution of the liquid takes place within the laminate grid and between the laminate grids independently of the gas flow, so that this lateral distribution is always optimally ensured even with only a small gas flow. I have to point that out.
充填物11,12の製造を第7図ないし第10
図により以下に説明する。充填物11,12の格
子に相当する第7図に示した薄板格子27は、第
8図に示した金属帯28から次のようにして得ら
れる。すなわち薄い帯28が、それぞれ複数の個
所29においてつながつている複数の平行な条片
30に切断され、しかも互いに隣接する条片30
を個所29においてつないでいる切断線部分31
が同じ長さを持ちかつこの長さの半分だけ隣接の
切断線部分31に対してずれているように切断さ
れている。この場合条片幅sは帯28の厚さtよ
り大きく選ばれ、なるべくこの条片幅sが帯厚さ
6の20倍ないし30倍になるように選ばれるのが好
ましい。各切断線部分31の中心において菱形穴
32が隣接する両方の条片30に打ち抜かれる。
この場合菱形穴の両対角線の長さは条片幅sより
大きく選ばれ、しかも切欠き20,21の長さg
および深さhの上記の有利な寸法が格子の引き離
された状態で得られるように選ばれる。その後条
片30が矢印33の方向に引き離され、しかも隣
接する条片30がつながつている個所29におい
て互いになす角度βがなるべく最低45゜および最
高90゜になるまで引き離される。条片30を引き
離した後、ジグザグ状に延びている薄板条片を持
つ薄片格子27が生じ、これらの薄板条片の薄片
は格子面に対して傾斜している。条片30が引き
離される程度に関係する傾斜角αを、続く処理段
階により拡大あるいは縮小することができる。傾
斜角αはなるべく25゜ないし75゜の範囲に選ばれ
るのが好ましい。こうして得られた薄板格子27
はそれから互いに積み重ねられかつ互いに結合さ
れ、例えば簡単に線を介して固定的に結合されあ
るいは互いに溶接される。 The manufacturing of the fillers 11 and 12 is shown in FIGS. 7 to 10.
This will be explained below using figures. The thin plate lattice 27 shown in FIG. 7, which corresponds to the lattice of the fillings 11, 12, is obtained from the metal strip 28 shown in FIG. 8 in the following manner. That is, the thin strip 28 is cut into a plurality of parallel strips 30 which are each connected at a plurality of points 29 and which are adjacent to each other.
A cutting line portion 31 connecting the two at point 29
have the same length and are cut so as to be offset from the adjacent cutting line portion 31 by half of this length. In this case, the strip width s is selected to be greater than the thickness t of the strip 28, preferably such that the strip width s is 20 to 30 times the strip thickness 6. At the center of each cutting line section 31 a diamond-shaped hole 32 is punched into both adjacent strips 30 .
In this case, the length of both diagonals of the diamond-shaped hole is selected to be greater than the strip width s, and the length g of the notches 20, 21 is
and the depth h are chosen such that the above-mentioned advantageous dimensions are obtained in the separated state of the grating. The strips 30 are then pulled apart in the direction of the arrow 33 until the angle .beta. between adjacent strips 30 at the point 29 where they join is preferably at least 45 DEG and at most 90 DEG. After pulling the strips 30 apart, a laminate lattice 27 with zigzag-extending lamella strips results, the lamina of these lamella strips being inclined with respect to the lattice plane. The angle of inclination α, which is related to the extent to which the strips 30 are pulled apart, can be increased or decreased by subsequent processing steps. The angle of inclination α is preferably selected in the range of 25° to 75°. Thin plate lattice 27 thus obtained
are then stacked one on top of the other and connected to one another, for example simply fixedly connected via wires or welded to one another.
