JPS6360017B2 - - Google Patents

Info

Publication number: JPS6360017B2
Authority: JP; Japan
Prior art keywords: sulfuric acid; reaction; acid; nitroaniline; chloro
Prior art date: 1983-06-01
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP9573883A

Other languages

English (en)

Japanese (ja)

Other versions

JPS59222451A (ja

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-06-01

Filing date

1983-06-01

Publication date

1988-11-22

1983-06-01 Application filed filed Critical

1983-06-01 Priority to JP9573883A priority Critical patent/JPS59222451A/ja

1984-12-14 Publication of JPS59222451A publication Critical patent/JPS59222451A/ja

1988-11-22 Publication of JPS6360017B2 publication Critical patent/JPS6360017B2/ja

Status Granted legal-status Critical Current

Links

QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 62
AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 claims description 26
QSNSCYSYFYORTR-UHFFFAOYSA-N 4-chloroaniline Chemical class NC1=CC=C(Cl)C=C1 QSNSCYSYFYORTR-UHFFFAOYSA-N 0.000 claims description 13
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
HIFJUMGIHIZEPX-UHFFFAOYSA-N sulfuric acid;sulfur trioxide Chemical compound O=S(=O)=O.OS(O)(=O)=O HIFJUMGIHIZEPX-UHFFFAOYSA-N 0.000 claims description 9
238000000034 method Methods 0.000 claims description 5
239000012429 reaction media Substances 0.000 claims description 5
238000004519 manufacturing process Methods 0.000 claims description 4
230000000802 nitrating effect Effects 0.000 claims description 3
238000006243 chemical reaction Methods 0.000 description 23
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 11
229910017604 nitric acid Inorganic materials 0.000 description 11
238000006396 nitration reaction Methods 0.000 description 9
239000002253 acid Substances 0.000 description 7
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
AKCRQHGQIJBRMN-UHFFFAOYSA-N 2-chloroaniline Chemical compound NC1=CC=CC=C1Cl AKCRQHGQIJBRMN-UHFFFAOYSA-N 0.000 description 5
KWIXNFOTNVKIGM-UHFFFAOYSA-N 2-chloro-5-nitroaniline Chemical compound NC1=CC([N+]([O-])=O)=CC=C1Cl KWIXNFOTNVKIGM-UHFFFAOYSA-N 0.000 description 4
FOHHWGVAOVDVLP-UHFFFAOYSA-N 4-chloro-3-nitroaniline Chemical compound NC1=CC=C(Cl)C([N+]([O-])=O)=C1 FOHHWGVAOVDVLP-UHFFFAOYSA-N 0.000 description 4
PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 4
KPFGGEHCIZEMTD-UHFFFAOYSA-N n-chloro-4-nitroaniline Chemical class [O-][N+](=O)C1=CC=C(NCl)C=C1 KPFGGEHCIZEMTD-UHFFFAOYSA-N 0.000 description 4
238000003756 stirring Methods 0.000 description 4
PBGKNXWGYQPUJK-UHFFFAOYSA-N 4-chloro-2-nitroaniline Chemical compound NC1=CC=C(Cl)C=C1[N+]([O-])=O PBGKNXWGYQPUJK-UHFFFAOYSA-N 0.000 description 3
230000000052 comparative effect Effects 0.000 description 3
239000000203 mixture Substances 0.000 description 3
239000000126 substance Substances 0.000 description 3
239000003795 chemical substances by application Substances 0.000 description 2
239000000543 intermediate Substances 0.000 description 2
LHHIALSOMNPUOW-UHFFFAOYSA-N n-chloro-n-phenylnitramide Chemical class [O-][N+](=O)N(Cl)C1=CC=CC=C1 LHHIALSOMNPUOW-UHFFFAOYSA-N 0.000 description 2
