KR20170077658A - soft nano mask pack using complex nano fiber sheet and the method for preparing thereof - Google Patents
soft nano mask pack using complex nano fiber sheet and the method for preparing thereof Download PDFInfo
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- 238000000034 method Methods 0.000 title claims description 7
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- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/22—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed
- B32B5/24—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer
- B32B5/26—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer another layer next to it also being fibrous or filamentary
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- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D44/00—Other cosmetic or toiletry articles, e.g. for hairdressers' rooms
- A45D44/002—Masks for cosmetic treatment of the face
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
- B32B5/022—Non-woven fabric
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
- B32B7/04—Interconnection of layers
- B32B7/12—Interconnection of layers using interposed adhesives or interposed materials with bonding properties
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
- D04H1/498—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres entanglement of layered webs
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/70—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
- D04H1/72—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged
- D04H1/728—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged by electro-spinning
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Mechanical Engineering (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Cosmetics (AREA)
Abstract
본 발명은 복합 나노섬유를 이용한 소프트 나노섬유 마스크 시트 및 이의 제조방법 에 관한 것으로, 부직포 시트층; 접착층 ; 및 나노 마스크 시트층이 순사적으로 적층되는 다층구조의 소프트 나노 마스크 시트를 제공한다.
또한 본 발명에 따른 부직포시트는 두께가 0.01~1mm로 형성되고, 접착층은 1~100um의 두께를 가지며, 나노 마스크 시트층의 두께는 10 ~ 200um를 형성하는 것을 특징으로 한다.
본 발명에 따른 소프트 나노 마스크 시트는 피부 밀착성이 우수하고, 가벼운 사용감을 가지고 있으며, 유효물질을 피부에 전달할수 있는 획기적인 스킨케어용 마스크 시트로 미용액 적용시 피부에 항산화, 미백, 항노화, 항염증, 주름개선, 피부탄력, 여드름 피부 개선, 아토피 피부 개선 등의 유효성분을 효과적으로 전달할 수 있는 장점이 있다.The present invention relates to a soft nano fiber mask sheet using composite nanofibers and a method of manufacturing the same, Adhesive layer; And a nanomask sheet layer are sequentially laminated on the surface of the soft nano mask sheet.
The nonwoven fabric sheet according to the present invention is formed to have a thickness of 0.01 to 1 mm, the adhesive layer has a thickness of 1 to 100 μm, and the nanomask sheet layer has a thickness of 10 to 200 μm.
The soft nano mask sheet according to the present invention is an epoch-making mask sheet for skin care which has excellent skin adhesion, light feeling, and can transmit an effective substance to the skin. It is a mask sheet for antioxidant, whitening, anti- , Wrinkle improvement, skin elasticity, acne skin improvement, atopic skin improvement, and the like.
Description
본 발명은 복합 나노섬유를 이용한 소프트 나노섬유 마스크 시트 및 이위 제조방법 에 관한 것이다. The present invention relates to a soft nano fiber mask sheet and a manufacturing method using the composite nano fiber.
일반적으로 현재 화장용 마스크 팩은 부직포에 기능성이 있다고 알려진 추출물 등을 첨가한 물이나 화장수에 침지시키는 에센스 마스크 팩이나 하이드로겔 형태의 마스크팩이 주를 이루고 있다. 그러나 마스크팩의 부직포시트는 합성 고분자로 제조되는데, 화장수나 기능성 추출물을 첨가하면 뻣뻣하게 되어 사용감이 좋지 않다. 또한 부직포를 화장액 등의 첨가제에 침지시켜 미용액의 흡수를 유도한 타입의 경우에는 피부에 대한 부착성이 낮으며, 미용액이 공기에 노출됨으로 인해 야기되는 미용성분들의 변성을 피하기 어렵고, 초기에 너무 고농도의 미용성분이 피부와 접촉함으로 인한 피부 자극 발생의 소지가 높다는 단점이 있고, 하이드로겔 형태의 마스크팩도 피부에 대한 밀착력이 낮고, 유효성분이 피부에 전달되어 침투되는 데에 상대적으로 장시간이 요구되고, 제조단가가 고가를 이루고 있다는 단점이 있다.
