JPS6422845A - Bischloroformate of tricyclo(5.2.1.02,6)decane-dimethanol and production thereof - Google Patents
Bischloroformate of tricyclo(5.2.1.02,6)decane-dimethanol and production thereofInfo
- Publication number
- JPS6422845A JPS6422845A JP17604587A JP17604587A JPS6422845A JP S6422845 A JPS6422845 A JP S6422845A JP 17604587 A JP17604587 A JP 17604587A JP 17604587 A JP17604587 A JP 17604587A JP S6422845 A JPS6422845 A JP S6422845A
- Authority
- JP
- Japan
- Prior art keywords
- compound
- dimethanol
- decane
- tricyclo
- synthesis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- ZFZDWMXUMXACHS-IACGZSPGSA-N tricyclo[5.2.1.02,6]decane-4,8-dimethanol Chemical compound C([C@H]1C2)C(CO)[C@H]2C2C1CC(CO)C2 ZFZDWMXUMXACHS-IACGZSPGSA-N 0.000 title 1
- 150000001875 compounds Chemical class 0.000 abstract 3
- 238000003786 synthesis reaction Methods 0.000 abstract 3
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 abstract 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 abstract 2
- 230000015572 biosynthetic process Effects 0.000 abstract 2
- 150000002170 ethers Chemical class 0.000 abstract 2
- 239000002994 raw material Substances 0.000 abstract 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 125000001309 chloro group Chemical group Cl* 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000004417 polycarbonate Substances 0.000 abstract 1
- 229920001692 polycarbonate urethane Polymers 0.000 abstract 1
- 229920000642 polymer Polymers 0.000 abstract 1
- 229920002635 polyurethane Polymers 0.000 abstract 1
- 239000004814 polyurethane Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
NEW MATERIAL:The compound of formula. USE:Useful for organic synthesis and polymer synthesis, especially for the synthesis of polycarbonate and polyurethane. It has reactive chlorine groups at both terminals of the molecule. The compound can be produced in high yield and purity by a simple method with little production of by-products. PREPARATION:The compound of formula can be produced by reacting tricyclo[5.2.1.0<2>,<6>]decane-dimethanol with phosgene in the presence of specific ethers as reaction assistant, especially preferably in a solvent such as tetrahydrofuran or dioxane at 0-20 deg.C. The amount of phosgene is 2.0-4.0mol. per 1mol. of the starting raw material and that of the ethers is 5-40pts.wt. per 1pt.wt. of the raw material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17604587A JPS6422845A (en) | 1987-07-16 | 1987-07-16 | Bischloroformate of tricyclo(5.2.1.02,6)decane-dimethanol and production thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17604587A JPS6422845A (en) | 1987-07-16 | 1987-07-16 | Bischloroformate of tricyclo(5.2.1.02,6)decane-dimethanol and production thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS6422845A true JPS6422845A (en) | 1989-01-25 |
Family
ID=16006754
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP17604587A Pending JPS6422845A (en) | 1987-07-16 | 1987-07-16 | Bischloroformate of tricyclo(5.2.1.02,6)decane-dimethanol and production thereof |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6422845A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5439207A (en) * | 1993-02-23 | 1995-08-08 | Hermann Schleicher Gmbh & Co. | Conveyor system for metallic plates and strips |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS507600A (en) * | 1973-05-18 | 1975-01-25 | ||
| JPS62226948A (en) * | 1986-03-28 | 1987-10-05 | Hodogaya Chem Co Ltd | Production of chloroformate having methacryl group at terminal |
-
1987
- 1987-07-16 JP JP17604587A patent/JPS6422845A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS507600A (en) * | 1973-05-18 | 1975-01-25 | ||
| JPS62226948A (en) * | 1986-03-28 | 1987-10-05 | Hodogaya Chem Co Ltd | Production of chloroformate having methacryl group at terminal |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5439207A (en) * | 1993-02-23 | 1995-08-08 | Hermann Schleicher Gmbh & Co. | Conveyor system for metallic plates and strips |
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