MX2019013201A - Metodo de produccion de acido 1-aminociclopropancarboxilico no hidrato. - Google Patents
Metodo de produccion de acido 1-aminociclopropancarboxilico no hidrato.Info
- Publication number
- MX2019013201A MX2019013201A MX2019013201A MX2019013201A MX2019013201A MX 2019013201 A MX2019013201 A MX 2019013201A MX 2019013201 A MX2019013201 A MX 2019013201A MX 2019013201 A MX2019013201 A MX 2019013201A MX 2019013201 A MX2019013201 A MX 2019013201A
- Authority
- MX
- Mexico
- Prior art keywords
- carboxylic acid
- cyclopropane carboxylic
- amino cyclopropane
- production method
- nonhydrate
- Prior art date
Links
- PAJPWUMXBYXFCZ-UHFFFAOYSA-N 1-aminocyclopropanecarboxylic acid Chemical compound OC(=O)C1(N)CC1 PAJPWUMXBYXFCZ-UHFFFAOYSA-N 0.000 title abstract 6
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000013078 crystal Substances 0.000 abstract 2
- WTZRHZRMLYNBRM-UHFFFAOYSA-N 1-aminocyclopropane-1-carboxylic acid;hydrochloride Chemical compound Cl.OC(=O)C1(N)CC1 WTZRHZRMLYNBRM-UHFFFAOYSA-N 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
- C07C227/16—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions not involving the amino or carboxyl groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
- C07C227/42—Crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/46—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino or carboxyl groups bound to carbon atoms of rings other than six-membered aromatic rings of the same carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/46—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino or carboxyl groups bound to carbon atoms of rings other than six-membered aromatic rings of the same carbon skeleton
- C07C229/48—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino or carboxyl groups bound to carbon atoms of rings other than six-membered aromatic rings of the same carbon skeleton with amino groups and carboxyl groups bound to carbon atoms of the same non-condensed ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La presente invención se relaciona con la obtención del ácido 1-aminociclopropancarboxílico no hidrato al tratar clorhidrato de ácido 1-aminociclopropancarboxílico con una amina terciaria en presencia de un alcohol C3-C4 y agua, mantener la mezcla de reacción a 50°C o menos, recolectar el cristal precipitado de ácido 1-aminociclopropancarboxílico hemihidrato por filtración y calentar el cristal obtenido de 80 a 245°C.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2017092614 | 2017-05-08 | ||
| PCT/JP2018/017481 WO2018207693A1 (ja) | 2017-05-08 | 2018-05-02 | １－アミノシクロプロパンカルボン酸非水和物の製造方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2019013201A true MX2019013201A (es) | 2020-01-20 |
Family
ID=64104578
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2019013201A MX2019013201A (es) | 2017-05-08 | 2018-05-02 | Metodo de produccion de acido 1-aminociclopropancarboxilico no hidrato. |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US10654793B2 (es) |
| EP (1) | EP3636630B1 (es) |
| JP (1) | JP7009460B2 (es) |
| KR (1) | KR102550280B1 (es) |
| CN (1) | CN110603242B (es) |
| AR (1) | AR111659A1 (es) |
| AU (1) | AU2018267358B2 (es) |
| BR (1) | BR112019022833B1 (es) |
| CL (1) | CL2019003160A1 (es) |
| DK (1) | DK3636630T3 (es) |
| ES (1) | ES2906445T3 (es) |
| HU (1) | HUE057914T2 (es) |
| IL (1) | IL270408B (es) |
| MX (1) | MX2019013201A (es) |