Generally, currently, the cosmetic mask pack mainly consists of an essence mask pack or a hydrogel-type mask pack which is immersed in water or a lotion added with an extract or the like known to have a functional property to a nonwoven fabric. However, the nonwoven fabric sheet of the mask pack is made of a synthetic polymer. When the cosmetic lotion or functional extract is added, it becomes stiff and the feeling of use is poor. In the case of a type in which the nonwoven fabric is immersed in an additive such as a cosmetic liquid to induce absorption of the serum, adhesion to the skin is low and it is difficult to avoid denaturation of the cosmetic ingredients caused by exposure of the serum to the air, There is a disadvantage in that a high concentration of cosmetic ingredients is liable to cause skin irritation due to contact with the skin. Also, since the hydrogel type mask pack has low adhesion to the skin and the effective ingredient is transmitted to the skin and penetrates, And the manufacturing cost is high.
이러한 마스크 팩들의 단점을 극복하기 위하여 전기방사 마스크팩에 대한 연구 개발이 활발히 이루어져 왔다. 전기 방사법은 다양한 용매를 통해 고분자와 혼합이 가능한 모든 재료를 사용하여 나노섬유를 제조할 수 있어 재료에 대한 제한이 없다. 그리고 나노섬유의 크기나 직경, 형상의 조절이 용이하여 재료 코팅, 필터, 약물전달 시스템, 나노/바이오 센서 등 많은 산업분야에 걸쳐 다양한 응용 가능성을 보여주고 있다. 피부미용분야에서의 전기방사 부직포는 일반 합성고분자 부직포 시트와 하이드로겔의 공통된 단점인 피부밀착력을 개선할 뿐만 아니라 사용감, 유효성분 전달 등을 개선시킬 수 있는 제품으로 말할 수 있다. In order to overcome the disadvantages of such mask packs, research and development of an electrospinning mask pack have been actively conducted. Electrospinning can produce nanofibers using any material that can be mixed with polymers through a variety of solvents, so there is no limit to materials. The size, diameter, and shape of nanofibers can be easily controlled to show various application possibilities in many industrial fields such as material coating, filter, drug delivery system, nano / biosensor. The nonwoven fabric in the field of skin care can be said to be a product which not only improves the skin adhesion force which is a common disadvantage of the general synthetic polymer nonwoven fabric sheet and the hydrogel, but also improves feeling of use and effective ingredient delivery.
본 발명에서는 전기방사법을 이용하여 복합 나노섬유 부직포를 제조하여 마스크팩의 피부 부착면에만 나노섬유화 함으로써 유효성분을 획기적으로 전달할 수 있고, 피부 부착성 증가, 제품의 경량화로써 사용감이 편리한 장점, 기존 제품의 제품들의 단점을 개선시킬 수 있는 독창적이고 독보적인 기술로 화장품 및 의약외품분야에서 차별화 될 수 있는 복합 나노섬유를 이용한 소프트 나노섬유 마스크 시트 및 이위 제조방법을 제공하는 것이다.In the present invention, the composite nanofiber nonwoven fabric is manufactured by using the electrospinning method, and the nanofiber is formed only on the skin-adhered surface of the mask pack. Thus, the effective ingredient can be transmitted remarkably, the skin adhesion is increased, The present invention is to provide a soft nano fiber mask sheet and a manufacturing method using the composite nanofibers that can be differentiated in the fields of cosmetics and quasi-drugs.
