KR101979658B1 - Manufacturing method of composition for hair-loss prevention and hair growth using shungite - Google Patents
Manufacturing method of composition for hair-loss prevention and hair growth using shungite Download PDFInfo
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- KR101979658B1 KR101979658B1 KR1020190010080A KR20190010080A KR101979658B1 KR 101979658 B1 KR101979658 B1 KR 101979658B1 KR 1020190010080 A KR1020190010080 A KR 1020190010080A KR 20190010080 A KR20190010080 A KR 20190010080A KR 101979658 B1 KR101979658 B1 KR 101979658B1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
본 발명은 순지트를 이용한 탈모 방지 및 발모 촉진용 화장료 조성물 및 그 제조 방법에 관한 것이다.
본 발명의 순지트를 이용한 탈모 방지 및 발모 촉진용 화장료 조성물은 상기와 같은 과제를 해결하기 위하여, 탈모 방지 및 발모 촉진용 화장료 조성물에 있어서, 화장료 베이스 100 중량부와, 하이드롤라이즈드케라틴 2 ~ 5중량부와, 허브수 3 ~ 6 중량부 및 순지트 분말 1 ~ 3 중량부를 포함하여 구성된다.
본 발명에 의해, 탈모 방지 및 발모 촉진에 효과가 있는 것으로 알려진 하이드롤라이즈드케라틴에 순지트 분말을 유효 성분으로 포함시킴으로써 제형의 안정성이 보다 더 향상될 수 있게 되고, 두피와 모발 안정화에 활력을 주고, 보습과 피지 분비를 돕고, 피부 탄력성을 높이는 허브수가 함께 함유되도록 구성됨으로써 탈모 방지 및 발모 촉진을 향상시킬 수 있게 되며, 유동층코팅기를 이용하여 순지트 분말에 하이드롤라이즈드케라틴이 견고하게 흡착된 상태의 비드를 제조하고, 이 비드를 이용하여 화장료 조성물을 제조함으로써 하이드롤라이즈드케라틴이 고르게 분산된 상태가 되도록 함으로써 효능 효과를 극대화시킬 수 있게 된다.The present invention relates to a cosmetic composition for preventing hair loss and promoting hair growth using a sunflower and a method for producing the same.
The present invention provides a cosmetic composition for preventing hair loss and promoting hair growth, which comprises 100 parts by weight of a cosmetic base, 2 parts by weight of hydrolyzed keratin, 3 to 6 parts by weight of a herb, and 1 to 3 parts by weight of a pure starch powder.
According to the present invention, the stability of the formulation can be further improved by incorporating the pure powder of the starch powder into the hydrolyzed keratin, which is known to be effective for preventing hair loss and promoting hair growth, as an active ingredient, It is possible to improve the hair loss prevention and hair growth promoting ability by providing the number of herbs that increase the elasticity of the skin together with moisturizing and sebum secretion, and it is possible to improve the hair loss prevention and promotion of hair growth, and the hydrolyzed keratin is firmly adsorbed , And the cosmetic composition is prepared by using the beads, so that the hydrolized keratin is uniformly dispersed, thereby maximizing the efficacy.
Description
본 발명은 탈모 방지 및 발모 촉진용 화장료 조성물 및 그 제조 방법에 관한 것으로, 특히 천연 플러렌이 다량 포함되어 있는 순지트에 케라틴과 허브수를 첨가하여 화장료를 제조함으로써, 탈모 방지 및 발모 촉진 효과를 높인, 순지트를 이용한 탈모 방지 및 발모 촉진용 화장료 조성물 및 그 제조 방법에 관한 것이다.The present invention relates to a cosmetic composition for preventing hair loss and promoting hair growth and a method for producing the same, and more particularly, to a cosmetic composition containing keratine and herb water in which a large amount of natural fullerene is contained, The present invention relates to a cosmetic composition for preventing hair loss and promoting hair growth using sunflower, and a method for producing the same.
탈모란 정상적으로 모발이 있어야 할 곳에 모발이 없는 상태를 말하며 유전적 요인이 가장 주요한 원인으로 알려져 있다. Hair loss refers to the state of hair where hair normally should be present, and genetic factors are known to be the main cause.
최근 사회적 스트레스의 증가와 더불어 환경오염 및 인스턴트 식품 등 서구화된 식습관, 잦은 파마와 염색, 잘못된 두피관리들로 인하여 탈모 인구가 점차 증가하고 있는 추세이다. Recently, with the increase of social stress, the hair loss population is gradually increasing due to westernized eating habits such as environmental pollution and instant food, frequent perm and dyeing, and incorrect scalp care.
그러나 아직까지 탈모에 대한 명확한 원인은 규명되고 있지 않았고, 최근 들어 오히려 탈모증으로 고민하는 사람이 점점 늘고 있으며 그 연령층도 낮아지고 있는 실정이다.However, the definite cause of hair loss has not yet been clarified. Recently, more and more people are suffering from alopecia, and the age group is lowering.
탈모증의 치료법에 관해서도 아직까지 뚜렷한 효과를 지닌 것은 없으며, 동의보감에서는 신응양진단 등 탈모에 관계되는 몇몇 복용하는 처방들이 있고, 호마유(참깨) 등을 탈모 부위에 마사지한다든지, 특정 한약처방을 주침해서 바르는 방법과 특정 혈위를 자극하는 방법 등이 있지만 효과에 있어서는 개인적 차이가 많다고 알려져 있다. There are no clear effects on the treatment of alopecia, and there are some prescriptions for taking hair loss, such as diagnosis of newborns in Dong-bo-gyung, and massage of sesame seeds on hair loss site, It is known that there are many individual differences in the effects, such as how to apply and how to stimulate specific blood circulation.
또한, 일반적으로 적용될 수 있는 신약 소재는 아직까지 보고되지 않고 있다.In addition, there is no report of a new drug substance that can be generally applied.
종래의 탈모증 치료방법으로는, 호르몬설과 관련하여 여성 호르몬을 주재료한 제제가 있으나 피부 염증 발생, 호르몬 투여에 의한 부작용 발생 등의 보고가 있어 현재는 사용이 중단되고 있다. As a conventional method for treating alopecia, there is a preparation based on female hormone in relation to hormonal theory, but there is a report of occurrence of skin inflammation and adverse effect due to administration of hormone, and its use is being stopped at present.
최근 사용되고 있는 대표적인 발모제로는, 처음에는 혈액 순환 촉진을 위한 용도로 개발되어 사용되다가 이를 사용하는 환자들 사이에서 부작용으로 발모 효과를 나타내는 것으로 알려져, 이후, 발모용 원료로 미국식품의약품안전청(FDA)에서 승인받아 발모 치료제로 사용되고 있는 미국특허 제3,382,247호의 미녹시딜(6-Amino-1,2-dihydro-1-hydroxy-2-imino-4-phenoxypyrimidine)및 미국특허 제 5,215,894 호에서 언급된 머크사의 피나스테라이드(finasteride)가 있다.It is known that the hair growth inhibitory effect is caused by side effects among patients who have been developed and used for promotion of blood circulation at first, and then the US Food and Drug Administration (FDA) 6-Amino-1,2-dihydro-1-hydroxy-2-imino-4-phenoxypyrimidine of U.S. Patent No. 3,382,247, which has been approved by the US Patent No. 5,215,894, finasteride.
