MY125174A - Improved process for coproduction of 6-aminocapronitrile and hexamethylenediamine. - Google Patents
Improved process for coproduction of 6-aminocapronitrile and hexamethylenediamine.Info
- Publication number
- MY125174A MY125174A MYPI99003039A MYPI19993039A MY125174A MY 125174 A MY125174 A MY 125174A MY PI99003039 A MYPI99003039 A MY PI99003039A MY PI19993039 A MYPI19993039 A MY PI19993039A MY 125174 A MY125174 A MY 125174A
- Authority
- MY
- Malaysia
- Prior art keywords
- aminocapronitrile
- hexamethylenediamine
- adiponitrile
- coproduction
- improved process
- Prior art date
Links
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 title abstract 10
- KBMSFJFLSXLIDJ-UHFFFAOYSA-N 6-aminohexanenitrile Chemical compound NCCCCCC#N KBMSFJFLSXLIDJ-UHFFFAOYSA-N 0.000 title abstract 5
- BTGRAWJCKBQKAO-UHFFFAOYSA-N adiponitrile Chemical compound N#CCCCCC#N BTGRAWJCKBQKAO-UHFFFAOYSA-N 0.000 abstract 6
- 239000000203 mixture Substances 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 1
- 230000007704 transition Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/82—Purification; Separation; Stabilisation; Use of additives
- C07C209/86—Separation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
A PROCESS FOR THE COPRODUCTION OF 6-AMINOCAPRONITRILE AND HEXAMETHYLENEDIAMINE STARTING FROM ADIPONITRILE BY A) HYDROGENATING ADIPONITRILE IN THE PRESENCE OF A CATALYST COMPRISING AN ELEMENT OF THE EIGHTH TRANSITION GROUP AS CATALYTICALLY ACTIVE COMPONENT, TO OBTAIN A MIXTURE COMPRISING 6-AMINOCAPRONITRILE, HEXAMETHYLENEDIAMINE, ADIPONITRILE AND HIGH BOILERS,B) DISTILLATIVELY REMOVING HEXAMETHYLENEDIAMINE FROM THE MIXTURE COMPRISING 6-AMINOCAPRONITRILE, HEXAMETHYLENEDIAMINE, ADIPONITRILE AND HIGH BOILERS, AND EITHER C1) DISTILLATIVELY REMOVING 6-AMINOCAPNITRILE, AND THEN D1)DISTILLATIVELY REMOVING ADIPONITRILE, OR C2) SIMULTANEOUSLY DISTILLATIVELY REMOVING 6- AMINOCAPRONITRILE AND ADIPONITRILE INTO SEPARATE FRACTIONS IS CHARACTERIZED BY BASE OF COLUMN TEMPERATURES BELOW 185? IN STEPS D1) OR C2).(FIGURE 1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19832529A DE19832529A1 (en) | 1998-07-20 | 1998-07-20 | Production of 6-amino-capronitrile and hexamethylene diamine from adiponitrile involves work-up by distillation with final recovery of adiponitrile |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MY125174A true MY125174A (en) | 2006-07-31 |
Family
ID=7874645
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MYPI99003039A MY125174A (en) | 1998-07-20 | 1999-07-19 | Improved process for coproduction of 6-aminocapronitrile and hexamethylenediamine. |
Country Status (15)
| Country | Link |
|---|---|
| EP (1) | EP1098869B1 (en) |
| JP (1) | JP2002521356A (en) |
| KR (1) | KR20010071989A (en) |
| CN (1) | CN1310701A (en) |
| AR (1) | AR019432A1 (en) |
| AT (1) | ATE251112T1 (en) |
| AU (1) | AU5029899A (en) |
| BR (1) | BR9912284A (en) |
| CA (1) | CA2337858A1 (en) |
| DE (2) | DE19832529A1 (en) |
| ES (1) | ES2211125T3 (en) |
| ID (1) | ID27066A (en) |
| MY (1) | MY125174A (en) |
| TW (1) | TW467882B (en) |
| WO (1) | WO2000005191A1 (en) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19839338A1 (en) | 1998-08-28 | 2000-03-02 | Basf Ag | Improved process for the simultaneous production of 6-aminocapronitrile and hexamethylenediamine |
| US6248926B1 (en) * | 2000-10-26 | 2001-06-19 | E. I. Du Pont De Nemours And Company | Recovery of hexamethylenediamine (HMD) with low polarographically reducible impurities (PRI) from mixtures of HMD, aminocapronitirle and PRI |
| FR2857965B1 (en) † | 2003-07-25 | 2005-08-26 | Rhodia Polyamide Intermediates | PROCESS FOR MANUFACTURING AND SEPARATING DINITRIL COMPOUNDS |
