MY163217A - Reactor for carrying out autothermal gas-phase dehydration - Google Patents

Reactor for carrying out autothermal gas-phase dehydration

Info

Publication number
MY163217A
MY163217A MYPI2013002303A MYPI2013002303A MY163217A MY 163217 A MY163217 A MY 163217A MY PI2013002303 A MYPI2013002303 A MY PI2013002303A MY PI2013002303 A MYPI2013002303 A MY PI2013002303A MY 163217 A MY163217 A MY 163217A
Authority
MY
Malaysia
Prior art keywords
reactor
carrying
gas
phase dehydration
area
Prior art date
Application number
MYPI2013002303A
Inventor
Gerhard Olbert
Ulrike Wegerle
- Ing Kolios Grigorios Dr
-Ing Kostova Albena Dr
Jasmina Kessel
Alexander Weck
Alireza Rezai
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MY163217A publication Critical patent/MY163217A/en

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/248—Reactors comprising multiple separated flow channels
    • B01J19/2485—Monolithic reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/56—Foraminous structures having flow-through passages or channels, e.g. grids or three-dimensional [3D] monoliths
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/42—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with a hydrogen acceptor
    • C07C5/48—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with a hydrogen acceptor with oxygen as an acceptor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/2402—Monolithic-type reactors
    • B01J2219/2409—Heat exchange aspects
    • B01J2219/2411—The reactant being in indirect heat exchange with a non reacting heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/2402—Monolithic-type reactors
    • B01J2219/2409—Heat exchange aspects
    • B01J2219/2416—Additional heat exchange means, e.g. electric resistance heater, coils
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/2402—Monolithic-type reactors
    • B01J2219/2418—Feeding means
    • B01J2219/2419—Feeding means for the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/2402—Monolithic-type reactors
    • B01J2219/2422—Mixing means, e.g. fins or baffles attached to the monolith or placed in the channel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/2402—Monolithic-type reactors
    • B01J2219/2441—Other constructional details
    • B01J2219/2443—Assembling means of monolith modules
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/90—Regeneration or reactivation
    • B01J23/96—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/10—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst using elemental hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/12—Treating with free oxygen-containing gas
    • B01J38/14—Treating with free oxygen-containing gas with control of oxygen content in oxidation gas
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2521/00—Catalysts comprising the elements, oxides or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium or hafnium
    • C07C2521/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2521/00—Catalysts comprising the elements, oxides or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium or hafnium
    • C07C2521/14—Silica and magnesia
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2521/00—Catalysts comprising the elements, oxides or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium or hafnium
    • C07C2521/16—Clays or other mineral silicates
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2523/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00
    • C07C2523/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00 of noble metals
    • C07C2523/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00 of noble metals combined with metals, oxides or hydroxides provided for in groups C07C2523/02 - C07C2523/36
    • C07C2523/56—Platinum group metals
    • C07C2523/62—Platinum group metals with gallium, indium, thallium, germanium, tin or lead
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2527/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • C07C2527/20—Carbon compounds
    • C07C2527/22—Carbides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2527/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • C07C2527/20—Carbon compounds
    • C07C2527/22—Carbides
    • C07C2527/224—Silicon carbide
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2527/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • C07C2527/24—Nitrogen compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Catalysts (AREA)
  • Hydrogen, Water And Hydrids (AREA)

Abstract

THE INVENTION RELATES TO A REACTOR (1) IN THE FORM OF A HORIZONTAL CYLINDER (3) FOR CARRYING OUT AUTOTHERMAL GAS PHASE DEHYDRATION OF A HYDROCARBON-CONTAINING GAS FLOW (2) WITH AN OXYGEN-CONTAINING GAS FLOW (3), YIELDING A REACTION GAS MIXTURE, AT A HETEROGENEOUS CATALYST DESIGNED AS A MONOLITH (4), WHEREIN THE INNER CHAMBER OF THE REACTOR (1) IS DIVIDED BY A REMOVABLE, CIRCULAR CYLINDRICAL OR PRISMATIC HOUSING G, WHICH IS DISPOSED IN THE LONGITUDINAL DIRECTION OF THE REACTOR (1) AND IS GAS-TIGHT IN THE CIRCUMFERENTIAL DIRECTION, INTO AN INNER AREA A HAVING ONE OR MORE CATALYTICALLY ACTIVE ZONES (5), IN EACH OF WHICH A PACKAGE OF MONOLITHS (4) STACKED ON EACH OTHER, ADJACENT TO EACH OTHER, AND ARRANGED ONE BEHIND THE OTHER IS PROVIDED, A MIXING ZONE (6) HAVING FIXED INSTALLED FIXTURES BEING PROVIDED IN FRONT OF EACH ACTIVE ZONE (5), AND INTO AN OUTER AREA B DISPOSED COAXIALLY TO THE INNER AREA A, AND WHEREIN A HEAT EXCHANGER (12) CONNECTED TO THE HOUSING G IS PROVIDED AT AN END OF THE REACTOR, CHARACTERIZED IN THAT AN INERT GAS IS SUPPLIED TO THE OUTER AREA B. (FIGURE 1)
MYPI2013002303A 2010-12-21 2011-12-13 Reactor for carrying out autothermal gas-phase dehydration MY163217A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10196216 2010-12-21
EP11168408 2011-06-01
EP11190117 2011-11-22

