JPS6450363U - - Google Patents
Info
- Publication number
- JPS6450363U JPS6450363U JP14592187U JP14592187U JPS6450363U JP S6450363 U JPS6450363 U JP S6450363U JP 14592187 U JP14592187 U JP 14592187U JP 14592187 U JP14592187 U JP 14592187U JP S6450363 U JPS6450363 U JP S6450363U
- Authority
- JP
- Japan
- Prior art keywords
- sample
- bubble detector
- way valve
- supply pipe
- detected
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000002347 injection Methods 0.000 claims description 3
- 239000007924 injection Substances 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims 1
- 238000010586 diagram Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
Landscapes
- Sampling And Sample Adjustment (AREA)
- Automatic Analysis And Handling Materials Therefor (AREA)
Description
第1図は本考案の一実施例を示す構成図、第2
図は一実施例の試料注入手順を示すフローチヤー
トである。
1……六方バルブ、2……試料ループ、3……
試料供給管、4……第1気泡検出器、5……試料
排出管、6……第2気泡検出器、7……計数手段
、8……出力手段、9……移動供給管、10……
カラム流路。
Fig. 1 is a configuration diagram showing one embodiment of the present invention;
The figure is a flowchart showing the sample injection procedure of one embodiment. 1...Six-way valve, 2...Sample loop, 3...
Sample supply pipe, 4...First bubble detector, 5...Sample discharge pipe, 6...Second bubble detector, 7...Counting means, 8...Output means, 9...Movement supply pipe, 10... …
Column flow path.
Claims (1)
との間、及び移動相供給管とカラム流路との間に
試料ループを備えた六方バルブが接続され、この
六方バルブの流路切換えによつて試料ループ内の
試料をカラムに圧送するように構成された自動試
料注入装置において、前記六方バルブの流路切換
え前に試料供給管に試料を流したときに試料供給
管を流れる気泡を検出するために試料供給管の六
方バルブ寄りに取りつけられた第1気泡検出器と
、試料排出管を流れる気泡を検出するために試料
排出管の六方バルブ寄りに取りつけられた第2気
泡検出器と、第1気泡検出器で検出された気泡数
を加算し、第2気泡検出器で検出された気泡数を
減算する計数手段と、この計数手段の計数値が零
になつたときに前記試料送液手段を停止する信号
を送り、次いで前記六方バルブに流路切換え信号
を出力する出力手段とを備えたことを特徴とする
自動試料注入装置。 A six-way valve equipped with a sample loop is connected between a sample supply pipe equipped with a sample liquid feeding means and a sample discharge pipe, and between a mobile phase supply pipe and a column flow path. Therefore, in an automatic sample injection device configured to pump a sample in a sample loop to a column, air bubbles flowing through the sample supply pipe can be detected when the sample is flowed into the sample supply pipe before switching the flow path of the six-way valve. a first air bubble detector installed near the six-way valve of the sample supply pipe to detect air bubbles flowing through the sample discharge pipe, and a second air bubble detector installed near the six-way valve of the sample discharge pipe to detect air bubbles flowing through the sample discharge pipe; a counting means for adding the number of bubbles detected by the first bubble detector and subtracting the number of bubbles detected by the second bubble detector; and a counting means for adding the number of bubbles detected by the first bubble detector and subtracting the number of bubbles detected by the second bubble detector; An automatic sample injection device comprising output means for sending a signal to stop the means and then outputting a flow path switching signal to the six-way valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14592187U JPS6450363U (en) | 1987-09-24 | 1987-09-24 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14592187U JPS6450363U (en) | 1987-09-24 | 1987-09-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS6450363U true JPS6450363U (en) | 1989-03-28 |
Family
ID=31414936
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP14592187U Pending JPS6450363U (en) | 1987-09-24 | 1987-09-24 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6450363U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004317420A (en) * | 2003-04-18 | 2004-11-11 | Hitachi Software Eng Co Ltd | Measuring instrument using capillary |
-
1987
- 1987-09-24 JP JP14592187U patent/JPS6450363U/ja active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004317420A (en) * | 2003-04-18 | 2004-11-11 | Hitachi Software Eng Co Ltd | Measuring instrument using capillary |
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