본 발명의 목적은 복합 나노섬유를 이용한 소프트 나노섬유 마스크 시트를 개발하기 위하여 부직포층과 복합나노섬유층의 제조시 박리되는 단점을 개선하기위해 많은 선행연구들이 이루어졌고, 이를 개선하기 위해 열처리를 통해 박리현상을 개선하였지만 전기방사 소프트 레이어의 표면이 열에 의해 녹아내려 표면이 매끄럽지 않는 점을 개선하기위해 천연고분자 및 생체고분자를 이용한 접착층을 구성하여 본 발명을 완성할 수 있으며 매끄러운 표면의 복합 나노섬유 마스크팩 시트를 제조하는 것이다.The object of the present invention is to develop a soft nano fiber mask sheet using composite nanofibers. In order to improve the disadvantages of peeling off the non-woven fabric layer and the composite nano fiber layer, many prior studies have been conducted. The present invention can be completed by constructing an adhesive layer using a natural polymer and a biomolecule in order to solve the problem that the surface of the electrospun soft layer is melted by heat and the surface is not smooth, To produce a sheet.
상기 목적을 달성하기 위하여 본 발명은 다음과 같은 수단을 제공한다.In order to achieve the above object, the present invention provides the following means.
본 발명은 복합 나노섬유를 이용한 소프트 나노섬유 마스크 시트 및 이의 제조방법에 관한 것으로 더욱 상세하게는 부직포 시트층; 접착층 ; 및 나노 마스크 시트층이 순사적으로 적층되는 다층구조의 소프트 나노 마스크 시트를 제공한다. The present invention relates to a soft nano fiber mask sheet using composite nanofibers and a method for manufacturing the same, and more particularly, Adhesive layer; And a nanomask sheet layer are sequentially laminated on the surface of the soft nano mask sheet.
또한 본 발명에 따른 부직포시트는 두께가 0.01~1mm로 형성되고, 접착층은 1~100um의 두께를 가지며, 나노 마스크 시트층의 두께는 10 ~ 200um를 형성하는 것을 특징으로 한다. 마스크팩으로 사용할 수 있는 부직포 시트 즉 면, 폴리비닐알코올, 모달, 라이오셀, 레이온, 실크, 바이오셀룰로오스, 셀룰로오스 유도사, 초극세사 시트위에 나노섬유를 형성할 수 있는 나노섬유 천연고분자, 접착 천연고분자로 구성하여 복합 나노섬유 시트를 형성하고 피부미용 에센스에 함침하여 피부 밀착력과 유효성분의 전달을 획기적으로 부여할 수 있는 피부 미용 마스크팩을 제공하고자 한다.The nonwoven fabric sheet according to the present invention is formed to have a thickness of 0.01 to 1 mm, the adhesive layer has a thickness of 1 to 100 μm, and the nanomask sheet layer has a thickness of 10 to 200 μm. Non-woven sheets that can be used as mask packs include cotton, polyvinyl alcohol, modal, lyocell, rayon, silk, bio-cellulose, cellulose inductors, nanofiber natural polymers capable of forming nanofibers on a sheet of micro- To form a composite nanofiber sheet and impregnate the skin with cosmetic essence to provide a skin care mask pack capable of dramatically imparting skin adhesion force and effective ingredient delivery.
본 발명에 따른 천연고분자 접착 스프레이와 천연고분자 전기방사용액을 이용한 소프트 나노 마스크 시트은 피부에 항산화, 미백, 항노화, 항염증, 주름개선, 피부탄력, 여드름 피부 개선 및 아토피 피부 개선 등의 유효성분을 효과적으로 전달할 수 있는 장점이 있으며, 천연고분자를 이용한 접착스프레이를 제조함으로 인해 종래의 전기방사 마스크팩시트 타입에 비해 부드럽고 매끄러운 표면을 가져 피부에 밀착성이 우수하며, 유효기능성물질 전달 능력도 높은 장점이 있다.
The soft nano mask sheet using the natural polymer adhesive spray and the natural polymer electric spinning solution according to the present invention can be used as an effective ingredient for skin such as antioxidant, whitening, anti-aging, anti-inflammation, wrinkle, skin elasticity, acne skin improvement, The present invention provides an adhesive spray using a natural polymer, which has a smooth and smooth surface compared to a conventional electrospinning mask pack sheet type, and thus has excellent skin adhesion and high effective functional substance delivery capability .
