MD636Y - Process for producing flavonoid glycosides from Linaria vulgaris Mill. - Google Patents
Process for producing flavonoid glycosides from Linaria vulgaris Mill. Download PDFInfo
- Publication number
- MD636Y MD636Y MDS20120181A MDS20120181A MD636Y MD 636 Y MD636 Y MD 636Y MD S20120181 A MDS20120181 A MD S20120181A MD S20120181 A MDS20120181 A MD S20120181A MD 636 Y MD636 Y MD 636Y
- Authority
- MD
- Moldova
- Prior art keywords
- temperature
- methanol
- flavonoid glycosides
- concentrated
- vacuum
- Prior art date
Links
- 241000167860 Linaria vulgaris Species 0.000 title abstract 2
- 229930182486 flavonoid glycoside Natural products 0.000 title abstract 2
- 150000007955 flavonoid glycosides Chemical class 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 abstract 2
- 239000004952 Polyamide Substances 0.000 abstract 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 1
- WORJEOGGNQDSOE-UHFFFAOYSA-N chloroform;methanol Chemical compound OC.ClC(Cl)Cl WORJEOGGNQDSOE-UHFFFAOYSA-N 0.000 abstract 1
- 238000010828 elution Methods 0.000 abstract 1
- 239000000284 extract Substances 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 229930182470 glycoside Natural products 0.000 abstract 1
- 150000002338 glycosides Chemical class 0.000 abstract 1
- GBMDVOWEEQVZKZ-UHFFFAOYSA-N methanol;hydrate Chemical compound O.OC GBMDVOWEEQVZKZ-UHFFFAOYSA-N 0.000 abstract 1
- 229920002647 polyamide Polymers 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 239000000741 silica gel Substances 0.000 abstract 1
- 229910002027 silica gel Inorganic materials 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Landscapes
- Pyrane Compounds (AREA)
Abstract
The invention relates to bioorganic chemistry and can be used for producing flavonoid glycosides from Linaria vulgaris Mill.The process, according to the invention, consists in that the freshly harvested raw material is ground and subjected to extraction with methanol 3 times, for 5 hours, at the temperature of 35…40°C, after which the extracts are combined and concentrated in vacuum at a temperature of 40°C up to a constant volume, then are extracted with benzene the ballast substances, and the resulting fractions are chromatographed on polyamide column with elution in the water-methanol system in the ratio of 4:1 and are analyzed in a thin layer of silica gel with chloroform-methanol in the ratio of 3:1, respectively, afterwards the fractions containing glycosides are combined and concentrated in vacuum at the temperature of 40°C in the presence of butanol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MDS20120181A MD636Z (en) | 2012-12-21 | 2012-12-21 | Process for producing flavonoid glycosides from Linaria vulgaris Mill. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MDS20120181A MD636Z (en) | 2012-12-21 | 2012-12-21 | Process for producing flavonoid glycosides from Linaria vulgaris Mill. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MD636Y true MD636Y (en) | 2013-05-31 |
| MD636Z MD636Z (en) | 2013-12-31 |
Family
ID=48537086
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MDS20120181A MD636Z (en) | 2012-12-21 | 2012-12-21 | Process for producing flavonoid glycosides from Linaria vulgaris Mill. |
Country Status (1)
| Country | Link |
|---|---|
| MD (1) | MD636Z (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MD4301C1 (en) * | 2013-06-12 | 2015-03-31 | Институт Генетики, Физиологии И Защиты Растений Академии Наук Молдовы | 1-epi-5-O-alozilantirinozide for the treatment of lettuce seeds |
| MD844Z (en) * | 2014-05-07 | 2015-07-31 | Институт Генетики, Физиологии И Защиты Растений Академии Наук Молдовы | Process for growing tobacco plants |
| MD893Z (en) * | 2014-10-08 | 2015-11-30 | Институт Генетики, Физиологии И Защиты Растений Академии Наук Молдовы | Process for presowing treatment of onion seeds |
| MD1012Z (en) * | 2015-09-09 | 2016-10-31 | Институт Генетики, Физиологии И Защиты Растений Академии Наук Молдовы | Process for treatment of grape-vine |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MD825Z (en) * | 2014-01-22 | 2015-05-31 | Алёна ГЕНДОВ-МОШАНУ | Process for producing polyphenols from grape pomace |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU990230A1 (en) * | 1981-09-04 | 1983-01-23 | Отдел Генетики Растений Ан Мсср | Method of producing steroid glicosides having antimicrobic activity |
| SU1696434A1 (en) * | 1989-10-18 | 1991-12-07 | Институт экологической генетики АН МССР | Method for preparation of steroid glycosides of furostane series |
| MD555G2 (en) * | 1995-10-04 | 1996-12-31 | Институт Генетики И Физиологии Растений Академии Наук Молдовы | Method of obtaining of steroidal glycosides |
| MD645G2 (en) * | 1996-02-07 | 1997-07-31 | Институт Генетики И Физиологии Растений Академии Наук Молдовы | Method of furostanol glycosides production |
| MD2004G2 (en) * | 2001-04-11 | 2003-03-31 | Институт Генетики И Физиологии Растений Академии Наук Молдовы | Process for obtaining of furastanolic glycosides |
| MD2037G2 (en) * | 2001-04-26 | 2003-05-31 | Институт Генетики И Физиологии Растений Академии Наук Молдовы | Process for obtaining the 22-O-hydroxyfurostanols |
| MD2716G2 (en) * | 2004-04-13 | 2005-10-31 | Институт Генетики И Физиологии Растений Академии Наук Молдовы | Antistressor for winter common wheat |
| MD3866C2 (en) * | 2008-12-19 | 2009-10-31 | Институт Генетики, Физиологии И Защиты Растений Академии Наук Молдовы | 5,4-dimethylcampherol 3-O--D-(6′′-a′-L-rhamnopyranosyl)-glucopyranoside as compound increasing the seed productivity |
| MD98Z (en) * | 2009-06-19 | 2010-06-30 | Институт Генетики, Физиологии И Защиты Растений Академии Наук Молдовы | Process for presowing treatment of sweet pepper seeds |
-
2012
- 2012-12-21 MD MDS20120181A patent/MD636Z/en not_active IP Right Cessation
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MD4301C1 (en) * | 2013-06-12 | 2015-03-31 | Институт Генетики, Физиологии И Защиты Растений Академии Наук Молдовы | 1-epi-5-O-alozilantirinozide for the treatment of lettuce seeds |
| MD844Z (en) * | 2014-05-07 | 2015-07-31 | Институт Генетики, Физиологии И Защиты Растений Академии Наук Молдовы | Process for growing tobacco plants |
| MD893Z (en) * | 2014-10-08 | 2015-11-30 | Институт Генетики, Физиологии И Защиты Растений Академии Наук Молдовы | Process for presowing treatment of onion seeds |
| MD1012Z (en) * | 2015-09-09 | 2016-10-31 | Институт Генетики, Физиологии И Защиты Растений Академии Наук Молдовы | Process for treatment of grape-vine |
Also Published As
| Publication number | Publication date |
|---|---|
| MD636Z (en) | 2013-12-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG9Y | Short term patent issued | ||
| KA4Y | Short-term patent lapsed due to non-payment of fees (with right of restoration) |