그러나, 미녹시딜의 경우 끈적이는 사용감과 피부에 자극을 유발하는 부작용이 보고된 바 있으며, 피나스테라이드의 경우 현재 경구투여용 제제로 사용되고 있으나, 이의 섭취에 따라 성기능 장애 등의 부작용이 보고된 일도 있을 뿐 아니라, 탈모에 대해서도 꾸준한 복용이 이루어져야만 효과가 있다는 부작용이 있다.However, minoxidil has been reported to have a sticky feel and side effects that cause irritation to the skin. In the case of pinasteride, it is currently used as a preparation for oral administration. However, adverse effects such as sexual dysfunction have been reported depending on its consumption, There is a side effect that hair loss should be treated consistently.
이러한 문제점을 해소하기 위한 노력의 하나로 "탈모방지 및 발모촉진용 주사용 조성물"(한국 등록특허공보 제10-1859421호, 특허문헌 1)에서는 가수분해된 케라틴을 이용하여 탈모 방지 및 발모 촉진이 이루어지는 것이 확인된 바 있다.As one of efforts to solve such a problem, "composition for preventing hair loss and promoting hair growth" (Korean Patent Registration No. 10-1859421, Patent Document 1) discloses a method of preventing hair loss and promoting hair growth by using hydrolyzed keratin It has been confirmed.
이러한 가수분해된 케라틴은 유해도 등급이 2로 낮으면서 발모 촉진 및 탈모 방지에 효과가 있는 것으로 알려졌다.These hydrolyzed keratins are known to be effective in promoting hair growth and preventing hair loss while lowering the harmfulness grade to 2.
그러나, 샴푸나 헤어 로션을 이루는 다른 성분과 고르게 혼합 또는 분산된 상태를 이루지 못하여 그 효과를 균일하게 보지 못하는 문제점이 있었다.However, there is a problem in that it can not be uniformly mixed or dispersed with other components constituting shampoo or hair lotion, and the effect can not be seen uniformly.
본 발명의 순지트를 이용한 탈모 방지 및 발모 촉진용 화장료 조성물 및 그 제조 방법은 상기와 같은 종래 기술에서 발생하는 문제점을 해소하기 위한 것으로, 탈모 방지 및 발모 촉진에 효과가 있는 것으로 알려진 하이드롤라이즈드케라틴에 순지트 분말을 유효 성분으로 포함시킴으로써 효능효과가 보다 더 향상될 수 있게 하려는 것이다.The cosmetic composition for preventing hair loss and promoting hair growth using the sunflower of the present invention and the method for producing the same are intended to overcome the problems caused by the conventional art as described above and to provide a cosmetic composition for preventing hair loss and hydrocolloid, It is intended to further enhance the efficacy by incorporating a nett powder into the keratin as an active ingredient.
또, 두피와 모발 안정화에 활력을 주고, 보습과 피지 분비를 돕고, 피부 탄력성을 높이는 허브수가 함께 함유되도록 구성됨으로써 탈모 방지 및 발모 촉진을 향상시킬 수 있게 하려는 것이다.In addition, it is constituted so as to provide vitality to scalp and hair stabilization, to help moisturizing and sebum secretion, and to contain a number of herbs that increase skin elasticity, thereby preventing hair loss and promoting hair growth.
또한, 유동층코팅기를 이용하여 순지트 분말에 하이드롤라이즈드케라틴이 견고하게 흡착된 상태의 비드를 제조하고, 이 비드를 이용하여 화장료 조성물을 제조함으로써 하이드롤라이즈드케라틴이 고르게 분산된 상태가 되도록 함으로써 효능효과를 극대화시킬 수 있게 하려는 것이다.Also, by using a fluidized bed coater to prepare a bead in which the hydrolized keratin is firmly adsorbed to the pure powder, and the cosmetic composition is prepared using the bead so that the hydrolized keratin is uniformly dispersed Thereby maximizing the efficacy effect.
본 발명의 순지트를 이용한 탈모 방지 및 발모 촉진용 화장료 조성물은 상기와 같은 과제를 해결하기 위하여, 탈모 방지 및 발모 촉진용 화장료 조성물에 있어서, 화장료 베이스 100 중량부와, 하이드롤라이즈드케라틴 2 ~ 5중량부와, 허브수 3 ~ 6 중량부 및 순지트 분말 1 ~ 3 중량부를 포함하여 구성된다.The present invention provides a cosmetic composition for preventing hair loss and promoting hair growth, which comprises 100 parts by weight of a cosmetic base, 2 parts by weight of hydrolyzed keratin, 3 to 6 parts by weight of a herb, and 1 to 3 parts by weight of a pure starch powder.
상기한 구성에 있어서, 상기 허브수는, 페퍼민트 잎수, 로즈마리 잎수, 카모마일 꽃수, 쟈스민 꽃수가 동일 중량비로 혼합되어 구성된 것을 특징으로 한다.In the above-mentioned constitution, the number of herbs is characterized in that the number of peppermint leaf, rosemary leaf, chamomile flower, and jasmine flower are mixed at the same weight ratio.
또, 상기 순지트 분말은 러시아 북부 카멜리아 지역의 슝가에서 생산되고, 플러렌 함량이 60 중량% 이상인 것을 특징으로 한다.In addition, the pure powder is produced in Schungga in the Camellia region, northern Russia, and has a fullerene content of 60 wt% or more.
또한, 상기 순지트 분말은 6.5 ~ 10㎛의 입자 크기를 갖는 것을 특징으로 한다.In addition, the pure powder is characterized by having a particle size of 6.5 to 10 탆.
본 발명의 순지트를 이용한 탈모 방지 및 발모 촉진용 화장료 조성물 제조 방법은, 화장료 베이스 100 중량부를 준비하는 베이스준비단계와; 순지트 광물을 준비한 후, 6.5 ~ 10㎛의 입자 크기를 갖도록 분쇄하여 순지트 분말 1 ~ 3 중량부를 제조하는 분쇄단계와; 페퍼민트 잎수, 로즈마리 잎수, 카모마일 꽃수, 쟈스민 꽃수를 동일 중량비로 혼합하여 허브수 3 ~ 6 중량부를 제조하는 허브수준비단계와; 하이드롤라이즈드케라틴 2 ~ 5 중량부를 준비한 후, 준비된 허브수 중 1 ~ 3 중량부와 혼합 교반하여 혼합액을 제조하는 혼합액제조단계와; 유동층 코팅기를 이용하여 상기 순지트 분말에 상기 혼합액을 유동층 코팅시키되, 유동층 코팅기의 내부로 상기 순지트 분말을 공급하면서, 흡입공기량 5 ~ 15㎥/sec, 투입관 온도 80 ~ 150℃, 분무압력 1.0 ~ 5.0bar, 분무속도 1 ~ 10kg/hr의 유동층코팅 조건 하에서 바텀스프레이 방식으로 혼합액을 분무하면서 유동화를 실시하여 입자 크기 8 ~ 15㎛ 크기의 순지트비드를 제조하는 유동층코팅단계와; 상기 순지트비드와 잔량의 허브수 및 화장료 베이스를 혼합하여 화장료 조성물을 제조하는 화장료제조단계;를 포함하여 구성된다.The method for preparing a cosmetic composition for preventing hair loss and promoting hair growth using the sunflower of the present invention comprises: a base preparation step of preparing 100 parts by weight of a cosmetic base; Preparing a pureite mineral and pulverizing it to have a particle size of 6.5 to 10 mu m to produce 1 to 3 parts by weight of a pure starch powder; Peppermint leaf water, rosemary leaf water, chamomile flower water, and jasmine flower water at an equal weight ratio to prepare 3 to 6 parts by weight of herbs; Preparing 2 to 5 parts by weight of hydrolyzed keratin, and mixing and stirring the mixture with 1 to 3 parts by weight of the prepared herb water to prepare a mixed solution; The mixture liquid was coated on the pure powder by using a fluidized bed coater, while the pure powder was supplied into the fluidized bed coater, the inlet air amount was 5 to 15 m 3 / sec, the inlet tube temperature was 80 to 150 ° C, the spray pressure was 1.0 A fluidized bed coating step of spraying a mixed solution in a bottom spraying method under a fluidized bed coating condition at a spray rate of 1 to 10 kg / And a cosmetic preparation step of preparing a cosmetic composition by mixing the purified tooth beads with the remaining number of herbs and the cosmetic base.
