MY143553A - PREPARATION OF CATALYTICALLY ACTIVE MULTIELEMENT OXIDE MATERIALS WHICH CONTAIN AT LEAST ONE THE ELEMENTS Nb AND W AND THE ELEMENTS Mo, V, Cu - Google Patents

PREPARATION OF CATALYTICALLY ACTIVE MULTIELEMENT OXIDE MATERIALS WHICH CONTAIN AT LEAST ONE THE ELEMENTS Nb AND W AND THE ELEMENTS Mo, V, Cu

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Publication number
MY143553A
MY143553A MYPI20094284A MYPI20094284A MY143553A MY 143553 A MY143553 A MY 143553A MY PI20094284 A MYPI20094284 A MY PI20094284A MY PI20094284 A MYPI20094284 A MY PI20094284A MY 143553 A MY143553 A MY 143553A
Authority
MY
Malaysia
Prior art keywords
elements
catalytically active
oxide materials
contain
preparation
Prior art date
Application number
MYPI20094284A
Inventor
Martin Dr Dieterle
Hartmut Prof Dr Hibst
Wolfgang Juergen Dr Poepel
Jochen Dr Petzoldt
Klaus Joachim Dr Mueller-Engel
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE2003125488 external-priority patent/DE10325488A1/en
Priority claimed from DE10360058A external-priority patent/DE10360058A1/en
Application filed by Basf Ag filed Critical Basf Ag
Publication of MY143553A publication Critical patent/MY143553A/en

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/20—Vanadium, niobium or tantalum
    • B01J23/22—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/887—Molybdenum containing in addition other metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/8877—Vanadium, tantalum, niobium or polonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/888—Tungsten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/888—Tungsten
    • B01J23/8885—Tungsten containing also molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/19—Catalysts containing parts with different compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B01J8/10—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/23—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
    • C07C51/235—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00389—Controlling the temperature using electric heating or cooling elements
    • B01J2208/00407—Controlling the temperature using electric heating or cooling elements outside the reactor bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00193—Sensing a parameter
    • B01J2219/00195—Sensing a parameter of the reaction system
    • B01J2219/002—Sensing a parameter of the reaction system inside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/887—Molybdenum containing in addition other metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/8876—Arsenic, antimony or bismuth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0221—Coating of particles
    • B01J37/0223—Coating of particles by rotation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)

Abstract

Disclosed is a method for producing catalytically active multielement oxide materials containing at least one of the elements Nb and W as well as elements Mo, V, and Cu. According to the inventive method, an intimate dry mixture containing ammonium ions is produced and is thermally treated at a raised temperature in an atmosphere that is low in molecular oxygen. A partial quantity of the ammonium ions contained in the intimate dry mixture is decomposed so as to release ammonia while the oxygen concentration of the thermal treatment atmosphere is increased in the course of the thermal treatment.
MYPI20094284A 2003-06-04 2004-05-20 PREPARATION OF CATALYTICALLY ACTIVE MULTIELEMENT OXIDE MATERIALS WHICH CONTAIN AT LEAST ONE THE ELEMENTS Nb AND W AND THE ELEMENTS Mo, V, Cu MY143553A (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US47548803P 2003-06-04 2003-06-04
DE2003125488 DE10325488A1 (en) 2003-06-04 2003-06-04 Preparing a multielement oxide material useful as catalyst active material, by thermally treating dry blend of ammonium ions and elemental components of oxide material, other than oxygen in atmosphere having low content of molecular oxygen
US53061703P 2003-12-19 2003-12-19
DE10360058A DE10360058A1 (en) 2003-12-19 2003-12-19 Preparing multi-oxide catalyst containing niobium, tungsten, molybdenum, vanadium and copper, involves heating ammonium-containing mixture to remove ammonia in controlled atmosphere

Publications (1)

Publication Number Publication Date
MY143553A true MY143553A (en) 2011-05-31

Family

ID=33514766

Family Applications (2)

Application Number Title Priority Date Filing Date
MYPI20094284A MY143553A (en) 2003-06-04 2004-05-20 PREPARATION OF CATALYTICALLY ACTIVE MULTIELEMENT OXIDE MATERIALS WHICH CONTAIN AT LEAST ONE THE ELEMENTS Nb AND W AND THE ELEMENTS Mo, V, Cu
MYPI20041938A MY140438A (en) 2003-06-04 2004-05-20 Preparation of catalytically active multielement oxide materials which contain at least one of the elements nb and w and the elements mo, v and cu

Family Applications After (1)

