JPS6351964B2 - - Google Patents

Info

Publication number: JPS6351964B2
Authority: JP; Japan
Prior art keywords: phosphoric acid; weight; amount; acetone; compound
Prior art date: 1979-01-25
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP55006735A

Other languages

English (en)

Japanese (ja)

Other versions

JPS55104909A (en

Inventor

Antoniasu Maria Ueteringusu Koonerisu

Anna Yansen Yohanesu

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Stamicarbon BV

Original Assignee

Stamicarbon BV

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1979-01-25

Filing date

1980-01-23

Publication date

1988-10-17

1980-01-23 Application filed by Stamicarbon BV filed Critical Stamicarbon BV

1980-08-11 Publication of JPS55104909A publication Critical patent/JPS55104909A/ja

1988-10-17 Publication of JPS6351964B2 publication Critical patent/JPS6351964B2/ja

Status Granted legal-status Critical Current

Links

NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 141
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 71
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 46
238000000034 method Methods 0.000 claims description 45
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims description 30
229910052770 Uranium Inorganic materials 0.000 claims description 29
JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 claims description 29
239000002244 precipitate Substances 0.000 claims description 26
150000001875 compounds Chemical class 0.000 claims description 16
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 15
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 15
239000002270 dispersing agent Substances 0.000 claims description 14
150000002222 fluorine compounds Chemical class 0.000 claims description 13
DDFHBQSCUXNBSA-UHFFFAOYSA-N 5-(5-carboxythiophen-2-yl)thiophene-2-carboxylic acid Chemical compound S1C(C(=O)O)=CC=C1C1=CC=C(C(O)=O)S1 DDFHBQSCUXNBSA-UHFFFAOYSA-N 0.000 claims description 11
238000001556 precipitation Methods 0.000 claims description 10
239000003638 chemical reducing agent Substances 0.000 claims description 8
239000003795 chemical substances by application Substances 0.000 claims description 8
230000001376 precipitating effect Effects 0.000 claims description 8
239000011737 fluorine Substances 0.000 claims description 6
229910052731 fluorine Inorganic materials 0.000 claims description 6
229910021529 ammonia Inorganic materials 0.000 claims description 5
150000003863 ammonium salts Chemical class 0.000 claims description 5
OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 5
AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 claims description 4
150000001553 barium compounds Chemical class 0.000 claims description 4
TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 4
229940043430 calcium compound Drugs 0.000 claims description 4
150000001674 calcium compounds Chemical class 0.000 claims description 4
239000012141 concentrate Substances 0.000 claims description 4
229910000069 nitrogen hydride Inorganic materials 0.000 claims description 2
PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims 3
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims 2
CJDPJFRMHVXWPT-UHFFFAOYSA-N barium sulfide Chemical compound [S-2].[Ba+2] CJDPJFRMHVXWPT-UHFFFAOYSA-N 0.000 claims 1
229910000019 calcium carbonate Inorganic materials 0.000 claims 1
JGIATAMCQXIDNZ-UHFFFAOYSA-N calcium sulfide Chemical compound [Ca]=S JGIATAMCQXIDNZ-UHFFFAOYSA-N 0.000 claims 1
235000011007 phosphoric acid Nutrition 0.000 description 59
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 31
239000000203 mixture Substances 0.000 description 18
229910052742 iron Inorganic materials 0.000 description 15
150000002576 ketones Chemical class 0.000 description 13
150000002500 ions Chemical class 0.000 description 7
239000007788 liquid Substances 0.000 description 7
239000007787 solid Substances 0.000 description 7
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
229910019142 PO4 Inorganic materials 0.000 description 6
238000004821 distillation Methods 0.000 description 6
229910052751 metal Inorganic materials 0.000 description 6
239000002184 metal Substances 0.000 description 6
235000021317 phosphate Nutrition 0.000 description 6
239000000243 solution Substances 0.000 description 6
ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 5
239000001099 ammonium carbonate Substances 0.000 description 5
239000012535 impurity Substances 0.000 description 5
239000010452 phosphate Substances 0.000 description 5
229910000013 Ammonium bicarbonate Inorganic materials 0.000 description 4
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 4
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
235000012538 ammonium bicarbonate Nutrition 0.000 description 4
239000011575 calcium Substances 0.000 description 4
239000000706 filtrate Substances 0.000 description 4
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 4
150000003016 phosphoric acids Chemical class 0.000 description 4
239000002904 solvent Substances 0.000 description 4
238000003756 stirring Methods 0.000 description 4
239000004254 Ammonium phosphate Substances 0.000 description 3
YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 3
239000002253 acid Substances 0.000 description 3
229910000148 ammonium phosphate Inorganic materials 0.000 description 3
235000019289 ammonium phosphates Nutrition 0.000 description 3
229910052791 calcium Inorganic materials 0.000 description 3
230000000052 comparative effect Effects 0.000 description 3
238000010411 cooking Methods 0.000 description 3
MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 3
238000001914 filtration Methods 0.000 description 3
150000002739 metals Chemical class 0.000 description 3
150000003013 phosphoric acid derivatives Chemical class 0.000 description 3
PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
150000004649 carbonic acid derivatives Chemical class 0.000 description 2
238000005119 centrifugation Methods 0.000 description 2
238000010908 decantation Methods 0.000 description 2
239000003337 fertilizer Substances 0.000 description 2
229910052749 magnesium Inorganic materials 0.000 description 2
239000011777 magnesium Substances 0.000 description 2
239000003960 organic solvent Substances 0.000 description 2
NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 description 2
238000011084 recovery Methods 0.000 description 2
150000003568 thioethers Chemical class 0.000 description 2
238000012546 transfer Methods 0.000 description 2
229910052684 Cerium Inorganic materials 0.000 description 1
KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 1
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
229910001515 alkali metal fluoride Inorganic materials 0.000 description 1
229910001618 alkaline earth metal fluoride Inorganic materials 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
235000012501 ammonium carbonate Nutrition 0.000 description 1
LDDQLRUQCUTJBB-UHFFFAOYSA-N ammonium fluoride Chemical compound [NH4+].[F-] LDDQLRUQCUTJBB-UHFFFAOYSA-N 0.000 description 1
150000001450 anions Chemical class 0.000 description 1
LDDQLRUQCUTJBB-UHFFFAOYSA-O azanium;hydrofluoride Chemical compound [NH4+].F LDDQLRUQCUTJBB-UHFFFAOYSA-O 0.000 description 1
229910052788 barium Inorganic materials 0.000 description 1
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 description 1
150000003841 chloride salts Chemical class 0.000 description 1
229910017052 cobalt Inorganic materials 0.000 description 1
239000010941 cobalt Substances 0.000 description 1
GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
229910001610 cryolite Inorganic materials 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000005265 energy consumption Methods 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
238000000605 extraction Methods 0.000 description 1
229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
229910052746 lanthanum Inorganic materials 0.000 description 1
FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 description 1
238000005259 measurement Methods 0.000 description 1
150000002823 nitrates Chemical class 0.000 description 1
235000003270 potassium fluoride Nutrition 0.000 description 1
239000011698 potassium fluoride Substances 0.000 description 1
239000000843 powder Substances 0.000 description 1
238000012545 processing Methods 0.000 description 1
239000000047 product Substances 0.000 description 1
239000002994 raw material Substances 0.000 description 1
235000019685 rice crackers Nutrition 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
-1 silicates Chemical class 0.000 description 1
150000004760 silicates Chemical class 0.000 description 1
239000007858 starting material Substances 0.000 description 1
229910052712 strontium Inorganic materials 0.000 description 1
CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
239000011593 sulfur Substances 0.000 description 1
229910052717 sulfur Inorganic materials 0.000 description 1
229910021653 sulphate ion Inorganic materials 0.000 description 1
150000003671 uranium compounds Chemical class 0.000 description 1
229910052720 vanadium Inorganic materials 0.000 description 1
GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
229910052727 yttrium Inorganic materials 0.000 description 1
VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 1
229910052725 zinc Inorganic materials 0.000 description 1
239000011701 zinc Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/46—Preparation involving solvent-solvent extraction
- C01B25/461—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound
- C01B25/463—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound the extracting agent being a ketone or a mixture of ketones
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0252—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries
- C22B60/026—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries liquid-liquid extraction with or without dissolution in organic solvents
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0252—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries
- C22B60/0278—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries by chemical methods
- C22B60/0282—Solutions containing P ions, e.g. treatment of solutions resulting from the leaching of phosphate ores or recovery of uranium from wet-process phosphoric acid

