MA61705A1 - Procédé de préparation d'un précurseur ternaire - Google Patents

Procédé de préparation d'un précurseur ternaire

Info

Publication number
MA61705A1
MA61705A1 MA61705A MA61705A MA61705A1 MA 61705 A1 MA61705 A1 MA 61705A1 MA 61705 A MA61705 A MA 61705A MA 61705 A MA61705 A MA 61705A MA 61705 A1 MA61705 A1 MA 61705A1
Authority
MA
Morocco
Prior art keywords
seed crystal
salt
precursor
stirring
crystal
Prior art date
Application number
MA61705A
Other languages
English (en)
Inventor
Changdong Li
Yong Cai
Weiquan Li
Genghao Liu
Yongguang Li
Dingshan Ruan
Original Assignee
Hunan Brunp Recycling Tech Co Ltd
Hunan Brunp Ev Recycling Co Ltd
Guangdong Brunp Recycling Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hunan Brunp Recycling Tech Co Ltd, Hunan Brunp Ev Recycling Co Ltd, Guangdong Brunp Recycling Technology Co Ltd filed Critical Hunan Brunp Recycling Tech Co Ltd
Publication of MA61705A1 publication Critical patent/MA61705A1/fr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Complex oxides containing nickel and at least one other metal element
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G53/82—Compounds containing nickel, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/04—Oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/50—Agglomerated particles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)

Abstract

La présente invention concerne un procédé de préparation d'un précurseur ternaire, comprenant : tout d'abord, le mélange d'une première solution de sel métallique contenant un sel de nickel, un sel de cobalt et un sel de manganèse solubles, de l'hydroxyde d'ammonium et une solution d'hydroxyde de sodium, la régulation du ph, la réaction sous chauffage et agitation, et le vieillissement et la filtration d'une suspension épaisse obtenue pour obtenir un germe cristallin précurseur ; et ensuite, l'introduction du germe cristallin précurseur dans une solution acide diluée pour agitation, la filtration en vue d'obtenir un germe cristallin acidifié, le mélange d'une seconde solution de sel métallique contenant le sel de nickel, le sel de cobalt et le sel de manganèse solubles, la solution d'hydroxyde de sodium, et le germe cristallin acidifié, l'ajustement du ph, la réaction sous chauffage et agitation, et le vieillissement, la filtration et le séchage de la suspension épaisse obtenue pour obtenir le précurseur ternaire. Selon la présente invention, le germe cristallin précurseur est placé dans la solution acide diluée pour être agité, de sorte que la micropoudre amorphe sur la surface du germe cristallin est dissoute, une structure cristalline se développe, et les particules primaires deviennent également plus fines et plus minces dans la condition de lixiviation acide, créant ainsi des conditions favorables pour la croissance continue d'une plaquette le long de la surface du germe cristallin dans le processus ultérieur sans ammoniac.
MA61705A 2021-08-17 2022-05-27 Procédé de préparation d'un précurseur ternaire MA61705A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN202110944650.1A CN113697868B (zh) 2021-08-17 2021-08-17 一种三元前驱体的制备方法
PCT/CN2022/095671 WO2023020063A1 (fr) 2021-08-17 2022-05-27 Procédé de préparation d'un précurseur ternaire

Publications (1)

Publication Number Publication Date
MA61705A1 true MA61705A1 (fr) 2024-01-31

Family

ID=78653196

Family Applications (1)

Application Number Title Priority Date Filing Date
MA61705A MA61705A1 (fr) 2021-08-17 2022-05-27 Procédé de préparation d'un précurseur ternaire

Country Status (8)

Country Link
US (1) US20240025760A1 (fr)
CN (1) CN113697868B (fr)
DE (1) DE112022000279T5 (fr)
ES (1) ES2968773R1 (fr)
GB (1) GB2618684A (fr)
HU (1) HUP2400114A1 (fr)
MA (1) MA61705A1 (fr)
WO (1) WO2023020063A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113697868B (zh) * 2021-08-17 2022-11-15 广东邦普循环科技有限公司 一种三元前驱体的制备方法
WO2024164414A1 (fr) * 2023-02-06 2024-08-15 广东邦普循环科技有限公司 Précurseur d'hydroxyde de nickel-cobalt-manganèse ayant une structure poreuse radiale, et son procédé de préparation

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103746110A (zh) * 2014-01-26 2014-04-23 中国科学院长春应用化学研究所 一种镍钴锰三元材料的制备方法和锂离子电池正极材料
CN105399154A (zh) * 2015-11-25 2016-03-16 兰州金川新材料科技股份有限公司 一种镍钴锰三元氢氧化物的生产方法
CN108807968A (zh) * 2018-08-09 2018-11-13 中国恩菲工程技术有限公司 镍钴锰三元前驱体材料及其合成方法
CN108807976A (zh) * 2018-08-09 2018-11-13 中国恩菲工程技术有限公司 窄粒径分布的镍钴锰三元材料前驱体材料及其制备方法
CN108767248A (zh) * 2018-08-09 2018-11-06 中国恩菲工程技术有限公司 制备窄粒径分布的镍钴锰三元材料前驱体材料的装置
CN109546144B (zh) * 2018-11-29 2020-07-31 广东佳纳能源科技有限公司 三元前驱体的制备方法及其应用
CN109896550B (zh) * 2019-04-29 2021-06-22 中钢集团南京新材料研究院有限公司 一种三元前驱体废液回收利用制备铁红的方法
CN110817976B (zh) * 2019-10-25 2022-05-17 合肥国轩高科动力能源有限公司 一种正极材料前驱体及其制备方法和用途
CN110808367B (zh) * 2019-11-19 2020-10-30 浙江帕瓦新能源股份有限公司 一种三元前驱体及其制备方法
CN111003734A (zh) * 2019-12-25 2020-04-14 南通金通储能动力新材料有限公司 一种三元前驱体废料回收再利用的方法
CN111434616B (zh) * 2019-12-26 2022-12-20 蜂巢能源科技有限公司 空心结构碳酸盐二元前驱体及其制备方法和应用
CN111717940B (zh) * 2020-06-22 2022-07-08 华友新能源科技（衢州）有限公司 一种分级制备窄分布前驱体的方法
CN112531158B (zh) * 2020-12-09 2022-03-11 合肥国轩高科动力能源有限公司 一种高镍三元单晶材料及其制备方法
CN113697868B (zh) * 2021-08-17 2022-11-15 广东邦普循环科技有限公司 一种三元前驱体的制备方法

Also Published As

Publication number Publication date
GB2618684A (en) 2023-11-15
WO2023020063A1 (fr) 2023-02-23
CN113697868B (zh) 2022-11-15
ES2968773A2 (es) 2024-05-13
DE112022000279T5 (de) 2023-11-02
HUP2400114A1 (hu) 2024-05-28
GB202310058D0 (en) 2023-08-16
ES2968773R1 (es) 2025-06-06
US20240025760A1 (en) 2024-01-25
CN113697868A (zh) 2021-11-26

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