第10図に示したように、充填物を円形の塔横
断面に合わせることができ、すなわち薄板条片の
数が少しずつ増加および減少し、したがつて幅が
増加および減少する格子が積み重ねられて、充填
物34の横断面が、段階的に円形の塔横断面35
に合わされた形状になる。充填物34において最
も幅の狭い両格子が36で示され、合計14個の最
も幅の広い格子のうちの1つが37で示されてい
る。重要なことは、薄板条片を1つずつ追加しま
たは省くことによつてのみ格子を塔横断面に段階
的に合わせかつ各格子の一番外側のジグザグ状の
両薄板条片が塔横断面に正確に合わせるためには
中断されないということである。それによつて、
一番外側の両薄板条片上を流下する液体がしたた
り落ちることもなくまた条片の全長に沿つて流下
することもなく、上述したように、交差個所を横
切つて隣接の薄板条片へ、したがつて再び充填物
の内部へ流れ返る。充填物をこのように段階的に
塔横断面に合わせることにより、充填物縁と塔壁
との間に空隙が生ずることは不可避である。塔の
直径が大きい場合はこの空隙を無視することがで
き、さらに例えば充填物に巻かれた切込みのある
織布帯によりふさぐことができ、それによつて好
ましくない塔壁に沿う気体流も回避される。 As shown in FIG. 10, the packing can be adapted to a circular column cross-section, i.e. grids with increasing and decreasing number of thin plate strips and therefore increasing and decreasing width are stacked. The cross section of the packing 34 gradually changes to a circular column cross section 35.
It has a shape that matches. Both of the narrowest gratings in the packing 34 are indicated at 36, and one of the 14 widest gratings in total is indicated at 37. Importantly, the grid can only be fitted stepwise to the tower cross section by adding or omitting one sheet strip at a time, and that both outermost zigzag sheet strips of each grid This means that there is no interruption in order to accurately match the By that,
Liquid flowing down on both outermost lamella strips does not drip or flow down the entire length of the strips, but instead flows across the point of intersection to the adjacent lamella strip, as described above. , and therefore flows back into the filling. Due to this stepwise adaptation of the packing to the column cross-section, it is unavoidable that voids occur between the packing edge and the column wall. If the diameter of the column is large, this void can be ignored and can be further closed, for example by a notched fabric strip wrapped around the packing, thereby also avoiding undesired gas flow along the column wall. Ru.
第9図に概略的に示したように、精留あるいは
吸収用の塔の中へ、薄板格子を塔軸線に対して平
行にして複数の充填物が重なり合つて挿入され
る。互いに隣接する充填物の格子が互いにほぼ直
角に設けられ、すなわち充填物は挿入の際前の充
填物に対してそれぞれ90゜だけ回転せしめられ
る。それによつて、矢印22の方向に塔を貫流す
る液体および矢印22′の方向に流れる気体の非
常に均質な横分布が得られ、充填物の薄板格子に
おける相の横分布と格子面に対して直角方向の相
の横分布との差が相殺される。 As shown schematically in FIG. 9, a plurality of packings are inserted one above the other into a rectification or absorption column with the laminar grid parallel to the column axis. The grids of adjacent fillings are arranged approximately at right angles to each other, ie the fillings are each rotated by 90 DEG relative to the previous filling during insertion. A very homogeneous lateral distribution of the liquid flowing through the column in the direction of the arrow 22 and of the gas flowing in the direction of the arrow 22' is thereby obtained, with respect to the lateral distribution of the phase in the laminar lattice of the packing and the lattice planes. The difference with the lateral distribution of the phase in the orthogonal direction cancels out.
上述したように、薄板格子を充填物11,12
の場合と異なるやり方でも互いに積み重ねること
ができる。例えばすべての格子の薄片を同じ向き
に格子面へ傾斜させることができる。この場合充
填物11の格子と同じく格子を互いにずらすこと
ができ、すなわち偶数の格子の交差個所の中心
が、奇数の格子の網目の中心を通つて延びている
共通な一列線上に位置することができる。この場
合は、充填物11および12の充填密度の間の充
填密度が得られる。しかし格子を他の仕方で互い
にずらすこともでき、例えば格子の交差個所の中
心を互いにずらして、水平切断面が互いに積み重
ねられている格子の平面交差個所を切る切断線が
互いに一直線をなすようにすることもできる。そ
の場合は充填密度が充填物12の充填密度と一致
する。さらに、同じ向きに格子面へ傾斜している
薄板条片を持つ格子を適切にずらすことにより、
充填物11の場合と同じ程度に密な充填物が得ら
れる。この場合は、充填物11の場合のように、
格子面に対して平行な各格子の区画面が隣接する
両方の格子の格子面と合致する。 As mentioned above, the thin plate lattice is filled with fillers 11, 12.