본 발명에 의해, 탈모 방지 및 발모 촉진에 효과가 있는 것으로 알려진 하이드롤라이즈드케라틴에 순지트 분말을 유효 성분으로 포함시킴으로써 효능 효과가 보다 더 향상될 수 있게 된다.According to the present invention, it is possible to further improve the efficacy by incorporating the purified powder into the hydrolyzed keratin, which is known to be effective in preventing hair loss and promoting hair growth.
또, 두피와 모발 안정화에 활력을 주고, 보습과 피지 분비를 돕고, 피부 탄력성을 높이는 허브수가 함께 함유되도록 구성됨으로써 탈모 방지 및 발모 촉진을 향상시킬 수 있게 된다.In addition, it is possible to improve the hair loss prevention and hair growth promotion by providing vitality to scalp and hair stabilization, helping moisturizing and sebum secretion, and containing the number of herbs that increase skin elasticity.
또한, 유동층코팅기를 이용하여 순지트 분말에 하이드롤라이즈드케라틴이 견고하게 흡착된 상태의 비드를 제조하고, 이 비드를 이용하여 화장료 조성물을 제조함으로써 하이드롤라이즈드케라틴이 고르게 분산된 상태가 되도록 함으로써 효능 효과를 극대화시킬 수 있게 된다.Also, by using a fluidized bed coater to prepare a bead in which the hydrolized keratin is firmly adsorbed to the pure powder, and the cosmetic composition is prepared using the bead so that the hydrolized keratin is uniformly dispersed Thereby maximizing the efficacy effect.
이하, 본 발명의 순지트를 이용한 탈모 방지 및 발모 촉진용 화장료 조성물 및 그 제조 방법에 대해 상세히 설명하기로 한다.Hereinafter, the cosmetic composition for preventing hair loss and promoting hair growth and using the sunflower of the present invention will be described in detail.
본 발명에서 화장료 조성물은, 그 종류나 제형 등은 제한되지 않는다. 본 발명에서 화장료 조성물은 모발에 적용되는 것이면 여기에 포함한다.The kind and formulation of the cosmetic composition in the present invention are not limited. The cosmetic composition according to the present invention is included in the present invention as long as it is applied to hair.
구체적으로 본 발명에 따른 화장료 조성물은, 그 제품 형태의 종류에 있어서, 모발의 청결을 위한 샴푸나 린스, 모발의 염색을 위한 염색제, 탈모를 방지하는 탈모 방지제, 발모를 촉진하는 발모제 등의 제품을 포함한다. Specifically, the cosmetic composition according to the present invention can be applied to various kinds of product types such as shampoo or rinse for cleansing hair, a dye for dyeing hair, a hair loss preventing agent for preventing hair loss, a hair growth agent for promoting hair growth .
즉, 본 발명에 따른 화장료 조성물은 샴푸, 린스, 염색제, 탈모 방지제 및 발모제 등으로부터 선택된 하나 이상의 제품이 될 수 있다. That is, the cosmetic composition according to the present invention may be at least one product selected from shampoos, rinses, dyes, hair loss inhibitors, hair growth agents and the like.
본 발명에 따른 화장료 조성물은 기본적으로 화장료의 기본적인 기능을 위한 화장료 베이스를 주성분으로 하며, 여기에 하이드롤라이즈드케라틴, 허브수 및 순지트 분말을 포함하여 구성된다.The cosmetic composition according to the present invention basically comprises a cosmetic base for the basic functions of the cosmetic as a main component, and comprises the hydrolized keratin, the number of herbs and the pure powder.
본 발명의 구성요소인 하이드롤라이즈드케라틴은 산이나 효소 등의 가수분해 방법으로 얻은 케라틴 단백 가수분해물의 수용액을 의미한다.The hydrolized keratin, which is a component of the present invention, means an aqueous solution of a keratin protein hydrolyzate obtained by a hydrolysis method of an acid or an enzyme.
이러한 하이드롤라이즈드케라틴은 모발에 컨디셔닝을 부여하여 활력을 주고, 머리 손질을 용이하게 하며, 모발 표면에 피막을 형성하여 정전기를 방지하는 것으로 알려져 근래에 샴푸, 탈모방지제 등으로 주로 사용되고 있다.These hydrolyzed keratins are known to impart conditioning to hair to provide vitality, facilitate hair treatment, and form a film on the surface of the hair to prevent static electricity, and have recently been used mainly as shampoos, hair loss inhibitors, and the like.
그런데, 이러한 하이드롤라이즈드케라틴은 비교적 점성이 높기 때문에 샴푸나 린스와 같이 액상의 화장료로 사용시 시간이 경과함에 따라 용기 내부에서 층을 이루거나 용기 벽면에 달라붙게 되어 배합 비율과 달리 실제 사용시 일정하고 고르게 분포되어 있지 못하게 되고, 이로 인해 화장료로 배합되는 성분 중의 피부 자극성 물질의 함량이 상대적으로 높아지게 되어 피부 자극 현상이 일어나게 될 수 있다.However, since the hydrolized keratin is relatively viscous, it becomes a layer in the container or adheres to the wall of the container due to the passage of time when it is used as a liquid cosmetic such as shampoo or rinse, So that the content of the skin irritating substance in the ingredient to be mixed with the cosmetic material becomes relatively high, and the skin irritation phenomenon may occur.
본 발명의 구성요소인 허브수는 이러한 문제를 해소할 수 있도록 하는 것으로, 염증에 대한 살균 및 정화 작용을 갖는 페퍼민트 잎수나 쟈스민 꽃수를 포함하여 피부 자극 물질로부터 두피를 보호해줄 수 있게 해준다.The number of herbs, which is a constituent of the present invention, can solve this problem, and it can protect the scalp from skin irritants such as peppermint leaves and jasmine flowers having sterilization and purifying action against inflammation.
또, 피부 탄력성을 높여주는 카모마일 잎수나 모발 성장을 촉진하는 것으로 알려져 있는 로즈마리 잎수가 함께 사용되어 그 자체로 탈모 방지 및 발모 촉진에 기여할 수 있도록 한다.In addition, the rosemary leaf number, which is known to promote the number of chamomile leaves or hair growth that increases the elasticity of the skin, is used together to contribute to prevention of hair loss and promotion of hair growth.
