MX355246B - Postratamiento de zeolita desboronada mww. - Google Patents

Postratamiento de zeolita desboronada mww.

Info

Publication number
MX355246B
MX355246B MX2015004948A MX2015004948A MX355246B MX 355246 B MX355246 B MX 355246B MX 2015004948 A MX2015004948 A MX 2015004948A MX 2015004948 A MX2015004948 A MX 2015004948A MX 355246 B MX355246 B MX 355246B
Authority
MX
Mexico
Prior art keywords
zeolitic material
post
wind
treatment
framework structure
Prior art date
Application number
MX2015004948A
Other languages
English (en)
Other versions
MX2015004948A (es
Inventor
Gaab Manuela
Maurer Stefan
Müller Ulrich
yang Jeff
Seidel Karsten
Parvulescu Andrei-Nicolae
Gerlach Olga
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2015004948A publication Critical patent/MX2015004948A/es
Publication of MX355246B publication Critical patent/MX355246B/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/007—Borosilicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/12—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least boron atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/16—After treatment, characterised by the effect to be obtained to increase the Si/Al ratio; Dealumination
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/37—Acid treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/40—Special temperature treatment, i.e. other than just for template removal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/05—Nuclear magnetic resonance [NMR]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/10—Infrared [IR]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)

Abstract

Un proceso para el postratamiento de un material zeolítico que tiene una estructura marco MWW, que comprende (i) brindar un material zeolítico que tiene una estructura marco MVVW, en donde la estructura marco del material zeolítico comprende X2O3 e YO2, en donde Y es un elemento tetravalente y X es un elemento trivalente y en donde la relación molar X2O3: YO2 es mayor que 0,02 1; (ii) tratar el material zeolítico proporcionado en (i) con un sistema solvente líquido obteniendo así un material zeolítico que tiene una relación molar X2O3: YO2 de a lo sumo 0,02: 1 y al menos separar parcialmente el material zeolítico del sistema solvente líquido; (iii) tratar el material zeolítico obtenido de (ii) con un sistema acuoso líquido que tiene un pH en el rango de 5,5 a 8 y una temperatura de al menos 75 °C.
MX2015004948A 2012-10-18 2013-10-09 Postratamiento de zeolita desboronada mww. MX355246B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12189042 2012-10-18
PCT/EP2013/071042 WO2014060261A1 (en) 2012-10-18 2013-10-09 Post-treatment of deboronated mww zeolite

Publications (2)

Publication Number Publication Date
MX2015004948A MX2015004948A (es) 2016-01-20
MX355246B true MX355246B (es) 2018-04-11

Family

ID=47046432

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2015004948A MX355246B (es) 2012-10-18 2013-10-09 Postratamiento de zeolita desboronada mww.

Country Status (13)

Country Link
US (1) US10099933B2 (es)
EP (1) EP2909141B1 (es)
JP (1) JP6267211B2 (es)
KR (1) KR102184609B1 (es)
CN (1) CN104854028B (es)
BR (1) BR112015008390B1 (es)
ES (1) ES2620030T3 (es)
MX (1) MX355246B (es)
MY (1) MY169039A (es)
RU (1) RU2638851C2 (es)
SG (1) SG11201503019SA (es)
WO (1) WO2014060261A1 (es)
ZA (1) ZA201503155B (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MX357216B (es) 2012-10-18 2018-06-29 Basf Se Postratamiento de un material zeolitico.
CN106536411B (zh) * 2014-06-06 2020-05-12 巴斯夫欧洲公司 具有mww骨架结构的含硼沸石的合成
ES2727604T3 (es) * 2014-09-09 2019-10-17 Basf Se Un proceso para la preparación de un material zeolítico MWW que contiene boro y titanio
WO2016058541A1 (en) 2014-10-15 2016-04-21 Basf Se Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom
CN109689572B (zh) * 2016-09-06 2023-01-24 巴斯夫欧洲公司 具有mww骨架结构的含硼沸石的固热合成
EP3558516A1 (en) 2016-12-20 2019-10-30 Basf Se A process for preparing an extrudable composition comprising a titanium-containing zeolitic material having framework type mww
CN110087768B (zh) * 2016-12-20 2023-09-01 巴斯夫欧洲公司 酸处理以使包含具有mww骨架类型的含钛沸石材料的组合物的可塑性降低的用途
JP7123955B2 (ja) 2017-02-28 2022-08-23 ビーエーエスエフ ソシエタス・ヨーロピア 不飽和アルコールを調製する方法
WO2018210809A1 (en) * 2017-05-15 2018-11-22 Basf Se A process for preparing a zeolitic material having framework type aei