They can also be stacked on top of each other in different ways. For example, all grating lamellas can be tilted in the same direction towards the grating plane. In this case, like the grid of the filling 11, the grids can be offset with respect to each other, ie the centers of the points of intersection of the even grids lie on a common line extending through the centers of the meshes of the odd grids. can. In this case, a packing density between the packing densities of the packings 11 and 12 is obtained. However, the grids can also be offset with respect to each other in other ways, for example by shifting the centers of the intersections of the grids with respect to each other so that the cutting lines cutting through the plane intersections of the grids whose horizontal cut planes are stacked on top of each other are in line with each other. You can also. In that case, the packing density matches that of the filling material 12. Furthermore, by appropriately shifting the lattice with thin plate strips inclined in the same direction to the lattice plane,
A packing as dense as in the case of packing 11 is obtained. In this case, as in the case of the filling 11,
The partition plane of each lattice parallel to the lattice plane matches the lattice planes of both adjacent lattices.
液体を交差個所を介して導くために、薄板条片
を他の仕方で構成することもできる。第11図に
示した変形例では、この目的のために各交差個所
の両側において薄板条片から3角形の耳片38が
折り曲げられている。液体を交差個所を介して導
くために、薄板条片はさらに交差個所に隆起ある
いは凹所、例えば波形溝あるいは細溝を持つこと
ができ、これらの溝は液体流の所望の推移に応じ
て一方の薄板条片の1つの薄片から交差個所を経
て隣接の薄板条片の次の薄片へ延びている。さら
に薄板条片の外縁は、他の仕方で形成された、例
えば半円形の切欠きを持つこともできる。 The sheet metal strips can also be configured in other ways in order to direct the liquid through the intersection points. In the variant shown in FIG. 11, triangular ears 38 are bent out of the sheet metal strips on both sides of each crossing point for this purpose. In order to direct the liquid through the intersection point, the sheet metal strips can additionally have ridges or depressions at the intersection point, for example corrugated grooves or slots, which grooves can be moved from one side to the other depending on the desired course of the liquid flow. It extends from one lamination of the sheet metal strips through the intersection point to the next lamination of the adjacent sheet metal strip. Furthermore, the outer edge of the sheet metal strip can also have a recess formed in another way, for example semicircular.
気相の圧力損失をさらに減少させかつ液相にお
ける乱流を増大させるために、薄片はさらに、第
12図および第13図に示したように、穴39あ
るいは側方切欠き39′を持つこともできる。 In order to further reduce pressure losses in the gas phase and increase turbulence in the liquid phase, the flakes may additionally have holes 39 or lateral notches 39', as shown in FIGS. 12 and 13. You can also do it.
上述したように、液体の横分布は一方では薄板
格子内で行なわれ、他方では充填物の薄板格子間
で行なわれる。しかし液体分布の程度はこれまで
述べた充填物においては同じでない。すなわち液
体は個々の格子間におけるより個々の格子内にお
ける方が一層良好に分布する。格子ごとの液体の
最適な横分布を行なうために、隣接する格子の薄
片が切欠かれた縁部において互いに係合するよう
に充填物を構成することができる。第14図は、
このような充填物用に定められ切欠かれた縁部4
0を持つ薄板格子を示し、第15図はこのような
充填物41の一部の横断面を示す。この充填物4
1の薄板格子は充填物11の薄板格子と同じよう
に設けられており、互いに隣接する格子の薄片は
逆向きに格子面へ傾斜しかつ偶数の格子の交差個
所の中心は、奇数の格子の網目の中心を通つて延
びている一列線上に位置している。充填物41の
場合は液体が一方の格子の薄片の縁から隣接の格
子の薄片に向かつて流れ、その際格子ごとの良好
な横分布のほかに高い程度の乱流が生ずることも
明らかである。その上に、充填物41は非常に高
い充填密度の利点を有する。勿論充填物41の場
合にも、液相が交差個所を横切つて流れるように
交差個所を構成することができ、そのためになる
べく薄板条片の外縁が切欠き20,21を持つの
が好ましい。これらの切欠きは、単に図面を簡単
化するために、第14図および第15図には省略
されている。 As mentioned above, the lateral distribution of the liquid takes place on the one hand within the laminar grid and on the other hand between the laminar grids of the filling. However, the degree of liquid distribution is not the same in the packings described so far. That is, the liquid is distributed better within the individual lattices than between the individual lattices. In order to achieve an optimal lateral distribution of liquid per grid, the filling can be configured such that the lamina of adjacent grids engage each other at the cut-out edges. Figure 14 shows
A notched edge 4 defined for such a filling
15 shows a cross-section of part of such a filling 41. FIG. This filling 4
The thin plate gratings of 1 are arranged in the same way as the thin plate gratings of the filling 11, the laminae of adjacent gratings being inclined in opposite directions towards the grating plane, and the centers of the intersections of the even numbered gratings are located at the intersections of the even numbered gratings. It is located on a line extending through the center of the mesh. In the case of packing 41, it is clear that the liquid flows from the edges of the lamellas of one lattice towards the lamellas of the adjacent lattice, and that, in addition to a good lateral distribution from one lattice to another, a high degree of turbulence also occurs. . Moreover, the packing 41 has the advantage of a very high packing density. Of course, also in the case of the filling 41, the crossing point can be constructed in such a way that the liquid phase flows across the crossing point, and for this purpose preferably the outer edges of the sheet metal strips have recesses 20, 21. These cutouts have been omitted from FIGS. 14 and 15 simply to simplify the drawing.