이를 위한 적절한 허브수의 배합은 페퍼민트 잎수, 로즈마리 잎수, 카모마일 꽃수, 쟈스민 꽃수가 동일 중량비로 혼합되어 구성된 것이 바람직하다.For this purpose, it is preferable that the combination of the number of herbs is the same as that of peppermint leaf, rosemary leaf, chamomile flower, and jasmine flower.
페퍼민트 잎은 가려움, 염증, 햇빛에 그을림 등을 진정시키며, 염증부위의 살균, 정화의 기능이 있어 두피와 모발을 안정시키면서 활력을 주는 효과가 있고, 여드름, 지성두피, 지성 머리결의 피지분비 정상화에 사용되어오고 있다.Peppermint leaves calms the itching, inflammation and sunburn, and has the function of sterilizing and cleansing the inflamed area, stabilizing the scalp and hair, revitalizing the sebaceous glands of acne, oily scalp and oily hair. Has been used.
쟈스민 꽃은 피부(건조성 민감피부)에 탄력을 주는 성분이 포함되어 있고, 염증을 줄이고 상처를 치료하며 적당한 보습과 피지의 분비를 도우며 민감성 피부에게도 적당할 정도로 부드럽고 자극이 적어 피부의 관리에 좋다고 알려져 있다.Jasmine blossom contains ingredients that give elasticity to the skin (dry sensitive skin), reduces inflammation, treats wounds, helps moisturize and secretes sebum, and is soft enough for sensitive skin have.
카모마일 꽃은 항염증 작용이 강하여 상처를 빠르게 회복시키고 조직 재생을 빠르게 하며 특히 화상에 뚜렷한 효과가 있으며, 피부의 탄력성을 높여주고 건조하고 가려움증이 있는 피부에 좋은 효과가 있고, 박테리아 감염이나 공기중의 물질에 의한 자극으로부터 보호하여 다른 허브들에 비해 독성이 적은 것으로 알려져 있다.Chamomile flower has a strong anti-inflammatory action, so it can quickly restore wounds and accelerate tissue regeneration. Especially, it has a remarkable effect on burns, increases elasticity of skin, has good effect on dry and itching skin, It is known to be less toxic than other herbs by protecting against stimuli by substances.
로즈마리 잎은 엘라스틴 분해효소를 억제하고 피부를 재생시켜 늘어진 조직에 활력을 주고 부종과 비듬 발생을 억제하며 모발 성장을 촉진하고, 피부의 윤기와 탄력을 유지하며 수렴작용을 하고 살균 소독력이 풍부한 것으로 알려져 있다.Rosemary leaves inhibit elastin degradation enzymes, regenerate skin, revitalize stretched tissues, inhibit swelling and dandruff, promote hair growth, maintain skin's radiance and elasticity, and act as a disinfectant. have.
특히, 로즈마리 잎에는 클롤로겐산이 다른 허브 원료에 비해 다량 포함되어 있는데, 이 클로로겐산은 항염 및 항균 작용을 하여 두피 질환 개선에 효과가 있는 것으로 알려져 있다.In particular, rosemary leaves contain clorogenic acid in a large amount compared to other herb ingredients, and this chlorogenic acid is said to be effective for the improvement of scalp disease by anti-inflammatory and antibacterial action.
상기한 허브 원료를 이용하여 허브수를 제조하는 방식은 호호바나 올리브 등과 같은 식물성 오일에 일정기간 동안 담궈 지용성 유효성분을 추출하는 방법, 도수가 높은 알콜에 담궈 수용성 및 지용성 성분을 모두 추출하는 방법, 물을 끓여 수용성 성분을 추출하는 방법 등이 알려져 있다.The method of manufacturing the herb water using the above-mentioned herb raw materials includes a method of extracting a fat-soluble active ingredient by dipping in a vegetable oil such as jojoba or olive for a certain period of time, a method of extracting both water- And a method in which water is boiled to extract a water-soluble component.
본 발명에서 가장 바람직한 허브수 제조 방식은 물에 넣고 끓인 다음 고형물을 제거하는 방식으로 제조됨이 가장 바람직하다.It is most preferred that the most preferred method for preparing the herb water in the present invention is prepared by adding water, boiling, and then removing the solids.
통상적으로 이러한 물 추출 방식을 사용할 경우 유통 기간이 짧아지는 단점이 있어 긴 유통기간을 요하는 공정에서는 사용하지 않는 방식이나, 본 발명에서는 순지트가 포함됨에 따라 종래와 유사한 보존 기간이 제공될 수 있게 되며, 다른 추출 방식에 비해 허브의 독성을 현저하게 낮춰줄 수 있게 된다.In general, when such a water extraction method is used, there is a disadvantage in that the distribution period is shortened and is not used in a process requiring a long circulation period. However, in the present invention, And can significantly reduce the toxicity of the herb compared to other extraction methods.
더불어, 전술한 원료의 배합비는 상기한 배합 비율로 한정될 경우가 가장 적절하다.In addition, it is most appropriate that the above-mentioned blending ratio of the raw materials is limited to the blending ratio described above.
만일 상기한 허브 원료의 배합을 가변시킬 경우 각 허브가 갖고 있는 고유의 향 때문에 향의 조화가 이루어지지 못해 사람에 따라 기호도를 떨어뜨리는 문제점이 발생할 수 있게 된다.If the mixing ratio of the raw materials of the hub is changed, the fragrance of the fragrance can not be harmonized due to the inherent fragrance of each hub, which may cause the preference of a person to be lowered.
본 발명의 구성요소인 순지트 분말은 하이드롤라이즈드케라틴이 화장료 베이스 상에 고르게 분포될 수 있도록 해줌과 더불어, 허브 원료가 물 추출되어 제조된 허브수의 보존 기간을 증대시켜주는 역할을 한다.The sunit powder, which is a component of the present invention, allows the hydrolized keratin to be evenly distributed on the cosmetic base, and enhances the shelf life of the herb water produced by the water extraction of the herb raw material.
순지트는 러시아의 카렐리아 슝가 지역을 원료로 하는 광물로 규산염과 플러렌을 주 성분으로 하며, 여기서 플러렌은 천연 플러렌을 의미한다.Sungit is a mineral originating from Russia's Karelia-Shunga region, mainly composed of silicate and fullerene, where fullerene refers to natural fullerene.
순지트에서 플러렌의 함량에 따라 순지트는 노멀 순지트, 엘리트 순지트로 구분하기도 한다.Depending on the content of fullerene in the nettit, the nettit may be divided into normal nettite and elite nettite.
순지트에 다량 포함되어 있는 플러렌은 흑연이나 다이아몬드와 같은 탄소 동소체이나 흑연이나 다이아몬드와는 다른 구조적 형태를 가짐으로 인하여, 제3의 탄소 동소체로 불린다.Fullerene, which is contained in a large amount in the pure tungsten, is called a third carbon isotope because it has a structural form different from carbon isotopes such as graphite and diamond or graphite or diamond.
