JPS6459155A - Determination of vanillyl mandelate - Google Patents
Determination of vanillyl mandelateInfo
- Publication number
- JPS6459155A JPS6459155A JP21868887A JP21868887A JPS6459155A JP S6459155 A JPS6459155 A JP S6459155A JP 21868887 A JP21868887 A JP 21868887A JP 21868887 A JP21868887 A JP 21868887A JP S6459155 A JPS6459155 A JP S6459155A
- Authority
- JP
- Japan
- Prior art keywords
- vanillyl
- mandelate
- anthryl
- methyl ester
- determination
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- CGQCWMIAEPEHNQ-UHFFFAOYSA-M vanillylmandelate Chemical compound COC1=CC(C(O)C([O-])=O)=CC=C1O CGQCWMIAEPEHNQ-UHFFFAOYSA-M 0.000 title abstract 5
- -1 anthryl methyl ester Chemical class 0.000 abstract 3
- XXDVOJKRZBNPFN-UHFFFAOYSA-N 9-[(e)-diazomethyl]anthracene Chemical compound C1=CC=C2C(C=[N+]=[N-])=C(C=CC=C3)C3=CC2=C1 XXDVOJKRZBNPFN-UHFFFAOYSA-N 0.000 abstract 2
- 238000004809 thin layer chromatography Methods 0.000 abstract 2
Landscapes
- Investigating Or Analysing Biological Materials (AREA)
Abstract
PURPOSE:To achieve a highly sensitive determination with a handy operation, by treating a vital sample by 9-anthryl diazomethane to form anthryl methyl ester of vanillyl mandelate, which is then applied for a thin layer chromatography. CONSTITUTION:A vital sample is mixed with a solution of 9-anthryl diazomethane under a normal temperature to form anthryl methyl ester of vanillyl mandelate. This treated solution is applied for a thin layer chromatography and vanillyl mandelate in the vital sample is determined from intensity of fluorescence from an anthryl methyl ester fraction produced by light irradiation. This enables easy highly sensitive determination of vanillyl mandelate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP21868887A JPS6459155A (en) | 1987-08-31 | 1987-08-31 | Determination of vanillyl mandelate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP21868887A JPS6459155A (en) | 1987-08-31 | 1987-08-31 | Determination of vanillyl mandelate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS6459155A true JPS6459155A (en) | 1989-03-06 |
Family
ID=16723856
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP21868887A Pending JPS6459155A (en) | 1987-08-31 | 1987-08-31 | Determination of vanillyl mandelate |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6459155A (en) |
-
1987
- 1987-08-31 JP JP21868887A patent/JPS6459155A/en active Pending
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