KR960010595A - 1-헥센의 제조방법 - Google Patents

1-헥센의 제조방법 Download PDF

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KR960010595A
KR960010595A KR1019950028634A KR19950028634A KR960010595A KR 960010595 A KR960010595 A KR 960010595A KR 1019950028634 A KR1019950028634 A KR 1019950028634A KR 19950028634 A KR19950028634 A KR 19950028634A KR 960010595 A KR960010595 A KR 960010595A
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hexene
atom
general formula
compound represented
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KR100339290B1 (ko
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미쓰히사 다무라
겐시 우찌다
기요시 이와나기
요시아끼 이또
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고오사이 아끼오
스미또모가가꾸고오교 가부시끼가이샤
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
    • C07C2/02—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons
    • C07C2/04—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons by oligomerisation of well-defined unsaturated hydrocarbons without ring formation
    • C07C2/06—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons by oligomerisation of well-defined unsaturated hydrocarbons without ring formation of alkenes, i.e. acyclic hydrocarbons having only one carbon-to-carbon double bond
    • C07C2/08—Catalytic processes
    • C07C2/26—Catalytic processes with hydrides or organic compounds
    • C07C2/30—Catalytic processes with hydrides or organic compounds containing metal-to-carbon bond; Metal hydrides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C07C11/107—Alkenes with six carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
    • C07C2/02—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons
    • C07C2/04—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons by oligomerisation of well-defined unsaturated hydrocarbons without ring formation
    • C07C2/06—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons by oligomerisation of well-defined unsaturated hydrocarbons without ring formation of alkenes, i.e. acyclic hydrocarbons having only one carbon-to-carbon double bond
    • C07C2/08—Catalytic processes
    • C07C2/26—Catalytic processes with hydrides or organic compounds
    • C07C2/36—Catalytic processes with hydrides or organic compounds as phosphines, arsines, stilbines or bismuthines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2527/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • C07C2527/06—Halogens; Compounds thereof
    • C07C2527/125—Compounds comprising a halogen and scandium, yttrium, aluminium, gallium, indium or thallium
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2531/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • C07C2531/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2531/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • C07C2531/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • C07C2531/22—Organic complexes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2531/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • C07C2531/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • C07C2531/24—Phosphines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2531/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • C07C2531/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups C07C2531/02 - C07C2531/24
    • C07C2531/34—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups C07C2531/02 - C07C2531/24 of chromium, molybdenum or tungsten

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

1-헥센용액 중에서 하기성분(A),(B),(C)및 (D)를 접촉시켜서 얻어지는 촉매계를 사용, 1-헥센용매중에서 에틸렌을 삼량화하는 것을 특징으로 하는 1-헥센의 제조방법.
(A): 일반식 CrXrYm으로 표시되는 크롬 함유 화합물, (여기에서,X는 카르복실산 잔기, 1,3-디케톤잔기, 할로겐원자 또는 알콕시기를 나타내며, k는 2 내지 4의 정수를 나타내고, Ym의 Y는 아민류, 포스핀류, 포스핀 옥사이드류, 니트로실기 또는 에테르류를 나타내며, m은 0 내기 6의 정수를 나타내고, 단, Ym의 각 Y는 동일하거나 상이하여도 좋다.)
(B): 트리알틸알루미늄 또는 디알킬알루미늄 히드리드, (C) : 피롤류 또는 그의 유도체, (D) : 일반식 MTtU3-t로 표시되는 13(ⅢB)족 할로겐화합물 또는 일반식 M´Tt´U4-t´로 표시되는 14(ⅣB)족 할로겐화합물, (여기에서, M은 13(ⅢB)족 원자를 나타내며, M´는 14(ⅣB)족 원자를 나타내고, T는 알킬기, 아릴기, 알릴기 또는 수소원자를 나타내며, U는 할로겐원자를 나타내고, t는 0 이상, 3미만의 실수를 나타내며, t´는 0이상,4미만의 실수를 나타낸다.)

Description

1-헥센의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (4)

1-헥센용매 중에서 하기성분(A),(B),(C)및 (D)를 접촉시켜서 얻어지는 초매계를 사용하는, 1-헥센용매중에서 에틸렌을 삼량화하는 것을 특징으로 하는 1-헥센의 제조방법.
(A) : 일반식 CrXkYm으로 표시되는 크롬 함유 화합물, (여기에서, X는 카르복실산 잔기, 1,3-디케톤잔기, 할로겐원자 또는 알콕시기를 나타내며, k는 2 내지 4의 정수를 나타내고, Ym의 Y는 아민류, 포스핀류, 포스핀 옥사이드류, 니트로실기 또는 에테르류를 나타내며, m은 0 내지 6의 정수를 나타내고, 단, Ym의 각 Y는 동일하거나 상이하여도 좋다.)
(B) : 트리알틸알루미늄 또는 디알킬알루미늄 히드리드, (C) : 피롤류 또는 그의 유도체, (D) : 일반식 MTtU3-t로 표시되는 13(ⅢB)족 할로겐화합물 또는 일반식 M´Tt´U4-t´로 표시되는 14(ⅣB)족 할로겐화합물,(여기에서, M은 13(ⅢB)족 원자를 나타내며,M'는 14(ⅣB)족 원자를 나타내고, T는 알킬기, 아릴기, 알릴기 또는 수소원자를 나타내며, U는 할로겐원자를 나타내고, t는 0이상, 3미만의 실수를 나타내며, t´는 0이상,4미만의 실수를 나타낸다.)
제1항에 있어서, (A) 성분이 X는 할로겐원자인 것을 특징으로 하는 1-헥센의제조방법.
제1항에 있어서, (B) 성분이 트리알킬알루미늄인 것을 특징으로 하는 1-헥센의 제조방법.
제1항에 있어서, 촉매계가 (A),(B),(C) 및 (D)성분을 용매주에 첨가하고, 다음에 (B) 성분을 첨가하여 얻어진 촉매계인 것을 특징으로 하는 1-헥센의 제조방법.
※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019950028634A 1994-09-05 1995-09-01 1-헥센의제조방법 Expired - Fee Related KR100339290B1 (ko)

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
JP94-211457 1994-09-05
JP21145794 1994-09-05
JP26984594 1994-11-02
JP94-269845 1994-11-02
JP95-141629 1995-06-08
JP14162995A JP3613642B2 (ja) 1994-09-05 1995-06-08 １−ヘキセンの製造方法

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KR960010595A true KR960010595A (ko) 1996-04-20
KR100339290B1 KR100339290B1 (ko) 2002-11-30

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US (1) US6521806B1 (ko)
EP (1) EP0699648B1 (ko)
JP (1) JP3613642B2 (ko)
KR (1) KR100339290B1 (ko)
CN (1) CN1057991C (ko)
CA (1) CA2156789A1 (ko)
DE (1) DE69502151T2 (ko)
TW (1) TW285662B (ko)

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DE69502151T2 (de) 1998-09-03
JPH08183747A (ja) 1996-07-16
EP0699648A1 (en) 1996-03-06
DE69502151D1 (de) 1998-05-28
CN1128745A (zh) 1996-08-14
US6521806B1 (en) 2003-02-18
JP3613642B2 (ja) 2005-01-26
KR100339290B1 (ko) 2002-11-30
TW285662B (ko) 1996-09-11
CN1057991C (zh) 2000-11-01
CA2156789A1 (en) 1996-03-06
EP0699648B1 (en) 1998-04-22

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