플러렌은, 탄소(C) 원자가 5각형이나 6각형으로 배열 연결된 탄소 고리를 가지며, 이러한 탄소 고리들이 대략 구체(구형) 등의 형상으로 결합되어 중공(中空)을 형성하고 있다. Fullerene has a carbon ring in which carbon (C) atoms are connected in a pentagonal or hexagonal arrangement, and these carbon rings are bonded in a substantially spherical shape to form a hollow.
이러한 플러렌의 기능으로 현재까지 전자파 차단, 살균, 항균, 항산화, 오염물질 정화, 산화방지제의 기능을 발휘하는 것으로 알려져 있다.As a function of such fullerene, it is known to exert functions of electromagnetic wave shielding, sterilization, antibacterial, antioxidant, pollutant purification and antioxidant to date.
본 발명에 적용되는 순지트 분말은 러시아 북부 카멜리아 지역의 슝가에서 생산되고, 플러렌 함량이 60 중량% 이상인 것이 바람직하다.The pure zeitic powders to be applied in the present invention are produced in Schunggas in the Camellia region, northern Russia, and preferably have a fullerene content of 60 wt% or more.
더하여, 입자 크기는 다양하게 미분화되어 적용될 수 있으나, 6.5 ~ 10㎛의 입자 크기를 갖는 것이 보다 바람직하다.In addition, the particle size can be applied in various micronized form, but it is more preferable to have a particle size of 6.5 to 10 mu m.
만일 상기 분말 크기보다 작게 이루어질 경우 후술하는 유동층 코팅 방식의 제조가 어렵게 되며, 상기 분말 크기보다 크게 이루어질 경우 비드의 크기가 커지게 되고 이로 인해 화장료 사용시 이물감이 발생할 수 있게 된다.If the size of the beads is smaller than the size of the powder, it becomes difficult to manufacture a fluidized bed coating method described later. When the size of the beads is larger than the size of the powder, the size of the beads becomes large.
이러한 순지트 분말은 원료 자체를 분쇄하여 플러렌만을 추출한 후 이물질을 제거하여 사용할 수 있다.Such pure powder can be used by pulverizing the raw material itself, extracting only fullerene, and removing the foreign material.
이때, 최대한 천연 플러렌 함량을 높일 수 있도록 하기 위하여 알칼리 용액을 이용한 가열 추출 방식이 적용될 수 있으며, 추출시 붕소 분위기로 유지하여 탄소 성분을 분리할 수 있다.In this case, in order to increase the natural fullerene content as much as possible, a heating extraction method using an alkali solution may be applied, and the carbon component may be separated by maintaining the boron atmosphere during the extraction.
또는 순지트를 미세하게 분쇄한 다음 알칼리 용액으로 가열하거나 그 자체로 원심분리하여 플러렌 성분을 분리할 수 있다.Alternatively, the fullerene may be finely pulverized and then heated with an alkali solution or centrifuged by itself to separate the fullerene component.
탄소 성분의 함량을 높이기 위해서는 전술한 방식이 적당하나, 이 경우 축구공 형태의 탄소 원자 결합 구조가 깨어지기 쉬위므로 미분쇄 후 원심분리 방식이 적절하다.In order to increase the content of the carbon component, the above-mentioned method is suitable. In this case, the carbon atom bonding structure in the form of a soccer ball is liable to break, so that the centrifugal separation method after pulverization is suitable.
본 발명의 순지트를 이용한 탈모 방지 및 발모 촉진용 화장료 조성물 제조는 통상의 화장료 조성물 제조 방식처럼 화장료 베이스와, 하이드롤라이즈드케라틴과, 허브수 및 순지트 분말을 단순 혼합 교반하는 방식으로 제조될 수 있다.The production of a cosmetic composition for preventing hair loss and hair growth using the sunflower of the present invention can be carried out by simply mixing and stirring a cosmetic base, a hydrated cheese, a herb lot and a pure starch powder, .
이때의 배합비는 화장료 베이스 100 중량부를 기준으로, 순지트 분말은 1 ~ 3중량부, 허브수 3 ~ 6 중량부, 하이드롤라이즈드케라틴 2 ~ 5 중량부로 구성됨이 바람직하다.At this time, the compounding ratio is preferably 1 to 3 parts by weight of the pure starch powder, 3 to 6 parts by weight of the herb and 2 to 5 parts by weight of the hydrolized keratin based on 100 parts by weight of the cosmetic base.
만일 순지트 분말이 상기 중량 최소치 미달일 경우 순지트의 효과 발휘가 원할하지 못하고, 상기 중량 최대치를 초과할 경우 제품 단가가 상승하고, 화장료로 사용시 이물감이 발생하는 문제점이 있게 된다.If the weight of the starch powder is less than the above minimum value of the weight, the effect of the pure starch may not be exhibited. If the weight of the starch powder exceeds the weight value, the unit price of the starch powder increases.
상기와 같은 단순 혼합 방식만으로도 충분히 순지트 분말의 중공 내부로 하이드롤라이즈드케라틴 성분과 허브수 성분이 포함될 수 있고, 이로 인해 제형 안정성이 향상되고, 하이드롤라이즈드케라틴 성분의 균일 분포가 이루어지나, 유동층 코팅 방식을 활용하여 하이드롤라이즈드케라틴 성분을 보다 균일하게 분포시키고, 유통 기간을 극대화시킬 수 있다.The hydrolized keratin component and the herb water component can be sufficiently contained in the hollow interior of the pure starch powder only by the simple mixing method as described above, thereby improving the formulation stability and uniform distribution of the hydrolized keratin components , The fluidized bed coating method can be utilized to more uniformly distribute the hydrolized keratin components and to maximize the circulation period.
이를 위한 제조 방법은 베이스준비단계, 분쇄단계, 허브수준비단계, 혼합액제조단계, 유동층코팅단계, 화장료제조단계로 구성된다.The preparation method comprises a base preparation step, a pulverization step, a hub preparation step, a mixture preparation step, a fluidized bed coating step, and a cosmetic preparation step.
베이스준비단계는 전술한 것처럼 화장료 베이스 100 중량부를 준비하는 것으로 구성되며, 분쇄단계는 순지트 광물을 준비한 후, 6.5 ~ 10㎛의 입자 크기를 갖도록 분쇄하여 순지트 분말 1 ~ 3 중량부를 제조하는 것으로 이루어진다.The base preparation step comprises preparing 100 parts by weight of a cosmetic base as described above, and the pulverization step is a step of preparing pure ground minerals and then pulverizing the particles to have a particle size of 6.5 to 10 탆 to prepare 1 to 3 parts by weight of pure starch powder .
허브수준비단계는 페퍼민트 잎수, 로즈마리 잎수, 카모마일 꽃수, 쟈스민 꽃수를 동일 중량비로 혼합하여 허브수 3 ~ 6 중량부를 제조하는 것으로 구성된다.The preparation step of the herb consists of mixing 3 to 6 parts by weight of herbs by mixing peppermint leaf water, rosemary leaf water, chamomile flower water and jasmine flower water at the same weight ratio.
이때의 허브수는 물에 허브 원료로 넣고 가열한 후 고형물을 제거한 것으로 특정될 수 있다.At this time, the number of the herb can be specified as the herb raw material in water, heated, and then the solids removed.