第16図に示した薄板格子42においては、ジ
グザグ状に順次に続く各薄板条片の薄片が交互に
穴対43を持つており、この場合穴対の代りにあ
るいは穴対に加えて第13図による側方切欠き3
9′を持つこともできる。それにより気体流は転
向に加えて薄片により流れ方向44に対して直角
に導かれ、この交互の穴43により、流れ方向4
4に対して傾斜して上方へ延びる通路が矢印45
の方向において気体流に開かれている。 In the sheet metal grid 42 shown in FIG. 16, the laminae of each successive sheet metal strip in a zigzag pattern have alternating pairs of holes 43, in which case instead of or in addition to the pairs of holes 13 Lateral cutout 3 according to the diagram
It can also have 9'. The gas flow is thereby, in addition to being diverted, guided by the lamina at right angles to the flow direction 44 and, by means of the alternating holes 43, in the flow direction 44.
A passageway extending upward at an angle with respect to 4 is indicated by an arrow 45.
open to gas flow in the direction of
さらに、薄板条片は条片の縦方向に対して直角
に延びる隆起あるいは凹所を持つことができる。
それについての一例として第17図は、条片の縦
方向に対して直角に延びている波形溝46を持ち
波形板から製造された薄板格子の2つの網目を示
している。このような薄板格子から成る充填物
は、ぬるさないまたは完全にはぬらさない液体に
特に有利であり、この液体においては横波形溝が
滴形成あるいは細流形成を防止しかつ薄片面上の
均一な分布を保証する。さらに波形溝46によ
り、液相において交差個所間にも乱流を発生させ
ることができる。 Furthermore, the sheet metal strips can have ridges or depressions extending at right angles to the longitudinal direction of the strip.
As an example thereof, FIG. 17 shows two meshes of a sheet metal grid made of corrugated plate with corrugated grooves 46 extending at right angles to the longitudinal direction of the strip. Packings consisting of such laminar grids are particularly advantageous for liquids that are not wet or completely wet, in which the transverse corrugated grooves prevent droplet or trickle formation and provide a uniform distribution on the lamina surface. Guaranteed distribution. Furthermore, the wave-shaped grooves 46 can also generate turbulence in the liquid phase between crossing points.
これまで述べた薄板格子はすべて薄い金属板か
らできている。しかし薄板格子をプラスチツク箔
あるいは織布帯から製造することもできる。 All the thin plate gratings mentioned so far are made from thin metal plates. However, the sheet metal grid can also be produced from plastic foil or a woven fabric strip.