235000011149 sulphuric acid Nutrition 0.000 description 2
CMYQDOILKQVRGN-UHFFFAOYSA-N 2-chloro-3-nitroaniline Chemical compound NC1=CC=CC([N+]([O-])=O)=C1Cl CMYQDOILKQVRGN-UHFFFAOYSA-N 0.000 description 1
PNPCRKVUWYDDST-UHFFFAOYSA-N 3-chloroaniline Chemical compound NC1=CC=CC(Cl)=C1 PNPCRKVUWYDDST-UHFFFAOYSA-N 0.000 description 1
WFMYUEXTOBKQOY-UHFFFAOYSA-N 4-chloroaniline;nitric acid Chemical class O[N+]([O-])=O.NC1=CC=C(Cl)C=C1 WFMYUEXTOBKQOY-UHFFFAOYSA-N 0.000 description 1
TYMLOMAKGOJONV-UHFFFAOYSA-N 4-nitroaniline Chemical class NC1=CC=C([N+]([O-])=O)C=C1 TYMLOMAKGOJONV-UHFFFAOYSA-N 0.000 description 1
IOVCWXUNBOPUCH-UHFFFAOYSA-N Nitrous acid Chemical compound ON=O IOVCWXUNBOPUCH-UHFFFAOYSA-N 0.000 description 1
125000003277 amino group Chemical group 0.000 description 1
BEHLMOQXOSLGHN-UHFFFAOYSA-N benzenamine sulfate Chemical class OS(=O)(=O)NC1=CC=CC=C1 BEHLMOQXOSLGHN-UHFFFAOYSA-N 0.000 description 1
238000004040 coloring Methods 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000006482 condensation reaction Methods 0.000 description 1
239000013078 crystal Substances 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
239000000975 dye Substances 0.000 description 1
239000000463 material Substances 0.000 description 1
KUDPGZONDFORKU-UHFFFAOYSA-N n-chloroaniline Chemical compound ClNC1=CC=CC=C1 KUDPGZONDFORKU-UHFFFAOYSA-N 0.000 description 1
VBEGHXKAFSLLGE-UHFFFAOYSA-N n-phenylnitramide Chemical compound [O-][N+](=O)NC1=CC=CC=C1 VBEGHXKAFSLLGE-UHFFFAOYSA-N 0.000 description 1
ZODDGFAZWTZOSI-UHFFFAOYSA-N nitric acid;sulfuric acid Chemical compound O[N+]([O-])=O.OS(O)(=O)=O ZODDGFAZWTZOSI-UHFFFAOYSA-N 0.000 description 1
150000002894 organic compounds Chemical class 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
-1 p- Among them Chemical compound 0.000 description 1
239000000049 pigment Substances 0.000 description 1
239000002994 raw material Substances 0.000 description 1
238000007086 side reaction Methods 0.000 description 1
IIACRCGMVDHOTQ-UHFFFAOYSA-N sulfamic acid group Chemical class S(N)(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 description 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

JP9573883A 1983-06-01 1983-06-01 モノクロル−モノニトロアニリン類の製造法 Granted JPS59222451A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP9573883A JPS59222451A (ja)	1983-06-01	1983-06-01	モノクロル−モノニトロアニリン類の製造法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP9573883A JPS59222451A (ja)	1983-06-01	1983-06-01	モノクロル−モノニトロアニリン類の製造法

Publications (2)

Publication Number	Publication Date
JPS59222451A JPS59222451A (ja)	1984-12-14
JPS6360017B2 true JPS6360017B2 (de)	1988-11-22

Family

ID=14145823

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP9573883A Granted JPS59222451A (ja)	1983-06-01	1983-06-01	モノクロル−モノニトロアニリン類の製造法

Country Status (1)

Country	Link
JP (1)	JPS59222451A (de)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP4516609B2 (ja) *	2006-02-10	2010-08-04	三井化学アグロ株式会社	Ｏ−メチル−ｎ−ニトロイソ尿素の製造方法

1983
- 1983-06-01 JP JP9573883A patent/JPS59222451A/ja active Granted

Also Published As

Publication number	Publication date
JPS59222451A (ja)	1984-12-14

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