도 1은 실시예 1에서 제조한 소프트 나노 마스크 시트의 전자현미경 사진.
도 2는 본 발명의 소트프 나노 마스크 시트의 모식도
부호의 설명
10 : 부직포 시트
20 : 접착층
30 : 나노 마스크 시트1 is an electron micrograph of the soft nano-mask sheet prepared in Example 1. Fig.
Fig. 2 is a schematic view of the soot nano mask sheet of the present invention
Explanation of symbols
10: Nonwoven sheet
20: Adhesive layer
30: Nano mask sheet
이하, 본 발명의 바람직한 실시예와 각 성분의 물성을 상세하게 설명하되, 이는 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자가 발명을 용이하게 실시할 수 있을 정도로 상세하게 설명하기 위한 것이지, 이로 인해 본 발명의 기술적인 사상이나 범주가 한정되는 것을 의미하지는 않는다.
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS The present invention will now be described more fully hereinafter with reference to the accompanying drawings, in which exemplary embodiments of the invention are shown. And does not mean that the technical idea or category of the present invention is limited.
본 발명에 따른 부직포 시트(10)는 두께가 0.01~1mm로 형성되고, 접착층은 1~100um의 두께를 가지며, 나노 마스크 시트층(30)의 두께는 10 ~ 200um를 형성하는 것을 특징으로 한다.The nonwoven fabric sheet 10 according to the present invention is formed to have a thickness of 0.01 to 1 mm, the adhesive layer has a thickness of 1 to 100 μm, and the nanomask sheet layer 30 has a thickness of 10 to 200 μm.
부직포 시트(10)와 나노 마스크 시트(30)의 접착 천연고분자(20)는 0.1중량%내지 10중량%, 정제수 90중량%내지 99.9중량%을 0~80도 조건에서 1시간내지 24시간 교반, 용해시켜서 제조된 접착 천연고분자 용액 제조한 후 스프레이방식으로 부직포 시트위에 접착제를 균일하게 도포하는 단계(단계 1);The adhesive natural polymer 20 of the nonwoven fabric sheet 10 and the nanomask sheet 30 is mixed with 0.1 wt% to 10 wt% and purified water 90 wt% to 99.9 wt% at 0 to 80 ° C for 1 to 24 hours, (Step 1) of uniformly applying the adhesive onto the nonwoven fabric sheet by a spraying method after preparing the adhesive natural polymer solution prepared by dissolving the adhesive natural polymer solution;
나노 마스크 시트(30) 제조시 나노섬유 천연고분자는 1중량% 내지 15중량%, 정제수 85중량% 내지 99중량%을 0~80도 조건에서 1시간내지 24시간 교반, 용해시켜서 제조된 나노섬유 천연고분자 용액 제조(단계 2)한 후 부직포 시트 위에 전기방사기를 이용하여 전기용량 0 ~ 40kV, 8~13cm TCD(Tip와 Controller간의 거리), 20~40도에서 전기방사 하여 소프트 나노섬유 시트 제조단계(단계 3);를 The nanofiber natural polymer prepared by the method of manufacturing the nanomask sheet 30 is prepared by dissolving 1 to 15 wt% of purified natural water and 85 to 99 wt% of purified water at 0 to 80 ° C for 1 to 24 hours, After preparing the polymer solution (Step 2), the non-woven fabric sheet was electrospun by using an electrospinning device and electrospun with a capacity of 0 to 40 kV, 8 to 13 cm TCD (distance between tip and controller) and 20 to 40 degrees, Step 3);
피부 미용에 효과적인 미용액은 스킨, 미스트, 에센스, 앰플, 로션을 10~30g을 충진하여 소프트 나노 마스크 시트에 함침하여 스킨케어용 소트프 마스크 시트(단계 4) 제조방법
Beauty essence, which is effective for skin beauty, is filled with 10 ~ 30g of skin, mist, essence, ampoule and lotion, and impregnated with soft nano mask sheet to produce soft mask sheet for skin care (step 4)
상기 접착 천연고분자(20)는 키토산, 알기네이트, 카라기난, 로커스트빈검, 전분, 한천, 만난, 잔탄검, 플루란, 폴리비닐알코올 등으로 구성된 군으로부터 선택된 어느 하나 이상을 사용하며, 나노 마스크(30) 천연고분자 전기방사 용액은 키토산, 알기네이트, 플루란, 폴리비닐알코올 등으로 구성된 군으로부터 선택된 어느 하나 이상을 사용하며, 상기 부직포 시트(10)는 면, 폴리비닐알코올, 모달, 라이오셀, 레이온, 실크, 바이오셀룰로오스, 셀룰로오스 유도사, 초극세사 시트 구성된 군으로부터 선택된 어느 하나 를 사용하는 것을 특징으로 한다.