第1図は、公知の薄板格子の立体的構成におけ
る格子網目の拡大斜視図、第2図は、互いに積み
重ねられた薄板格子から成る充填物の一部の側面
図、第3図は、第2図の―線に沿う第2図の
充填物部分の横断面図、第4図は、第2図および
第3図の充填物と同じであるが、しかし積み重ね
方が異なる薄板格子から構成された別の充填物の
一部の側面図、第5図は第4図の―線に沿う
第4図の充填物部分の横断面図、第6図は、液体
の流れ方向を示す矢印を記入した第2図ないし第
5図の薄板格子のうちの1つの薄板格子の交差個
所を拡大して示す図、第7図および第8図は、第
2図ないし第5図の充填物の薄板格子の一部の縮
小図およびこの薄板格子の製造のために用意され
た帯を示す図、第9図は、互いに重ねて塔の中に
挿入された複数の充填物の概略の軸線方向断面
図、第10図は、第9図の充填物のうちの1つの
充填物の拡大平面図、第11図は第6図の交差個
所の変形例を示す図、第12図は、第2図ないし
第5図の薄板格子の変形例の2つの網目を示す
図、第13図は、第2図ないし第5図の薄板格子
の別の変形例の2つの網目を示す図、第14図
は、互いに係合する薄板格子を有する充填物用の
側方切欠きを持つ薄板格子を示す図、第15図
は、互いに係合する薄板格子を有する充填物の一
部の拡大横断面図、第16図は、薄板条片が交互
に穴を持つ薄板格子を示す図、第17図は、第2
図ないし第5図の薄板格子の変形例の2つの網目
を示す図である。
13ないし17…薄板条片、18…交差個所、
20,21…切欠き、23…液相、a,b,c,
…薄板格子、A,B,C,…格子面。
FIG. 1 is an enlarged perspective view of a lattice network in a three-dimensional configuration of a known thin plate lattice; FIG. 2 is a side view of a portion of a packing consisting of stacked thin plate lattices; A cross-sectional view of the portion of the infill of FIG. 2 along the line of FIG. A side view of a part of another filling, FIG. 5 is a cross-sectional view of the filling part of FIG. 4 along the line - in FIG. 4, and FIG. FIGS. 7 and 8 are enlarged views showing the intersection points of one of the thin plate lattices of FIGS. 2 to 5, and FIGS. FIG. 9 is a schematic axial section of a plurality of packings inserted into the column one on top of the other, FIG. 10 is an enlarged plan view of one of the packings shown in FIG. 9, FIG. 11 is a view showing a modification of the intersection of FIG. 6, and FIG. 12 is a plan view of one of the packings shown in FIG. FIG. 13 is a diagram showing two meshes of a modification of the thin plate lattice in FIGS. 2 to 5; FIG. 14 is a diagram showing two meshes of another modification of the thin plate lattice of FIGS. FIG. 15 is an enlarged cross-sectional view of a part of the packing with interlocking sheet metal grids; FIG. , a diagram showing a thin plate grid in which the thin plate strips have holes alternately, FIG.
FIG. 6 shows two meshes of a modification of the thin plate lattice of FIGS. 13 to 17...Thin plate strip, 18...Intersecting point,
20, 21... Notch, 23... Liquid phase, a, b, c,
...thin plate lattice, A, B, C, ... lattice plane.
Claims (1)
れ、各格子a,b,c,…がほぼジグザグ状に曲
げられて格子面A,B,C,…に対して傾斜する
薄板条片13〜17から成り、これらの薄板条片
が曲げ個所18で一体につながつてそこに格子の
面状交差個所を形成している、物質交換塔用充填
物において、流れ方向に延びる薄板条片13〜1
7が、交差個所18に流れ案内部20,21;3
8を持ち、この流れ案内部により、薄板条片17
上を流下する液相22,23の流れ方向が変化し
て、液相22,23の一部が交差個所18を経て
隣接する薄板条片16へ偏向されることを特徴と