| PE (1) | PE20200236A1 (es) |
| PL (1) | PL3636630T3 (es) |
| PT (1) | PT3636630T (es) |
| SI (1) | SI3636630T1 (es) |
| TW (1) | TWI757479B (es) |
| WO (1) | WO2018207693A1 (es) |
| ZA (1) | ZA201908126B (es) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11014872B1 (en) * | 2017-05-08 | 2021-05-25 | Sumitomo Chemical Company, Limited | Production method for 1-amino cyclopropane carboxylic acid nonhydrate |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4116862B1 (es) * | 1964-05-16 | 1966-09-24 | ||
| DE2936038A1 (de) | 1979-09-06 | 1981-03-26 | Bayer Ag, 51373 Leverkusen | Verfahren zur herstellung von 1-aminocyclopropan-carbonsaeure und deren derivaten |
| JP4519564B2 (ja) * | 2004-08-05 | 2010-08-04 | ダイセル化学工業株式会社 | １−アミノシクロプロパンカルボン酸の精製方法及び製造方法 |
| JP2020016862A (ja) * | 2018-07-27 | 2020-01-30 | 京セラ株式会社 | カメラ装置、カメラシステム、移動体およびカメラ装置の製造方法 |
-
2018
- 2018-05-02 PT PT187989827T patent/PT3636630T/pt unknown
- 2018-05-02 PL PL18798982T patent/PL3636630T3/pl unknown
- 2018-05-02 TW TW107114867A patent/TWI757479B/zh active
- 2018-05-02 WO PCT/JP2018/017481 patent/WO2018207693A1/ja not_active Ceased
- 2018-05-02 HU HUE18798982A patent/HUE057914T2/hu unknown
- 2018-05-02 ES ES18798982T patent/ES2906445T3/es active Active
- 2018-05-02 BR BR112019022833-0A patent/BR112019022833B1/pt active IP Right Grant
- 2018-05-02 DK DK18798982.7T patent/DK3636630T3/da active
- 2018-05-02 US US16/611,577 patent/US10654793B2/en active Active
- 2018-05-02 JP JP2019517590A patent/JP7009460B2/ja active Active
- 2018-05-02 EP EP18798982.7A patent/EP3636630B1/en active Active
- 2018-05-02 CN CN201880029850.0A patent/CN110603242B/zh active Active
- 2018-05-02 MX MX2019013201A patent/MX2019013201A/es unknown
- 2018-05-02 SI SI201830539T patent/SI3636630T1/sl unknown
- 2018-05-02 AR ARP180101128A patent/AR111659A1/es active IP Right Grant
- 2018-05-02 PE PE2019002287A patent/PE20200236A1/es unknown
- 2018-05-02 KR KR1020197034780A patent/KR102550280B1/ko active Active
- 2018-05-02 AU AU2018267358A patent/AU2018267358B2/en active Active
-
2019
- 2019-11-04 CL CL2019003160A patent/CL2019003160A1/es unknown
- 2019-11-04 IL IL270408A patent/IL270408B/en unknown
- 2019-12-05 ZA ZA2019/08126A patent/ZA201908126B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BR112019022833A2 (pt) | 2020-05-26 |
| AU2018267358B2 (en) | 2021-07-01 |
| US10654793B2 (en) | 2020-05-19 |
| ES2906445T3 (es) | 2022-04-18 |
| CA3062789A1 (en) | 2018-11-28 |
| NZ759688A (en) | 2024-04-26 |
| CN110603242A (zh) | 2019-12-20 |
| KR102550280B1 (ko) | 2023-06-30 |
| SI3636630T1 (sl) | 2022-04-29 |
| AU2018267358A1 (en) | 2019-12-19 |
| DK3636630T3 (da) | 2022-01-31 |
| PE20200236A1 (es) | 2020-02-03 |
| HUE057914T2 (hu) | 2022-07-28 |
| AR111659A1 (es) | 2019-08-07 |
| CN110603242B (zh) | 2022-06-28 |
| PL3636630T3 (pl) | 2022-03-07 |
| BR112019022833B1 (pt) | 2022-12-20 |
| TWI757479B (zh) | 2022-03-11 |
| JPWO2018207693A1 (ja) | 2020-03-12 |
| US20200095188A1 (en) | 2020-03-26 |
| ZA201908126B (en) | 2021-04-28 |
| EP3636630B1 (en) | 2021-12-15 |
| IL270408B (en) | 2021-12-01 |
| WO2018207693A1 (ja) | 2018-11-15 |
| EP3636630A4 (en) | 2021-01-27 |
| CL2019003160A1 (es) | 2020-04-13 |
| PT3636630T (pt) | 2022-01-31 |
| EP3636630A1 (en) | 2020-04-15 |
| KR20200003001A (ko) | 2020-01-08 |
| TW201900602A (zh) | 2019-01-01 |
| JP7009460B2 (ja) | 2022-01-25 |
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