MA62361A1 - Procédé de récupération de nickel à partir de laitier de fer-aluminium obtenu par lixiviation de poudre de batterie - Google Patents

Procédé de récupération de nickel à partir de laitier de fer-aluminium obtenu par lixiviation de poudre de batterie

Info

Publication number
MA62361A1
MA62361A1 MA62361A MA62361A MA62361A1 MA 62361 A1 MA62361 A1 MA 62361A1 MA 62361 A MA62361 A MA 62361A MA 62361 A MA62361 A MA 62361A MA 62361 A1 MA62361 A1 MA 62361A1
Authority
MA
Morocco
Prior art keywords
iron
nickel
aluminum
solution
add
Prior art date
Application number
MA62361A
Other languages
English (en)
Inventor
Haijun Yu
Yinghao Xie
Xuemei Zhang
Changdong Li
Yingsheng Zhong
Aixia Li
Original Assignee
Guangdong Brunp Recycling Technology Co Ltd
Hunan Brunp Recycling Tech Co Ltd
Hunan Brunp Ev Recycling Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangdong Brunp Recycling Technology Co Ltd, Hunan Brunp Recycling Tech Co Ltd, Hunan Brunp Ev Recycling Co Ltd filed Critical Guangdong Brunp Recycling Technology Co Ltd
Publication of MA62361A1 publication Critical patent/MA62361A1/fr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B21/00—Obtaining aluminium
    • C22B21/0015—Obtaining aluminium by wet processes
    • C22B21/0023—Obtaining aluminium by wet processes from waste materials
    • C22B21/003—Obtaining aluminium by wet processes from waste materials from spent catalysts
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0407—Leaching processes
    • C22B23/0415—Leaching processes with acids or salt solutions except ammonium salts solutions
    • C22B23/043—Sulfurated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/44—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water
    • C01F7/441—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water by calcination
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00—Compounds of iron
    • C01G49/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/04—Oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/10—Sulfates
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B21/00—Obtaining aluminium
    • C22B21/0015—Obtaining aluminium by wet processes
    • C22B21/0023—Obtaining aluminium by wet processes from waste materials
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0407—Leaching processes
    • C22B23/0446—Leaching processes with an ammoniacal liquor or with a hydroxide of an alkali or alkaline-earth metal
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0453—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B23/0461—Treatment or purification of solutions, e.g. obtained by leaching by chemical methods
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/006—Wet processes
    • C22B7/007—Wet processes by acid leaching
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/006—Wet processes
    • C22B7/008—Wet processes by an alkaline or ammoniacal leaching
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/04—Working-up slag
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/54—Reclaiming serviceable parts of waste accumulators
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/84—Recycling of batteries or fuel cells

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Electrochemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

La présente invention divulgue un procédé de récupération de nickel à partir de laitier de fer-aluminium obtenu par lixiviation de poudre de batterie. Le procédé comprend les étapes suivantes consistant à : ajouter une solution d'acide sulfurique à un laitier de fer-aluminium pour qu'il se dissolve, de manière à obtenir une solution de sulfate ; puis ajouter un agent oxydant ; ajouter de l'eau ammoniaquée et du carbonate à la solution de sulfate oxydé ; ajuster le ph à 1,0-3,2 pour la réaction ; séparer l'hydroxyde ferrique en précipité pour obtenir une solution dont le fer a été éliminé ; ajouter du carbonate à la solution dont le fer a été éliminé, ajuster le ph à 3,2-5,5 pour la réaction ; séparer l'hydroxyde d'aluminium en précipité afin d'obtenir une solution dont l'aluminium a été éliminé ; ajouter de l'eau ammoniaquée à la solution dont l'aluminium a été éliminé, ajuster le ph à 7,0-8,8 pour la réaction ; laver et éliminer les impuretés pour obtenir un complexe de nickel ; ajouter un agent oxydant au complexe de nickel pour rompre le complexe, de façon à obtenir une solution contenant du nickel. Au moyen du présent procédé, une séparation efficace du fer, de l'aluminium et du nickel dans le laitier de fer-aluminium est réalisée efficacement, l'effet de séparation du fer, de l'aluminium et du nickel est amélioré, la perte de nickel est réduite, et le taux de récupération de nickel est amélioré.
MA62361A 2021-08-31 2022-05-12 Procédé de récupération de nickel à partir de laitier de fer-aluminium obtenu par lixiviation de poudre de batterie MA62361A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN202111013492.4A CN113789447B (zh) 2021-08-31 2021-08-31 回收电池粉浸出所得铁铝渣中镍的方法
PCT/CN2022/092486 WO2023029570A1 (fr) 2021-08-31 2022-05-12 Procédé de récupération de nickel à partir de laitier de fer-aluminium obtenu par lixiviation de poudre de batterie

Publications (1)

Publication Number Publication Date
MA62361A1 true MA62361A1 (fr) 2024-05-31

Family

ID=78876764

Family Applications (1)

Application Number Title Priority Date Filing Date
MA62361A MA62361A1 (fr) 2021-08-31 2022-05-12 Procédé de récupération de nickel à partir de laitier de fer-aluminium obtenu par lixiviation de poudre de batterie