する、物質交換塔用充填物。 2 複数の薄板格子a,b,c,…から構成さ
れ、各格子a,b,c,…がほぼジグザグ状に曲
げられて格子面A,B,C,…に対して傾斜する
薄板条片13〜17から成り、これらの薄板条片
が曲げ個所18で一体につながつてそこに格子の
面状交差個所を形成している物質交換塔用充填物
において、流れ方向に延びる薄板条片13〜17
が、交差個所18に、各交差個所18の両側にお
いて薄板条片外側範囲に設けられる切欠き20,
21の縁または各交差個所18の両側において薄
板条片13〜17に設けられる隆起あるいは凹所
により形成される流れ案内部20,21,38を
持ち、薄板条片17上を流下する液相22,23
の流れ方向が変化して、液相22,23の一部が
交差個所18を経て隣接する薄板条片16へ偏向
されるように、切欠き20,21の縁または隆起
あるいは凹所が延びていることを特徴とする、物
質交換塔用充填物。 3 切欠き20,21が、薄板条片13〜17が
ジグザグ状に延びている方向において、薄板条片
の幅sより長くかつ薄板条片に対して直角方向に
おいてこの幅sの半分より深いことを特徴とす
る、特許請求の範囲第2項に記載の充填物。 4 薄板条片13〜17が交差個所18間に穴3
9,43およびあるいは側方切欠き39′を持つ
ていることを特徴とする、特許請求の範囲第2項
あるいは第3項に記載の充填物。 5 ジグザグ状に順次に続く各薄板条片13〜1
7の薄片が穴43および(あるいは)側方切欠き
を交互に備えていることを特徴とする、特許請求
の範囲第4項に記載の充填物。 6 すべての薄板格子a,b,c,…が直接互い
に積み重ねられていることを特徴とする、特許請
求の範囲第2項ないし第5項のうち1つに記載の
充填物。 7 第1、第3、第5等々の格子a,b,c,…
の薄板条片が同じ向きに格子面A,B,C,…へ
傾斜し、第2、第4、第6等々の格子b,d,
f,…の薄板条片が逆向きに格子面A,B,C,
…へ傾斜していることを特徴とする、特許請求の
範囲第6項に記載の充填物。 8 薄板格子a,b,c,…が、各格子の薄板条
片が両方の隣接する格子の網目へ突出するように
互いにずらして積み重ねられていることを特徴と
する、特許請求の範囲第6項あるいは第7項に記
載の充填物。 9 隣接する格子の薄板条片が、切欠かれた縁部
40において互いに係合していることを特徴とす
る、特許請求の範囲第8項に記載の充填物。 10 第1、第3、第5等々の格子a,c,e,
…の交差個所の中心が、格子面A,B,C,…に
対して垂直な共通の一列線上に位置し、第2、第
4、第6等々の格子b,d,f,…の交差個所の
中心が、第1、第3、第5等々の格子a,c,
e,…の網目の中心を通つて延びかつ格子面A,
B,C,…に対して垂直な共通の一列線上に位置
していることを特徴とする、特許請求の範囲第8
項あるいは第9項に記載の充填物。 11 異なる数の薄板条片を持つ格子36,37
が互いに積み重ねられて、充填物横断面34が段
階的に円形の塔横断面35に合わせられた形状を
持ち、各格子の一番外側のジグザグ状の両薄板条
片が中断されていないことを特徴とする、特許請
求の範囲第6項ないし第10項のうち1つに記載
の充填物。 12 薄板条片が、条片の縦方向に対して直角に
延びている隆起あるいは凹所を持ち、例えば波形
溝46を付けられていることを特徴とする、特許
請求の範囲第2項ないし第11項のうち1つに記
載の充填物。 13 薄板条片13〜17の幅sがこの薄板条片
の厚さtの20倍ないし30倍であることを特徴とす
る、特許請求の範囲第2項ないし第12項のうち
1つに記載の充填物。 14 流れ方向に延びる薄板条片13〜17が、
交差個所18に流れ案内部20,21;38を持
ち、この流れ案内部により、薄板条片17上を流
下する液相22,23の流れ方向が変化して、液
相22,23の一部が交差個所18を経て隣接す
る薄板条片16へ偏向される薄板格子を製造する
ために、帯28がそれぞれ複数の個所29でつな
がつている平行な条片30に切断されて、互いに
隣接する条片30をつないでいる切断線部分31
が同じ長さを持ち、かつこの長さの半分だけ隣接
の切断線部分31に対してずらされ、その後条片
30が引き離される33ようにする、物質交換塔
用充填物の製造方法において、各切断線部分31
の中央において穴32が両方の互いに隣接する条
片30に打ち抜かれあるいは穿孔され、条片30
がその後にはじめて引き離されることを特徴とす
る、充填物の製造方法。[Scope of Claims] 1. Consisting of a plurality of thin plate gratings a, b, c, ..., each grating a, b, c, ... is bent in a substantially zigzag shape so that the grid faces A, B, C, ... In a packing for a mass exchange column, consisting of thin plate strips 13 to 17 which are inclined in the direction of flow and which are joined together at bending points 18 and form there the planar intersections of the grid, thin plate strips 13-1 extending to
7 has a flow guide section 20, 21; 3 at the intersection point 18.