Application Number Title Priority Date Filing Date
MYPI20041938A MY140438A (en) 2003-06-04 2004-05-20 Preparation of catalytically active multielement oxide materials which contain at least one of the elements nb and w and the elements mo, v and cu

Country Status (6)

Country Link
EP (1) EP1633478B1 (en)
JP (1) JP4488244B2 (en)
KR (1) KR100975474B1 (en)
AT (1) ATE516082T1 (en)
MY (2) MY143553A (en)
WO (1) WO2004108284A1 (en)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4933736B2 (en) * 2005-02-02 2012-05-16 三菱レイヨン株式会社 Catalyst for producing methacrylic acid, method for producing the same, and method for producing methacrylic acid
DE102007010422A1 (en) * 2007-03-01 2008-09-04 Basf Se Preparation of a catalyst, useful in the heterogeneously catalyzed partial gas phase oxidation of acrolein to acrylic acid, comprises attaching one of the active mass to the surface of the carrier body with the help of a binding agent
TW200948474A (en) 2008-04-09 2009-12-01 Basf Se Coated catalysts comprising a multimetal oxide comprising molybdenum
DE102013202048A1 (en) 2013-02-07 2013-04-18 Basf Se Preparing catalytically active composition useful for preparing a catalyst, comprises e.g. thermally treating geometrical precursor bodies formed by a mixture obtained by uniformly mixing e.g. a spray-dried powder and molybdenum oxide
JP5455099B1 (en) 2013-09-13 2014-03-26 大日本印刷株式会社 Metal plate, metal plate manufacturing method, and mask manufacturing method using metal plate
JP5516816B1 (en) 2013-10-15 2014-06-11 大日本印刷株式会社 Metal plate, method for producing metal plate, and method for producing vapor deposition mask using metal plate
JP5641462B1 (en) 2014-05-13 2014-12-17 大日本印刷株式会社 Metal plate, metal plate manufacturing method, and mask manufacturing method using metal plate
CN114774854B (en) 2015-02-10 2024-09-06 大日本印刷株式会社 Metal plate and method for manufacturing vapor deposition mask
CN106302215A (en) * 2016-08-30 2017-01-04 华为技术有限公司 A kind of method and device E-Packeted
EP3770145A1 (en) 2019-07-24 2021-01-27 Basf Se A process for the continuous production of either acrolein or acrylic acid as the target product from propene
KR20230002897A (en) 2020-04-21 2023-01-05 바스프 에스이 Process for preparing catalytically active multi-element oxides containing the elements Mo, W, V and Cu
KR102876188B1 (en) 2020-09-03 2025-10-27 가부시키가이샤 닛폰 쇼쿠바이 Catalyst for producing acrylic acid and method for producing the same, and method for producing acrylic acid
CN116490275A (en) 2020-10-29 2023-07-25 巴斯夫欧洲公司 Method for preparing core-shell catalyst
JP2025541831A (en) 2022-12-07 2025-12-23 ベーアーエスエフ・エスエー Process for producing catalytically active multi-element oxides containing the elements Mo, W, V, Cu, and Sb
WO2025125092A1 (en) * 2023-12-14 2025-06-19 Basf Se Process for producing a catalytically active multi-element oxide containing the elements mo, w, v, cu and sb
WO2026017456A1 (en) 2024-07-15 2026-01-22 Basf Se Method for producing a catalyst, involving a water treatment process

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4111983A (en) * 1973-10-18 1978-09-05 Union Carbide Corporation Oxidation of unsaturated aldehydes to unsaturated acids
IT1160321B (en) 1978-12-12 1987-03-11 Euteco Spa CATALYSTS FOR THE OXIDATION OF ACROLEIN TO ACRYLIC ACID
DE4335973A1 (en) * 1993-10-21 1995-04-27 Basf Ag Process for the preparation of catalytically active multimetal oxide compositions containing as basic constituents the elements V and Mo in oxidic form
DE10046928A1 (en) 2000-09-21 2002-04-11 Basf Ag Process for the preparation of multimetal oxide materials

Also Published As

Publication number Publication date
KR20060021343A (en) 2006-03-07
MY140438A (en) 2009-12-31
ATE516082T1 (en) 2011-07-15
EP1633478B1 (en) 2011-07-13
JP4488244B2 (en) 2010-06-23
JP2006526495A (en) 2006-11-24
KR100975474B1 (en) 2010-08-11
EP1633478A1 (en) 2006-03-15
WO2004108284A1 (en) 2004-12-16

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