| FR2902425B1 (en) * | 2006-06-20 | 2008-07-18 | Rhodia Recherches & Tech | PROCESS FOR PRODUCING PRIMARY DIAMINS |
| EP2459515B1 (en) | 2009-07-31 | 2015-08-19 | Dow Global Technologies LLC | Process for reductive amination of aliphatic cyanoaldehydes to aliphatic diamines |
| CN104923240B (en) * | 2015-06-03 | 2018-07-31 | 湘潭大学 | A kind of nickel-base catalyst, preparation method and the application of sepiolite supported bimetallic-modified |
| CN109821551A (en) * | 2019-02-14 | 2019-05-31 | 上海释颉化工技术合伙企业(有限合伙) | Unsupported porous metal catalyst, preparation method and application thereof |
| CN111672526B (en) * | 2020-06-10 | 2023-07-14 | 江苏扬农化工集团有限公司 | The preparation method of the catalyst for the synthesis of hexamethylenediamine intermediate 6-aminocapronitrile and the synthetic method of 6-aminocapronitrile |
| CN113072451B (en) * | 2021-04-14 | 2023-10-24 | 江苏扬农化工集团有限公司 | Method for recycling hexamethylenediamine key intermediate reaction wastewater |
| CN116943549A (en) * | 2022-04-19 | 2023-10-27 | 中国石油天然气股份有限公司 | Method and production system for synthesizing hexamethylenediamine by hydrogenation of adiponitrile |
| CN117986124A (en) * | 2022-10-28 | 2024-05-07 | 中国石油化工股份有限公司 | Method for catalyzing the aminolysis of bis(hexamethylene)triamine |
| CN116217405A (en) * | 2022-12-16 | 2023-06-06 | 中触媒新材料股份有限公司 | Method for preparing hexamethylenediamine by hydrogenation of hexamethylenediamine intermediate based on iron catalyst |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19548289A1 (en) * | 1995-12-22 | 1997-06-26 | Basf Ag | Process for the simultaneous production of caprolactam and hexamethylenediamine |
| DE19636766A1 (en) * | 1996-09-10 | 1998-03-12 | Basf Ag | Process for the simultaneous production of 6-aminocapronitrile and hexamethylenediamine |
-
1998
- 1998-07-20 DE DE19832529A patent/DE19832529A1/en not_active Withdrawn
-
1999
- 1999-07-02 EP EP99934555A patent/EP1098869B1/en not_active Revoked
- 1999-07-02 JP JP2000561148A patent/JP2002521356A/en not_active Withdrawn
- 1999-07-02 WO PCT/EP1999/004583 patent/WO2000005191A1/en not_active Ceased
- 1999-07-02 ID IDW20010161A patent/ID27066A/en unknown
- 1999-07-02 CA CA002337858A patent/CA2337858A1/en not_active Abandoned
- 1999-07-02 ES ES99934555T patent/ES2211125T3/en not_active Expired - Lifetime
- 1999-07-02 BR BR9912284-7A patent/BR9912284A/en not_active IP Right Cessation
- 1999-07-02 AT AT99934555T patent/ATE251112T1/en not_active IP Right Cessation
- 1999-07-02 AU AU50298/99A patent/AU5029899A/en not_active Abandoned
- 1999-07-02 KR KR1020017000832A patent/KR20010071989A/en not_active Ceased
- 1999-07-02 DE DE59907216T patent/DE59907216D1/en not_active Expired - Lifetime
- 1999-07-02 CN CN99808945A patent/CN1310701A/en active Pending
- 1999-07-19 MY MYPI99003039A patent/MY125174A/en unknown
- 1999-07-20 TW TW088112315A patent/TW467882B/en not_active IP Right Cessation
- 1999-07-20 AR ARP990103558A patent/AR019432A1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ES2211125T3 (en) | 2004-07-01 |
| ID27066A (en) | 2001-02-22 |
| EP1098869A1 (en) | 2001-05-16 |
| BR9912284A (en) | 2001-04-17 |
| ATE251112T1 (en) | 2003-10-15 |
| DE59907216D1 (en) | 2003-11-06 |
| CN1310701A (en) | 2001-08-29 |
| CA2337858A1 (en) | 2000-02-03 |
| EP1098869B1 (en) | 2003-10-01 |
| WO2000005191A1 (en) | 2000-02-03 |
| KR20010071989A (en) | 2001-07-31 |
| JP2002521356A (en) | 2002-07-16 |
| AU5029899A (en) | 2000-02-14 |
| TW467882B (en) | 2001-12-11 |
| AR019432A1 (en) | 2002-02-20 |
| DE19832529A1 (en) | 2000-01-27 |
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