8, and by means of this flow guide, the thin plate strip 17
Mass exchange column, characterized in that the flow direction of the liquid phases 22, 23 flowing down above is changed such that a part of the liquid phases 22, 23 is deflected via the intersection point 18 into the adjacent sheet metal strip 16 Filling for. 2. A thin plate strip consisting of a plurality of thin plate gratings a, b, c, ..., each of which is bent in a substantially zigzag shape and inclined with respect to the grating planes A, B, C, ... A mass exchange column packing consisting of thin plate strips 13 to 17 which are joined together at bending points 18 and form there the planar intersections of the grid, in which the thin plate strips 13 to 17 extend in the flow direction. 17
but at the crossing point 18, a cutout 20, which is provided in the outer region of the sheet metal strip on both sides of each crossing point 18,
The liquid phase 22 flowing down over the sheet metal strips 17 has flow guides 20, 21, 38 formed by ridges or depressions provided in the sheet metal strips 13-17 on both sides of the edges of 21 or at each crossing point 18. ,23
The edges or ridges or recesses of the notches 20, 21 are extended such that the direction of flow of the liquid phases 22, 23 is deflected through the intersection point 18 into the adjacent sheet strip 16. A packing for a mass exchange column, characterized in that: 3. The notches 20, 21 are longer than the width s of the thin plate strips in the direction in which the thin plate strips 13 to 17 extend in a zigzag manner and are deeper than half of this width s in the direction perpendicular to the thin plate strips. The filling according to claim 2, characterized by: 4 Hole 3 between the intersection points 18 of the thin plate strips 13 to 17
Packing according to claim 2 or 3, characterized in that it has 9, 43 and/or lateral cutouts 39'. 5 Each thin plate strip 13 to 1 successively following a zigzag pattern
Packing according to claim 4, characterized in that the 7 laminae are provided alternately with holes 43 and/or lateral notches. 6. Packing according to one of claims 2 to 5, characterized in that all the laminar grids a, b, c,... are stacked directly on top of each other. 7 First, third, fifth, etc. grids a, b, c,...
are inclined in the same direction to the grating planes A, B, C, ..., and the second, fourth, sixth, etc. grating planes b, d, etc.
The thin plate strips of f,... are arranged in opposite directions on the lattice planes A, B, C,
The filling according to claim 6, characterized in that it is inclined towards... 8. Claim 6, characterized in that the sheet metal gratings a, b, c, ... are stacked offset from one another in such a way that the sheet metal strips of each grating protrude into the meshes of both adjacent gratings. The filling according to item 1 or item 7. 9. Packing according to claim 8, characterized in that the sheet metal strips of adjacent grids engage one another at the cutout edges 40. 10 first, third, fifth etc. grids a, c, e,
The center of the intersection of ... is located on a common line perpendicular to the lattice planes A, B, C, ..., and the intersections of the second, fourth, sixth, etc. lattices b, d, f, ... The centers of the points are the first, third, fifth, etc. grids a, c,
extending through the center of the mesh of e,... and lattice plane A,
Claim 8, characterized in that it is located on a common line perpendicular to B, C,...
The filling according to item 9 or item 9. 11 Grids 36, 37 with different numbers of thin plate strips
are stacked on top of each other so that the packing cross-section 34 has a shape adapted to the circular tower cross-section 35 in stages and that the two outermost zigzag-shaped sheet metal strips of each grid are uninterrupted. Filler according to one of claims 6 to 10, characterized in that: 12. Claims 2 to 12, characterized in that the sheet metal strip is provided with ridges or depressions extending at right angles to the longitudinal direction of the strip, for example with corrugated grooves 46. Filling according to one of clauses 11. 13. According to one of the claims 2 to 12, characterized in that the width s of the sheet metal strips 13 to 17 is between 20 and 30 times the thickness t of this sheet metal strip. filling. 14 The thin plate strips 13 to 17 extending in the flow direction are
At the point of intersection 18 there are flow guides 20, 21; 38, which change the flow direction of the liquid phases 22, 23 flowing down on the thin plate strip 17, so that part of the liquid phases 22, 23 In order to produce a sheet metal grating in which the beams are deflected via crossing points 18 onto adjacent sheet metal strips 16, the strip 28 is cut into parallel strips 30, each of which is connected at a plurality of points 29, so that the adjacent strips 16 Cutting line portion 31 connecting pieces 30
have the same length and are offset relative to the adjacent cutting line section 31 by half this length, after which the strips 30 are pulled apart 33. Cutting line portion 31
A hole 32 is punched or drilled in both adjacent strips 30 in the center of the strip 30.