한편, 혼합액제조단계는 상기 하이드롤라이즈드케라틴 2 ~ 5 중량부를 준비한 후, 준비된 허브수 중 1 ~ 3 중량부와 혼합 교반하여 혼합액을 제조하는 것으로 구성된다.Meanwhile, 2 to 5 parts by weight of the hydrolized keratin is prepared, and 1 to 3 parts by weight of the prepared herbal water is mixed and stirred to prepare a mixed solution.
유동층코팅단계는 유동층 코팅기를 이용하여 상기 순지트 분말에 상기 혼합액을 유동층 코팅시키되, 유동층 코팅기의 내부로 상기 순지트 분말을 공급하면서, 흡입공기량 5 ~ 15㎥/sec, 투입관 온도 80 ~ 150℃, 분무압력 1.0 ~ 5.0bar, 분무속도 1 ~ 10kg/hr의 유동층코팅 조건 하에서 바텀스프레이 방식으로 혼합액을 분무하면서 유동화를 실시하여 입자 크기 8 ~ 15㎛ 크기의 순지트비드를 제조하는 것으로 구성된다.In the fluidized bed coating step, the mixed fluid is coated on the pure powder by using a fluidized bed coater, while supplying the pure powder to the inside of the fluidized bed coater, the inlet air amount is 5 to 15 m 3 / sec, the inlet tube temperature is 80 to 150 ° C , A spraying pressure of 1.0 to 5.0 bar, and a spraying rate of 1 to 10 kg / hr, while spraying the mixed solution in a bottom spraying manner, thereby preparing pure bead particles having a particle size of 8 to 15 μm.
마지막 화장료제조단계는 상기 순지트비드와 잔량의 허브수 및 화장료 베이스를 혼합하여 화장료 조성물을 제조하는 것으로 구성된다.The final cosmetic preparation step consists of mixing the pure starch beads with the remaining amount of herb and the cosmetic base to prepare a cosmetic composition.
이하에서는 본 발명의 실시예에 대해 상세히 설명하기로 한다.Hereinafter, embodiments of the present invention will be described in detail.
아래 조성으로 이루어진 화장료 베이스 100 중량부를 준비하였다.100 parts by weight of a cosmetic base composed of the following composition was prepared.
더하여, 하이드롤라이즈드케라틴 3 중량부, 허브수 4 중량부, 러시아 카렐리아 지역에서 생산된 노멀순지트(플러렌 함량 60 중량%) 2 중량부를 계량하여 준비하였다.In addition, 3 parts by weight of hydrolyzed keratin, 4 parts by weight of herbs, and 2 parts by weight of normal tungsten (60% by weight of fullerene) produced in Karelia, Russia were weighed and prepared.
허브수는 시중에서 판매되는 페퍼민트 잎수를 구입하여 사용하였다.The number of herbs was purchased from commercially available peppermint leaf water.
상기 표 1의 원료 중 정제수를 평량하여 50 내지 55℃로 가열하고 가열한 원료에 하이드로제네이티드 레시틴, 글리세린과, 보습제 성분들인 Dipropylene glycol, Butyleneglycol, Pentyleneglycol, Glycereth-26을 혼합하여 혼합 용액을 만들고, 이어 나머지 원료를 순차적으로 투입 및 교반하여 화장료 베이스를 만들고, 그 다음에 전술한 본 발명의 주요 원료를 혼합하고, 마지막으로 중화제인 L-arginine를 넣어 점증시킨 후, 미량의 방부제를 첨가하여 모발용 화장수를 제조하였다.The purified water in Table 1 was weighed and heated to 50 to 55 占 폚. Hydrogenated lecithin and glycerin were mixed with Dipropylene glycol, Butyleneglycol, Pentyleneglycol and Glycereth-26, which are moisturizing components, to prepare a mixed solution. Then, the remaining raw materials are sequentially added and stirred to prepare a cosmetic base. Next, the main raw materials of the present invention are mixed, and finally L-arginine, a neutralizing agent, is added to the mixture to increase the amount. .
실시예 2는 실시예 1과 동일하게 제조하되, 허브수를 시중에서 구입하여 준비하지 않고 직접 페퍼민트 잎, 로즈마리 잎, 카모마일 꽃, 쟈스민 꽃을 동일 중량 준비한 후 각각을 물에 넣고 끓인 다음 고형물을 제거하여 페퍼민트 잎수, 로즈마리 잎수, 카모마일 꽃수, 쟈스민 꽃수를 제조하고 이들을 동일 중량으로 혼합하여 제조하여 모발용 화장수를 제조하였다.Example 2 was prepared in the same manner as in Example 1 except that peppermint leaves, rosemary leaves, chamomile flowers, and jasmine flowers were directly prepared in the same weight without preparing the herb water, and then boiled in water, Rosemary leaf water, chamomile flower, and jasmine flowering were prepared and mixed with the same weight to prepare a hair lotion.
실시예 3은 실시예 2와 동일하게 제조하되, 페퍼민트 잎수를 배제한 채 허브수를 제조하여 모발용 화장수를 제조하였다.Example 3 was prepared in the same manner as in Example 2 except that peppermint leaf water was excluded and herbal water was prepared to prepare a hair lotion.
실시예 4는 실시예 2와 동일하게 제조하되, 로즈마리 잎수를 배제한 채 허브수를 제조하여 모발용 화장수를 제조하였다.Example 4 was prepared in the same manner as in Example 2 except that rosemary leaf water was excluded and herbal water was prepared to produce hair lotion.
실시예 5는 실시예 2와 동일하게 제조하되, 카모마일 꽃수를 배제한 채 허브수를 제조하여 모발용 화장수를 제조하였다.Example 5 was prepared in the same manner as in Example 2 except that the herbal water was prepared with the exception of chamomile flower water to prepare a hair lotion.
실시예 6은 실시예 2와 동일하게 제조하되, 쟈스민 꽃수를 배제한 채 허브수를 제조하여 모발용 화장수를 제조하였다.Example 6 was prepared in the same manner as in Example 2 except that jasmine flower water was excluded, and herbal water was prepared to prepare hair cosmetic lotion.
실시예 7은 실시예 2와 동일하게 제조하되, 순지트 분말을 플러렌 함량 90 중량% 이상인 엘리트 순지트를 사용하여 모발용 화장수를 제조하였다.Example 7 was prepared in the same manner as in Example 2 except that Elite sunflower having a fullerene content of 90% by weight or more was used as a sunflower powder to produce a hair lotion.
실시예 8은 실시예 7과 동일하게 제조하되, 순지트 분말은 7㎛의 입자 크기를 갖도록 분쇄하여 모발용 화장수를 제조하였다.Example 8 was prepared in the same manner as in Example 7 except that the pure starch powder was pulverized to have a particle size of 7 mu m to prepare a hair lotion.