Country Status (9)

Country Link
US (1) US20240124953A1 (fr)
CN (1) CN113789447B (fr)
DE (1) DE112022000718T5 (fr)
ES (1) ES2956183B2 (fr)
GB (1) GB2621293A (fr)
HU (1) HUP2300324A2 (fr)
MA (1) MA62361A1 (fr)
MX (1) MX2023014181A (fr)
WO (1) WO2023029570A1 (fr)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113789447B (zh) * 2021-08-31 2022-11-15 广东邦普循环科技有限公司 回收电池粉浸出所得铁铝渣中镍的方法
CN115821041B (zh) * 2022-09-01 2024-09-10 广东邦普循环科技有限公司 一种回收镍的方法
CN116274305A (zh) * 2023-03-22 2023-06-23 鲁西化工集团股份有限公司硅化工分公司 一种有机硅水解渣无害化处置的系统及方法
CN116924483A (zh) * 2023-07-11 2023-10-24 浙江海创锂电科技有限公司 一种镍铁锰前驱体固废料回收利用制备镍锰盐溶液的方法
CN117795107A (zh) * 2023-10-13 2024-03-29 广东邦普循环科技有限公司 一种铁铝渣资源化回收铝和铁的方法
WO2025228961A1 (fr) * 2024-04-29 2025-11-06 Genomines Procédés et plantes pour phytominage
CN118516567B (zh) * 2024-05-21 2025-04-25 宜春江理锂电新能源产业研究院 一种从含锂酸浸液中除铝的方法
CN118957269B (zh) * 2024-07-30 2025-05-27 山东省昔利环境科技有限公司 一种赤泥酸浸回收铁铝及回收酸的方法

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103031441B (zh) * 2011-09-30 2014-03-26 武汉格林美资源循环有限公司 废旧镍氢电池中金属元素回收方法
CN102616867B (zh) * 2012-04-11 2013-07-31 合肥工业大学 一种由蛇纹石及其尾矿中提取制备碳酸镍、硫酸镍和氧化铁红的方法
CN103288145B (zh) * 2013-05-30 2015-02-25 先进储能材料国家工程研究中心有限责任公司 一种制备球形α-氢氧化镍的方法
FR3013359B1 (fr) * 2013-11-18 2016-01-01 Commissariat Energie Atomique Procede de recuperation des metaux contenus dans un accumulateur de type ni-mh
CN104787928B (zh) * 2015-04-16 2016-10-05 南阳师范学院 一种含铁、铬、镍不锈钢酸洗废液的回收处理方法
JP6622998B2 (ja) * 2015-08-10 2019-12-18 Ｊｘ金属株式会社 リチウムイオン電池スクラップからの鉄及びアルミニウムの除去方法及び、有価金属の回収方法
CN105506290B (zh) * 2015-11-30 2018-01-09 湖南邦普循环科技有限公司 一种铁铝渣综合利用的方法
CN109072335B (zh) * 2016-03-16 2021-07-20 捷客斯金属株式会社 锂离子电池废料的处理方法
CN108866328A (zh) * 2018-04-27 2018-11-23 湖南邦普循环科技有限公司 一种镍钴锰溶液中除铁铝的方法
CN110492193A (zh) * 2019-08-09 2019-11-22 珠海格力电器股份有限公司 一种从废旧三元锂离子电池中回收铁、铝的方法
CN111004918B (zh) * 2019-12-23 2021-11-12 先进储能材料国家工程研究中心有限责任公司 利用废旧镍氢电池回收制备α球镍的方法
CN111041214B (zh) * 2019-12-23 2021-08-31 先进储能材料国家工程研究中心有限责任公司 利用废旧含锌镍氢电池回收制备α球镍的方法
CN111261967A (zh) * 2020-01-22 2020-06-09 宁波容百新能源科技股份有限公司 一种废旧锂电池的回收方法及回收制备的电池级镍钴锰混合晶体
CN111519031B (zh) * 2020-04-29 2022-06-28 江苏北矿金属循环利用科技有限公司 一种从废旧动力锂离子电池黑粉中回收镍钴锰锂的方法
CN113249574A (zh) * 2021-04-07 2021-08-13 广东邦普循环科技有限公司 利用选择性浸出回收废正极片中铝的方法及其应用
CN113789447B (zh) * 2021-08-31 2022-11-15 广东邦普循环科技有限公司 回收电池粉浸出所得铁铝渣中镍的方法

Also Published As

Publication number Publication date
CN113789447A (zh) 2021-12-14
US20240124953A1 (en) 2024-04-18
ES2956183R1 (es) 2024-11-11
GB2621293A (en) 2024-02-07
DE112022000718T5 (de) 2023-11-09
ES2956183B2 (es) 2025-10-09
ES2956183A2 (es) 2023-12-14
WO2023029570A1 (fr) 2023-03-09
MX2023014181A (es) 2024-03-13
HUP2300324A2 (hu) 2023-12-28
CN113789447B (zh) 2022-11-15
GB202318269D0 (en) 2024-01-17

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