MX373873B - Proceso de sintesis de ambrox a partir de 13,14,15,16,-tetranor-8a,12-labdanodiol. - Google Patents

Proceso de sintesis de ambrox a partir de 13,14,15,16,-tetranor-8a,12-labdanodiol.

Info

Publication number
MX373873B
MX373873B MX2015014942A MX2015014942A MX373873B MX 373873 B MX373873 B MX 373873B MX 2015014942 A MX2015014942 A MX 2015014942A MX 2015014942 A MX2015014942 A MX 2015014942A MX 373873 B MX373873 B MX 373873B
Authority
MX
Mexico
Prior art keywords
labdanodiol
ambroxide
tetranor
synthesising
compound
Prior art date
Application number
MX2015014942A
Other languages
English (en)
Other versions
MX2015014942A (es
Inventor
Pacheco Iroel García
Hurtado Mario Armando Gómez
Pacheco Mauro Manuel Martínez
Río Torres Rosa Elva Norma Del
Original Assignee
Univ Michoacana De San Nicolas De Hidalgo
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Univ Michoacana De San Nicolas De Hidalgo filed Critical Univ Michoacana De San Nicolas De Hidalgo
Priority to MX2015014942A priority Critical patent/MX373873B/es
Priority to PCT/IB2015/058938 priority patent/WO2017068400A1/es
Publication of MX2015014942A publication Critical patent/MX2015014942A/es
Publication of MX373873B publication Critical patent/MX373873B/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/77—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D307/92—Naphthofurans; Hydrogenated naphthofurans

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

La presente invención se refiere a un proceso de síntesis del compuesto (±)-ambrox a partir del compuesto (±) 13,14,15,16-tetranor-8a,12-labdanodiol, el proceso comprende los pasos de: a) disolver el compuesto (±) 13,14,15,16-tetranor-8a,12-Iabdanodiol en un disolvente orgánico; b) adicionar BF3.OEt2 para obtener (±)-ambrox; y c) remover el disolvente orgánico.
MX2015014942A 2015-10-23 2015-10-23 Proceso de sintesis de ambrox a partir de 13,14,15,16,-tetranor-8a,12-labdanodiol. MX373873B (es)

Priority Applications (2)

Application Number Priority Date Filing Date Title
MX2015014942A MX373873B (es) 2015-10-23 2015-10-23 Proceso de sintesis de ambrox a partir de 13,14,15,16,-tetranor-8a,12-labdanodiol.
PCT/IB2015/058938 WO2017068400A1 (es) 2015-10-23 2015-11-18 Proceso de síntesis de ambrox a partir de 13,14,15,16-tetranor-8α,12-labdanodiol

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
MX2015014942A MX373873B (es) 2015-10-23 2015-10-23 Proceso de sintesis de ambrox a partir de 13,14,15,16,-tetranor-8a,12-labdanodiol.

Publications (2)

Publication Number Publication Date
MX2015014942A MX2015014942A (es) 2017-04-24
MX373873B true MX373873B (es) 2020-03-26

Family

ID=58556761

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2015014942A MX373873B (es) 2015-10-23 2015-10-23 Proceso de sintesis de ambrox a partir de 13,14,15,16,-tetranor-8a,12-labdanodiol.

Country Status (2)

Country Link
MX (1) MX373873B (es)
WO (1) WO2017068400A1 (es)

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4613710A (en) * 1984-08-08 1986-09-23 Firmenich Sa Process for the preparation of (±)-3a-6,6,9a-tetramethylperhydronaphto[2,]furan
US5463089A (en) * 1994-07-22 1995-10-31 Quest International B.V. Preparation of ambrox
ES2195777B1 (es) * 2002-03-22 2005-03-16 Universidad De Granada Procedimiento para la obtencion de productos olorosos tipo ambar gris a partir de esclareol.
ES2536876T3 (es) * 2007-10-23 2015-05-29 Firmenich S.A. Procedimiento de preparación de derivados de tetranorlabdano
US9518037B2 (en) * 2012-10-19 2016-12-13 Kao Corporation Method for producing N,N-dialkylhomofarnesic acid amide

Also Published As

Publication number Publication date
MX2015014942A (es) 2017-04-24
WO2017068400A1 (es) 2017-04-27

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