The adhesive natural polymer 20 may be at least one selected from the group consisting of chitosan, alginate, carrageenan, locust bean gum, starch, agar, mannan, xanthan gum, pullulan, polyvinyl alcohol, The natural polymer electrospinning solution may be one or more selected from the group consisting of chitosan, alginate, pullulan, polyvinyl alcohol and the like. The nonwoven fabric sheet 10 may be made of cotton, polyvinyl alcohol, modal, , Silk, bio-cellulose, cellulose derivative yarn, and microfiber sheet.
이하, 실시 예를 통하여 본 발명의 구성 및 효과를 더욱 상세히 설명하고자 한다. 이들 실시 예는 오로지 본 발명을 예시하기 위한 것일 뿐 본 발명의 범위가 이들 실시 예에 의해 제한되는 것은 아니다.
Hereinafter, the constitution and effects of the present invention will be described in more detail through examples. These embodiments are only for illustrating the present invention, and the scope of the present invention is not limited by these embodiments.
실시예 1Example 1
1 용기에 키토산 20g, 락틱엑시드 15g과 정제수 965g 을 투입하고 25에서 3~4시간 동안 교반하여 천연고분자를 이용한 접착 천연고분자 조성물(30)을 만들었다.20 g of chitosan, 15 g of lactic acid, and 965 g of purified water were added to 1 container and stirred at 25 for 3 to 4 hours to prepare an adhesive natural polymer composition (30) using a natural polymer.
상기 천연고분자를 이용한 접착 천연고분자 조성물을 일반마스크시트에 분사 한 후, 전기방사기를 사용하여 복합 나노섬유 마스크팩 시트(20)를 제조하였다.After the adhesive natural polymer composition using the natural polymer was sprayed onto a general mask sheet, a composite nanofiber mask pack sheet 20 was prepared by using an electrospinning machine.
또한, 1 용기에 폴리비닐알코올 90g과 정제수 910g을 투입하고 75에서 5~8시간 동안 교반하여 나노섬유 천연고분자 조성물을 만들었고, 부직포 시트(10) 위에 전기방사기를 이용하여 전기용량 2kV, 10cm TCD(Tip와 Controller간의 거리), 25도에서 소프트 나노 마스크 시트를 제조하였다. 90 g of polyvinyl alcohol and 910 g of purified water were added to 1 container and stirred at 75 for 5 to 8 hours to prepare a nanofiber natural polymer composition. The nonwoven fabric sheet (10) The distance between Tip and Controller), at 25 degrees, a soft nano mask sheet was manufactured.
상기와 같이 제조된 소프트 나노 마스크 시트를 피부 미용에 효과적인 미용액은 에센스 20g을 충진하여 소트프 나노 마스크 팩 제조를 완성하였다.
The soft nanomask sheet prepared as described above was filled with 20 g of essence, which is effective for skin care, to complete the preparation of the Sotphon nanoscale mask pack.