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2445747A1 (fr) 1979-01-05 1980-08-01 Armines Procede de fabrication de pieces en silicium nitrure
US4622166A (en) * 1982-03-17 1986-11-11 Mizusawa Kagaku Kogyo Kabushiki Kaisha Process for preparation of zeolite slurry excellent in static stability and dynamic stability
DE4207745A1 (de) * 1992-03-11 1993-09-16 Basf Ag Azofarbstoffe enthaltende molekularsiebe
WO2002057181A2 (en) 2000-12-22 2002-07-25 California Institute Of Technology Synthesis of molecular sieves by hydrothermal treatment with acid
JP4241068B2 (ja) * 2002-03-07 2009-03-18 昭和電工株式会社 Ｍｗｗ型ゼオライト物質の製造方法
WO2006002116A2 (en) * 2004-06-17 2006-01-05 Yale University Size-controllable transition metal clusters in mcm-41 for improving chemical catalysts
CN100363259C (zh) 2004-12-23 2008-01-23 中国科学院大连化学物理研究所 一种高硅mcm-22分子筛的制备方法
WO2008016456A2 (en) * 2006-07-28 2008-02-07 Exxonmobil Chemical Patents Inc. Molecular sieve composition (emm-10), its method of making, and use for hydrocarbon conversions
EP2025402A1 (en) * 2007-07-31 2009-02-18 Total Petrochemicals Research Feluy Phosphorus modified molecular sieves, their use in conversion of organics to olefins
US7737313B2 (en) * 2006-12-21 2010-06-15 Exxonmobil Chemical Patents Inc. Catalyst composition, the method of manufacturing, and the process of using thereof in hydrocarbon conversions
US20110313179A1 (en) * 2009-03-13 2011-12-22 Sumitomo Chemical Company, Limited Method for producing olefin oxide
WO2012074033A1 (ja) * 2010-11-30 2012-06-07 住友化学株式会社 チタン含有珪素酸化物成形体の製造方法及びオキシラン化合物の製造方法
US9522390B2 (en) * 2010-12-10 2016-12-20 The Regents Of The University Of California Oxide materials and synthesis by fluoride/chloride anion promoted exfoliation

Also Published As

Publication number Publication date
KR102184609B1 (ko) 2020-12-01
KR20150074076A (ko) 2015-07-01
US10099933B2 (en) 2018-10-16
BR112015008390B1 (pt) 2021-11-03
ZA201503155B (en) 2017-11-29
MX2015004948A (es) 2016-01-20
EP2909141B1 (en) 2016-12-14
MY169039A (en) 2019-02-07
EP2909141A1 (en) 2015-08-26
CN104854028A (zh) 2015-08-19
WO2014060261A1 (en) 2014-04-24
US20150329368A1 (en) 2015-11-19
ES2620030T3 (es) 2017-06-27
RU2015118225A (ru) 2016-12-10
BR112015008390A2 (pt) 2017-08-08
SG11201503019SA (en) 2015-05-28
JP6267211B2 (ja) 2018-01-24
CN104854028B (zh) 2017-07-18
RU2638851C2 (ru) 2017-12-18
JP2015532259A (ja) 2015-11-09

Similar Documents

Publication Publication Date Title
MX355246B (es) Postratamiento de zeolita desboronada mww.
MX2015004946A (es) Postratamiento de un material zeolitico.
MY195237A (en) Process For The Preparation of a Zeolitic Material
BR112015023198A2 (pt) materiais compósitos aerados, metodos de produção e usos dos mesmos
AR076027A1 (es) Metodos e intermediarios para la preparacion de agentes farmaceuticos
CL2013002712A1 (es) Composicion inmunogénica para modular sistema inmune que comprende agentes con patrones asociados a bacterias, virus, hongos y levaduras, protozoos, helmintos y/o priones; uso para tratar enfermedades autoinmunes o infecciosas.
WO2014197928A8 (en) Biorefining method
BR112015029175A2 (pt) processo para preparar ácido levulínico
BR112015022795A2 (pt) processo de conversão de hmf em fdca
BR112015022618A2 (pt) processo para a preparação de ácido levulínico
MX2015004945A (es) Postratamiento de zeolita beta desboronada.
CO2018004288A2 (es) Método de preparación de una sustancia de p-fenilendiamina sustituida con arilo
BR112015032223A2 (pt) processo para a preparação por fermentação de ácido
BR112015000864A2 (pt) processo para remoção de peróxido de hidrogênio a partir de uma solução aquosa
BR112017016430A2 (pt) processo para preparação de diosmina
RU2012157327A (ru) Способ получения полимер-неорганических композитных сорбентов
WO2015020769A3 (en) Controllable nucleic acid delivery systems
AR097100A1 (es) Proceso para la deshidrohalogenación de un compuesto orgánico no polimérico halogenado
BR112015031531A2 (pt) produção de solvente
BR112016007654A2 (pt) processo para preparar ácido levulínico
TW201612110A (en) Water-molecule synchronous resonance manufacturing method
TH106349B (th) การบำบัดขั้นหลังของซีโอไลท์เบต้าที่ถูกดึงโบรอนออก
RU2015140786A (ru) Способ получения состава с гербицидной активностью
BR112012024534A2 (pt) interconversão entre ácidos p-metano-3-carboxílicos isoméricos
Echi Rational solutions of Riccati differential equation with coefficients rational

Legal Events

Date Code Title Description
FG Grant or registration