원료는 실시예 8과 동일하게 준비하되, 허브수 4 중량부 중 2 중량부를 먼저 하이드롤라이즈드케라틴과 혼합 교반하여 혼합액을 제조하고, 유동층 코팅기를 이용하여 순지트 분말에 상기 혼합액을 유동층 코팅시키되, 유동층 코팅기의 내부로 상기 순지트 분말을 공급하면서, 흡입공기량 5 ~ 15㎥/sec, 투입관 온도 80 ~ 150℃, 분무압력 1.0 ~ 5.0bar, 분무속도 1 ~ 10kg/hr의 유동층코팅 조건 하에서 바텀스프레이 방식으로 혼합액을 분무하면서 유동화를 실시하여 입자 크기 10㎛ 크기의 순지트비드를 제조한 다음 상기 순지트비드와 잔량의 허브수 및 화장료 베이스를 혼합하여 모발용 화장수를 제조하였다.The starting materials were prepared in the same manner as in Example 8 except that 2 parts by weight of 4 parts by weight of the herb were mixed and stirred with hydrolyzed keratin to prepare a mixed solution and the mixed solution was coated on the pure powder using a fluidized bed coater, , Under the fluidized bed coating conditions of an intake air amount of 5 to 15 m 3 / sec, a feed pipe temperature of 80 to 150 ° C., a spray pressure of 1.0 to 5.0 bar, and a spray rate of 1 to 10 kg / hr while supplying the pure powder into the fluidized bed coater The mixture was fluidized while spraying the mixture in a bottom spraying manner to prepare pure beaded beads having a particle size of 10 mu m. Then, the pure beaded beads, the remaining number of herbs and the cosmetic base were mixed to prepare hair cosmetic lotion.
실시예 10은 실시예 9와 동일하게 제조하되, 순지트 분말은 5㎛의 입자 크기를 갖도록 분쇄하여 모발용 화장수를 제조하였다.Example 10 was prepared in the same manner as in Example 9 except that the pure starch powder was pulverized to have a particle size of 5 탆 to prepare a hair lotion lotion.
<비교예의 모발용 화장수 제조><Preparation of hair lotion for comparison>
화장료 베이스를 실시예 1과 동일한 조성으로 준비하고, 하이드롤라이즈드케라틴, 허브수, 순지트 분말을 아래 표 2와 같은 중량부 단위로 준비한 후 혼합하여 비교예의 모발용 화장수를 제조하였다.The cosmetic base was prepared in the same composition as in Example 1, and the hydrolized keratin, the herb number and the pure starch powder were prepared in the parts by weight as shown in Table 2 below and mixed to prepare a hair lotion for comparison.
(단위:중량부)(Unit: parts by weight)
<실험예 1><Experimental Example 1>
본 발명의 조성물로 탈모증이 있는 대상자를 선정하여 테스트를 실시하였다.Subjects who had alopecia were selected and tested by the composition of the present invention.
피험자는 35-50세까지의 탈모증이 있는 성인남녀를 대상으로 1일 1회, 제공된 조성물 10㎖를 두피 및 모발에 충분히 도포하는 방법으로 3개월간 사용하여 그 결과를 관찰하였다. The subjects were used for 3 months by applying 10 ml of the composition provided on scalp and hair once a day to adult men and women having alopecia of 35-50 years old and observing the results.
이때, 한 그룹을 남성 5명, 여성 5명으로 하여 각 그룹으로 나눈 후, 그룹별로 실시예 및 비교예의 화장수를 제공하였다.At this time, one group was divided into 5 males and 5 females, and each group was provided with lotion lotages of Examples and Comparative Examples.
효과의 판정은 세발시 일일 평균 탈모량, 모발 굵기 개선, 모발 탄력 개선, 육안판정소견, 증상 개선 정도를 평가척도로써 5단계로 평가하고 종합적인 개선도를 상기 평가 척도의 평균으로 하였는데, 그 점수는 5점 만점으로 단계에 따라 1점 단위로 부여하였다.The evaluation of efficacy was as follows: average daily hair loss, hair thickness improvement, hair elasticity improvement, visual judgment findings, symptom improvement degree were evaluated in five stages as a evaluation scale, and the overall improvement degree was taken as an average of the above evaluation scales. Was given as a 5-point scale.
<1:악화, 2:불변, 3:조금 개선, 4:중간 개선, 5: 많이 개선><1: worse, 2: unchanged, 3: slight improvement, 4: moderate improvement, 5: much improvement>
상기 표 3에서 확인할 수 있는 바와 같이 본 발명의 실시예들을 사용한 그룹이 모발 굵기 개선, 모발 탄력 개선, 탈모 수, 육안, 자각 증상, 종합 개선의 모든 면에서 비교예 1 내지 6의 사용 그룹보다 현저힌 좋은 점수를 받아 우수한 탈모 개선 및 발모 효과를 보임을 확인할 수 있었다.As can be seen from the above Table 3, the groups using the examples of the present invention were significantly superior to those of Comparative Examples 1 to 6 in all aspects of hair thickness improvement, hair elasticity improvement, hair loss, visual acuity, subjective symptoms, It was confirmed that the hair loss was improved and the hair growth effect was improved.
<실험예 2><Experimental Example 2>
실시예 및 비교예의 화장수를 용기에 넣은 다음, 제조 직후의 색상, 냄새를 인지시킨 다음, 1달 간격으로 10개월 동안 5명의 피검자에게 내용물을 육안, 후각 을 이용하여 변질 여부를 확인하여 평균을 산출하였으며, 그 결과를 표 4 내지 6에 나타냈다.After putting the lotion of Examples and Comparative Examples into a container, the color and odor immediately after the preparation were recognized, and after 5 months at intervals of one month, the contents were visually checked by naked eye and smell to five subjects and the average was calculated And the results are shown in Tables 4 to 6.
<0: 색상 변화 없음, 1: 색상이 조금 변함,2: 색상이 많이 변함><0: no color change, 1: slightly changed color, 2: color changed a lot>
<0: 냄새 변화 없음, 1: 냄새가 조금 변함, 2: 냄새가 많이 변함><0: no change of odor, 1: odor slightly changed, 2: odor changed much>
상기한 표 4 및 표 5를 통해 보건데, 초기에는 색상 및 냄새가 실시예 및 비교예 모두 변화가 없는 것으로 나타났으나, 비교예들의 경우 대략 3,4개월차부터 냄새의 변화를 먼저 인지하게 된 것으로 나타난 반면 실시예들은 이러한 변화가 더 늦게 나타난 것을 알 수 있다.From the above Tables 4 and 5, it can be seen that color and odor did not change in both the Examples and Comparative Examples at the beginning, but in the Comparative Examples, the change in odor was first recognized from about 3,4 months While the embodiments show that this change is later.
또한, 실시예 중에서실시예 9, 10의 경우 10개월이 지나더라도 색상 및 냄새의 변화가 없는 것으로 나타나, 변질되기 쉬운 허브수를 사용했음에도 불구하고 오랫동안 사용할 수 있는 것을 알 수 있었다.Also, in Examples 9 and 10, no change in color and odor was observed even after 10 months in Examples, and it was found that even though the number of herbs easily deteriorated, they could be used for a long time.
화장료 베이스를 아래 표 6에 나타나 있는 조성의 트리트먼트용으로 구성하고, 실시예 1 내지 10 및 비교예 1 내지 6과 동일하게 실시예 11 내지 실시예 20 및 비교예 7 내지 12를 제조하였다.Examples 11 to 20 and Comparative Examples 7 to 12 were prepared in the same manner as in Examples 1 to 10 and Comparative Examples 1 to 6, except that the cosmetic base was constituted for the treatment of the composition shown in Table 6 below.