Publications (1)

Publication Number Publication Date
MY163217A true MY163217A (en) 2017-08-30

Family

ID=45422130

Family Applications (1)

Application Number Title Priority Date Filing Date
MYPI2013002303A MY163217A (en) 2010-12-21 2011-12-13 Reactor for carrying out autothermal gas-phase dehydration

Country Status (7)

Country Link
EP (1) EP2654941B1 (en)
JP (1) JP5968334B2 (en)
KR (1) KR20130130791A (en)
CN (1) CN103391812B (en)
EA (1) EA024781B1 (en)
MY (1) MY163217A (en)
WO (1) WO2012084609A1 (en)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MY163298A (en) * 2011-08-02 2017-09-15 Basf Se Reactor for carrying out autothermal gas-phase dehydrogenation
JP6109169B2 (en) * 2011-08-02 2017-04-05 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ Continuous process for carrying out autothermal gas phase dehydrogenation
MA37710B1 (en) * 2012-07-05 2016-05-31 Basf Se Reactor enabling the implementation of an exothermic reaction in the gas phase
US8790611B2 (en) 2012-07-05 2014-07-29 Basf Se Reactor for carrying out an exothermic reaction in the gas phase
WO2014090841A2 (en) * 2012-12-12 2014-06-19 Basf Se Reactor for performing an autothermal gas-phase dehydrogenation
US9611191B2 (en) 2012-12-12 2017-04-04 Basf Se Reactor for carrying out an autothermal gas-phase dehydrogenation
US9616406B2 (en) * 2013-02-14 2017-04-11 Basf Se Installing monoliths in a reactor for conducting heterogeneously catalyzed gas phase reactions
EP2956236A1 (en) 2013-02-14 2015-12-23 Basf Se Method for mounting monoliths in a reactor for carrying out heterogeneously catalyzed gas-phase reactions
WO2015104397A1 (en) * 2014-01-13 2015-07-16 Basf Se Method of starting up a reactor for the oxidative dehydrogenation of n-butenes
DK2993323T3 (en) 2014-09-04 2017-10-16 3M Innovative Properties Co MOUNTING FOR A POLLUTION CONTROL OR CHEMICAL REACTOR
CN104888664B (en) * 2015-04-22 2017-11-10 华东理工大学 A kind of self-heating hydrogen supply device and its application
WO2018024740A1 (en) 2016-08-02 2018-02-08 Basf Se Reactor for carrying out the autothermal gas phase dehydrogenation of a hydrocarbon-containing gas flow
EP3801871B1 (en) 2018-05-31 2026-03-04 Topsoe A/S Endothermic reactions heated by resistance heating
EP3574991A1 (en) 2018-05-31 2019-12-04 Haldor Topsøe A/S Steam reforming heated by resistance heating
CN121847002A (en) 2019-04-08 2026-04-14 托普索公司 Chemical synthesis equipment
CN110575809B (en) * 2019-09-27 2024-06-04 江苏扬农化工集团有限公司 Reactor and method for continuously synthesizing epichlorohydrin
CA3153229A1 (en) 2019-10-01 2021-04-08 Haldor Topsoe A/S Synthesis gas on demand
JP7840261B2 (en) 2019-10-01 2026-04-03 トプソー・アクチエゼルスカベット Methanol to on-demand hydrogen
MX2022003308A (en) 2019-10-01 2022-04-12 Haldor Topsoe As CYANIDE ON DEMAND.
CN119660676A (en) 2019-10-01 2025-03-21 托普索公司 On demand production of synthesis gas from methanol
KR20220075347A (en) 2019-10-01 2022-06-08 할도르 토프쉐 에이/에스 Customized hydrogen from ammonia
US12246298B2 (en) 2019-10-01 2025-03-11 Haldor Topsøe A/S Offshore reforming installation or vessel
BR112022009054A2 (en) 2019-11-12 2022-08-09 Haldor Topsoe As ELECTRIC STEAM CRACKER
EP3974793B1 (en) * 2020-09-25 2024-06-26 L'air Liquide, Société Anonyme Pour L'Étude Et L'exploitation Des Procédés Georges Claude Measuring device for measuring axial temperature profiles in a reactor tube
KR20240005808A (en) * 2021-06-02 2024-01-12 엑손모빌 케미칼 패턴츠 인코포레이티드 Methods for catalyst regeneration and alkane and/or alkyl aromatic hydrocarbon upgrading

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US4452760A (en) * 1982-01-18 1984-06-05 The M. W. Kellogg Company Horizontal ammonia converter
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DE102006060509A1 (en) * 2006-12-19 2008-06-26 Basf Se Reactor for continuous oxide hydrogenation of feed gas flow of saturated hydrocarbons on moving catalyst bed, comprises four reactor sections, which are separated from each other and split into sub-sections by alternating deflector plates
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Also Published As

Publication number Publication date
CN103391812B (en) 2015-04-08
WO2012084609A1 (en) 2012-06-28
JP5968334B2 (en) 2016-08-10
EP2654941B1 (en) 2014-11-26
CN103391812A (en) 2013-11-13
KR20130130791A (en) 2013-12-02
EA201390915A1 (en) 2014-02-28
EA024781B1 (en) 2016-10-31
EP2654941A1 (en) 2013-10-30
JP2014511342A (en) 2014-05-15

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