A method for producing a filling, characterized in that the filling is only then separated.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH4480/81-6 | 1981-07-08 | ||
| CH448081 | 1981-07-08 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5811001A JPS5811001A (en) | 1983-01-21 |
| JPS6234401B2 true JPS6234401B2 (en) | 1987-07-27 |
Family
ID=4276879
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP57111846A Granted JPS5811001A (en) | 1981-07-08 | 1982-06-30 | Filler for mass exchange tower and production thereof |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US4501707A (en) |
| EP (1) | EP0069241B1 (en) |
| JP (1) | JPS5811001A (en) |
| DE (1) | DE3266166D1 (en) |
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| EP2380660B1 (en) | 2010-04-20 | 2018-01-24 | Sulzer Chemtech AG | Mass transfer column and a crown element for a mass transfer column |
| WO2013015415A1 (en) | 2011-07-28 | 2013-01-31 | 株式会社Ihi | Gas separation device, and filler |
| JPWO2014017111A1 (en) * | 2012-07-27 | 2016-07-07 | 株式会社Ihi | Gas separator and filler |
| US20150048528A1 (en) * | 2013-08-19 | 2015-02-19 | Sean Anderson Barton | Fill material for direct-contact heat/mass exchangers |
| JP6460629B2 (en) | 2014-01-27 | 2019-01-30 | 三菱重工エンジニアリング株式会社 | Gas-liquid contact device and CO2 recovery device |
| EP3808446A1 (en) | 2019-10-14 | 2021-04-21 | Sulzer Management AG | Structured cross-channel packing element with reduced material requirement |
| EP3808445A1 (en) | 2019-10-14 | 2021-04-21 | Sulzer Management AG | Structured packing element with reduced material requirement |
| WO2024220045A1 (en) * | 2023-04-19 | 2024-10-24 | Aspen Yapi Ve Zemi̇n Si̇stemleri̇ Sanayi̇ Ve Ti̇caret Anoni̇m Şi̇rketi̇ | Perforated expanded metal |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE532764C (en) * | 1927-08-12 | 1932-04-07 | Hugo Kosmack | Filler |
| DE551071C (en) * | 1930-08-14 | 1932-05-26 | Rudolf Timm Dipl Ing | Filling body or reaction body made of metal |
| US2003271A (en) * | 1932-09-19 | 1935-05-28 | Beimann Wilhelm | Hurdle washer |
| US2018085A (en) * | 1934-05-29 | 1935-10-22 | Allegheny Steel Co | Method of making flat expanded grilles |
| US2405593A (en) * | 1944-02-04 | 1946-08-13 | Francis L Melvill | Packing for vapor and liquid contacting apparatus |
| GB734874A (en) * | 1953-11-17 | 1955-08-10 | Atomic Energy Authority Uk | Improvements in or relating to packings for vapour-liquid and gas-liquid contacting systems |
| US3346246A (en) * | 1965-01-25 | 1967-10-10 | Marley Co | Cooling tower fill assembly of foraminous sheet material |
| GB1263479A (en) | 1969-02-05 | 1972-02-09 | Albright & Wilson | Distillation apparatus |
| US3570086A (en) * | 1969-04-21 | 1971-03-16 | Metalex Corp | Methods and machines for manufacture of expanded metal |
| GB1285495A (en) * | 1970-11-03 | 1972-08-16 | Bischoff Gasreinigung | Packing for incorporation in a cooling tower of a cooling water circulation system |
| JPS4719441U (en) * | 1971-02-17 | 1972-11-04 | ||
| US3878594A (en) * | 1973-01-12 | 1975-04-22 | Carrier Corp | Process for manufacturing humidifier filter media |
| JPS5540704Y2 (en) * | 1973-06-05 | 1980-09-22 | ||
| GB1470196A (en) * | 1974-11-13 | 1977-04-14 | Cooling Dev Ltd | Contact packing |
| CH618006A5 (en) * | 1977-05-12 | 1980-06-30 | Sulzer Ag | |
| US4304738A (en) * | 1979-10-15 | 1981-12-08 | Nutter Dale E | Packing Material and apparatus |
| US4338266A (en) * | 1981-04-08 | 1982-07-06 | Research Products Corporation | Device for conditioning air with improved gas-liquid contact pad |
-
1982
- 1982-06-11 DE DE8282105106T patent/DE3266166D1/en not_active Expired
- 1982-06-11 EP EP82105106A patent/EP0069241B1/en not_active Expired
- 1982-06-30 JP JP57111846A patent/JPS5811001A/en active Granted
- 1982-07-07 US US06/395,996 patent/US4501707A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5811001A (en) | 1983-01-21 |
| DE3266166D1 (en) | 1985-10-17 |
| EP0069241B1 (en) | 1985-09-11 |
| EP0069241A1 (en) | 1983-01-12 |
| US4501707A (en) | 1985-02-26 |
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