<실험예 3><Experimental Example 3>
실험예 1과 동일한 방법으로 모발의 굵기 개선, 탄력 개선, 탈모 수, 육안, 자각 증상, 종합 개선에 대한 실험을 실시하여 그 결과를 아래 표 7에 타나냈다.Experiments were carried out on the improvement of the thickness of the hair, the improvement of the elasticity, the number of the hair loss, the visual acuity, the subjective symptoms and the comprehensive improvement in the same manner as in Experimental Example 1, and the results are shown in Table 7 below.
<1:악화, 2:불변, 3:조금 개선, 4:중간 개선, 5: 많이 개선>상기 표 3에서 확인할 수 있는 바와 같이 본 발명의 실시예들을 사용한 그룹이 모발 굵기 개선, 모발 탄력 개선, 탈모 수, 육안, 자각 증상, 종합 개선의 모든 면에서 비교예의 사용 그룹보다 현저힌 좋은 점수를 받아 우수한 탈모 개선 및 발모 효과를 보임을 확인할 수 있었다.As can be seen from Table 3, the group using the examples of the present invention can improve the thickness of the hair, improve the elasticity of the hair, improve the elasticity of the hair, Hair loss, visual acuity, subjective symptom, and overall improvement were superior to those of the control group, and it was confirmed that the hair loss was improved and hair growth was improved.
<실험예 4><Experimental Example 4>
실시예 및 비교예의 화장수(트리트먼트)를 용기에 넣은 다음, 제조 직후의 색상, 냄새를 인지시킨 다음, 1달 간격으로 10개월 동안 5명의 피검자에게 내용물을 육안, 후각 을 이용하여 변질 여부를 확인하여 평균을 산출하였으며, 그 결과를 표 4 내지 6에 나타냈다.After putting the cosmetic lotions (treatment) of the examples and the comparative examples into a container, the color and odor immediately after the preparation were recognized, and the contents were visually inspected by five eyes of the subject for 10 months at intervals of one month , And the results are shown in Tables 4 to 6. < tb > < TABLE >
<0: 색상 변화 없음, 1: 색상이 조금 변함,2: 색상이 많이 변함><0: no color change, 1: slightly changed color, 2: color changed a lot>
<0: 냄새 변화 없음, 1: 냄새가 조금 변함, 2: 냄새가 많이 변함><0: no change of odor, 1: odor slightly changed, 2: odor changed much>
상기한 표 8 및 표 9를 통해 보건데, 초기에는 색상 및 냄새가 실시예 및 비교예 모두 변화가 없는 것으로 나타났으나, 비교예들의 경우 대략 3개월차부터 냄새의 변화를 먼저 인지하게 된 것으로 나타난 반면 실시예들은 이러한 변화가 더 늦게 나타난 것을 알 수 있다.From the above Table 8 and Table 9, it can be seen that color and odor were not changed in the early days, but in the comparative examples, the change in smell was recognized first from about three months The embodiments can be seen that this change is later.
또한, 실시예 중에서 실시예 19, 20의 경우 10개월이 지나더라도 색상 및 냄새의 변화가 없는 것으로 나타나, 변질되기 쉬운 허브수를 사용했음에도 불구하고 오랫동안 사용할 수 있는 것을 알 수 있었다.Also, in Examples 19 and 20, no change in color and odor was observed even after 10 months in Examples, and it was found that even though the number of susceptible herbs was used, they could be used for a long time.
Claims (5)
화장료 베이스 100 중량부를 준비하는 베이스준비단계와;
러시아 북부 카멜리아 지역의 슝가에서 생산되고, 플러렌 함량이 90 중량% 이상인 순지트 광물을 준비한 후, 7㎛의 입자 크기를 갖도록 분쇄하여 순지트 분말 2 중량부를 제조하는 분쇄단계와;
페퍼민트 잎, 로즈마리 잎, 카모마일 꽃, 쟈스민 꽃을 동일 중량 준비한 후 각각을 물에 넣고 끓인 다음 고형물을 제거하여 페퍼민트 잎수, 로즈마리 잎수, 카모마일 꽃수, 쟈스민 꽃수를 제조하고 이들을 동일 중량으로 혼합하여 허브수 4 중량부를 제조하는 허브수준비단계와;
하이드롤라이즈드케라틴 3 중량부를 준비한 후, 준비된 허브수 중 2 중량부와 혼합 교반하여 혼합액을 제조하는 혼합액제조단계와;
유동층 코팅기를 이용하여 상기 순지트 분말에 상기 혼합액을 유동층 코팅시키되, 유동층 코팅기의 내부로 상기 순지트 분말을 공급하면서, 흡입공기량 5 ~ 15㎥/sec, 투입관 온도 80 ~ 150℃, 분무압력 1.0 ~ 5.0bar, 분무속도 1 ~ 10kg/hr의 유동층코팅 조건 하에서 바텀스프레이 방식으로 혼합액을 분무하면서 유동화를 실시하여 입자 크기 10㎛ 크기의 순지트비드를 제조하는 유동층코팅단계와;
상기 순지트비드와 잔량의 허브수 및 화장료 베이스를 혼합하여 화장료 조성물을 제조하는 화장료제조단계;를 포함하여 구성된,
순지트를 이용한 탈모 방지 및 발모 촉진용 화장료 조성물 제조 방법.A method for producing a cosmetic composition for hair loss prevention and promotion of hair growth,
A base preparation step of preparing 100 parts by weight of a cosmetic base;
A crushing step of preparing a pure zeitgeite which is produced in Schungkah in the northern Camellia region of Russia and has a fullerene content of 90% by weight or more and then pulverized to have a particle size of 7 탆 to prepare 2 parts by weight of a pure zeitite powder;
Peppermint leaves, rosemary leaves, chamomile flowers, and jasmine flowers were prepared in equal weight, and then boiled in water. Then, the solids were removed to prepare peppermint leaf water, rosemary leaf water, chamomile flower water and jasmine flower water. A number of hubs for preparing a weight part;
3 parts by weight of hydrolyzed keratin were prepared and mixed with 2 parts by weight of the prepared herb water to prepare a mixture solution;
The mixture liquid was coated on the pure powder by using a fluidized bed coater, while the pure powder was supplied into the fluidized bed coater, the inlet air amount was 5 to 15 m 3 / sec, the inlet tube temperature was 80 to 150 ° C, the spray pressure was 1.0 A fluidized bed coating step of spraying a mixed solution in a bottom spraying method under fluidized bed coating conditions of 1 to 10 kg /
Preparing a cosmetic composition by mixing the purified tooth beads with the remaining number of herbs and a cosmetic base;
A method for preparing a cosmetic composition for preventing hair loss and promoting hair growth using sunflower.
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| KR101859421B1 (en) | 2017-01-31 | 2018-05-21 | 주식회사 케라메딕스 | Injectable composition for prevention of depilation or improvement of hair growth |
| JP2018172362A (en) * | 2017-03-30 | 2018-11-08 | ビタミンＣ６０バイオリサーチ株式会社 | Fullerene-containing cosmetic composition |
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| JP4399341B2 (en) * | 2004-10-29 | 2010-01-13 | 一丸ファルコス株式会社 | Hair treatment agent |
| KR20110037777A (en) * | 2009-10-07 | 2011-04-13 | 주식회사 케이티앤지 | Bath preparation method using red ginseng |
| KR20130067004A (en) * | 2011-12-13 | 2013-06-21 | (주)케이피티 | The granules comprising charcoal and process for preparing the same |
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