[실험예 1][Experimental Example 1]
실시예 1에서 제조한 소프트 나노 마스크팩 시트를 전자현미경으로 측정하여 도 2에 나타내었다.
The soft nano mask pack sheet prepared in Example 1 was measured with an electron microscope and is shown in Fig.
[실험예 2][Experimental Example 2]
실시예 1에서 제조한 소프트 나노 마스크팩 시트를 에센스 20g을 충진한 후 피부 자극도를 알아보기 위하여, 얼굴에 30분간 적용후 피부 반응을 관찰하였다. 피시험자는 20 ~ 40대 성인남녀 40명을 대상으로 하였다. 시험결과는 국제 국제 접촉피부염 연구위원회 (International Contact Dermatitis Research Group)의 기준을 적용하여 평가하였으며 이의 평균값을 계산하였다. 이의 결과를 하기 표 1에 나타내었다.After filling the soft nano mask pack sheet prepared in Example 1 with 20 g of essence, skin reaction was observed after application to the face for 30 minutes in order to examine the degree of skin irritation. The subjects were 40 men and women in their 20s and 40s. The test results were evaluated by applying the criteria of the International Contact Dermatitis Research Group and their average values were calculated. The results are shown in Table 1 below.
(- : 반응없음)(- : no response)
표 1에 나타낸 바와 같이, 본 발명의 소프트 나노 마스크 시트를 적용한 성인 남녀 각 20명은 모두 발적, 홍반 및 가려움 등의 피부 트러블이 전혀 일어나지 않아, 본 발명의 소프트 나노 마스크 시트의 피부 안전성이 검증되었다.
As shown in Table 1, all 20 adult men and women who applied the soft nano mask sheet of the present invention did not cause any skin troubles such as redness, redness and itching, and skin safety of the soft nano mask sheet of the present invention was verified.
Claims (5)
상기 부직포 시트층은 두께가 0.01~1mm인 것을 특징으로 하는 소프트 나노 마스크 시트The method according to claim 1,
The nonwoven fabric sheet layer has a thickness of 0.01 to 1 mm.
상기 접착층은 두께가 1 ~ 100um의 두께를 가진 것을 특징으로 하는 소프트 나노 마스크 시트The method according to claim 1,
Characterized in that the adhesive layer has a thickness of 1 to 100 < RTI ID = 0.0 > um. ≪
상기 나노 마스크 시트층의 두께는 10 ~ 200um인 것을 특징으로 하는 소프트 나노 마스크 시트The method according to claim 1,
Characterized in that the thickness of the nanomask sheet layer is 10-200 < RTI ID = 0.0 > um. ≪
부직포 시트(10)와 나노섬유 시트(20)의 접착 천연고분자(30)는 0.1중량%내지 10중량%, 정제수 90중량%내지 99.9중량%을 0~80도 조건에서 1시간내지 24시간 교반, 용해시켜서 제조된 접착 천연고분자 용액 제조한 후 스프레이방식으로 부직포 시트위에 접착제를 균일하게 도포하는 단계(단계 1);
나노섬유 시트(20) 제조시 나노섬유 천연고분자는 1중량% 내지 15중량%, 정제수 85중량% 내지 99중량%을 0~80도 조건에서 1시간내지 24시간 교반, 용해시켜서 제조된 나노섬유 천연고분자 용액 제조(단계 2)한 후 부직포 시트 위에 전기방사기를 이용하여 전기용량 0 ~ 40kV, 8~13cm TCD(Tip와 Controller간의 거리), 20~40도에서 전기방사 하여 소프트 나노섬유 시트 제조단계(단계 3);를
피부 미용에 효과적인 미용액은 스킨, 미스트, 에센스, 앰플, 로션을 10~30g을 충진하여 소프트 나노 마스크 시트에 함침하여 스킨케어용 소트프 마스크 시트(단계 4) 제조하는 것을 특징으로 하는 소프트 나노 마스크 시트의 제조방법
The method according to claim 1,
The adhesive natural polymer 30 between the nonwoven fabric sheet 10 and the nanofiber sheet 20 is mixed with 0.1 to 10 wt% and purified water 90 to 99.9 wt% at 0 to 80 ° C for 1 to 24 hours, (Step 1) of uniformly applying the adhesive onto the nonwoven fabric sheet by a spraying method after preparing the adhesive natural polymer solution prepared by dissolving the adhesive natural polymer solution;