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
General Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Organic Chemistry (AREA)
Environmental & Geological Engineering (AREA)
Materials Engineering (AREA)
Metallurgy (AREA)
Chemical Kinetics & Catalysis (AREA)
Geology (AREA)
Mechanical Engineering (AREA)
Manufacturing & Machinery (AREA)
Inorganic Chemistry (AREA)
Analytical Chemistry (AREA)
General Chemical & Material Sciences (AREA)
Inorganic Compounds Of Heavy Metals (AREA)
Manufacture And Refinement Of Metals (AREA)
Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

JP673580A 1979-01-25 1980-01-23 Method of regenerating uraniummcontained concentrate and purified phosphoric acid Granted JPS55104909A (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
NL7900579A NL7900579A (nl)	1979-01-25	1979-01-25	Werkwijze voor het winnen van een uraniumbevattend concentraat en gezuiverd fosforzuur.

Publications (2)

Publication Number	Publication Date
JPS55104909A JPS55104909A (en)	1980-08-11
JPS6351964B2 true JPS6351964B2 (fr)	1988-10-17

Family

ID=19832515

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP673580A Granted JPS55104909A (en)	1979-01-25	1980-01-23	Method of regenerating uraniummcontained concentrate and purified phosphoric acid

Country Status (5)

Country	Link
JP (1)	JPS55104909A (fr)
MA (1)	MA18712A1 (fr)
NL (1)	NL7900579A (fr)
SU (1)	SU955851A3 (fr)
ZA (1)	ZA80333B (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
AU2009347055B2 (en) *	2009-05-27	2014-12-11	Easymining Sweden Ab	Production of ammonium phosphates

1979
- 1979-01-25 NL NL7900579A patent/NL7900579A/nl not_active Application Discontinuation
1980
- 1980-01-21 ZA ZA00800333A patent/ZA80333B/xx unknown
- 1980-01-23 JP JP673580A patent/JPS55104909A/ja active Granted
- 1980-01-24 SU SU802872551A patent/SU955851A3/ru active
- 1980-01-24 MA MA18909A patent/MA18712A1/fr unknown

Also Published As

Publication number	Publication date
SU955851A3 (ru)	1982-08-30
MA18712A1 (fr)	1980-10-01
JPS55104909A (en)	1980-08-11
ZA80333B (en)	1981-01-28
NL7900579A (nl)	1980-07-29

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