In producing the nanofiber sheet 20, the nanofiber natural polymer is prepared by dissolving 1 to 15% by weight of purified natural water and 85 to 99% by weight of purified water in 0 to 80 ° C for 1 to 24 hours, After preparing the polymer solution (Step 2), the non-woven fabric sheet was electrospun by using an electrospinning device and electrospun with a capacity of 0 to 40 kV, 8 to 13 cm TCD (distance between tip and controller) and 20 to 40 degrees, Step 3);
A soft nano mask sheet (Step 4) for skin care is prepared by impregnating soft nano mask sheet with 10 to 30 g of skin, mist, essence, ampoule and lotion, ≪ / RTI &
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20180085682A (en) * | 2017-01-19 | 2018-07-27 | 최성현 | A pad for treating and alleviating the skin diseases associated with the exudation of plasma protein comprising atopic disease |
| CN109853130A (en) * | 2018-12-21 | 2019-06-07 | 北京工商大学 | A kind of ultra-thin and ultra-dry nanofiber membrane paper and preparation method thereof |
| KR20200013554A (en) * | 2018-07-30 | 2020-02-07 | 한국섬유개발연구원 | The wet-laid non-woven fabric for facial mask pack including pulp extracted from Rhodophyta and manufacturing method thereof |
| WO2020067798A1 (en) * | 2018-09-27 | 2020-04-02 | 주식회사 엘지화학 | Bio-cellulose sheet and preparation method thereof |
| CN111411403A (en) * | 2020-03-04 | 2020-07-14 | 扬州大学 | Electrospinning preparation device for nanofiber filter and working method thereof |
| CN112513356A (en) * | 2018-09-27 | 2021-03-16 | 株式会社Lg化学 | Biological cellulose tablet and preparation method thereof |
| CN113265762A (en) * | 2020-08-07 | 2021-08-17 | 李潮云 | Biomedical non-woven fabric based on nano fibers |
-
2015
- 2015-12-28 KR KR1020150187783A patent/KR20170077658A/en not_active Withdrawn
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20180085682A (en) * | 2017-01-19 | 2018-07-27 | 최성현 | A pad for treating and alleviating the skin diseases associated with the exudation of plasma protein comprising atopic disease |
| KR20200013554A (en) * | 2018-07-30 | 2020-02-07 | 한국섬유개발연구원 | The wet-laid non-woven fabric for facial mask pack including pulp extracted from Rhodophyta and manufacturing method thereof |
| WO2020067798A1 (en) * | 2018-09-27 | 2020-04-02 | 주식회사 엘지화학 | Bio-cellulose sheet and preparation method thereof |
| CN112513356A (en) * | 2018-09-27 | 2021-03-16 | 株式会社Lg化学 | Biological cellulose tablet and preparation method thereof |
| CN109853130A (en) * | 2018-12-21 | 2019-06-07 | 北京工商大学 | A kind of ultra-thin and ultra-dry nanofiber membrane paper and preparation method thereof |
| CN111411403A (en) * | 2020-03-04 | 2020-07-14 | 扬州大学 | Electrospinning preparation device for nanofiber filter and working method thereof |
| CN113265762A (en) * | 2020-08-07 | 2021-08-17 | 李潮云 | Biomedical non-woven fabric based on nano fibers |
| CN113265762B (en) * | 2020-08-07 | 2023-04-14 | 苏州鱼得水电气科技有限公司 | Biomedical non-woven fabric based on nano fibers |
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| PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 20151228 |
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| PG1501 | Laying open of application | ||
| PC1203 | Withdrawal of no request for examination |