MY171361A - Method for producing a methionine salt - Google Patents

Method for producing a methionine salt

Info

Publication number
MY171361A
MY171361A MYPI2014000554A MYPI2014000554A MY171361A MY 171361 A MY171361 A MY 171361A MY PI2014000554 A MYPI2014000554 A MY PI2014000554A MY PI2014000554 A MYPI2014000554 A MY PI2014000554A MY 171361 A MY171361 A MY 171361A
Authority
MY
Malaysia
Prior art keywords
methionine salt
producing
relates
methylmercaptopropionaldehyde
mmp
Prior art date
Application number
MYPI2014000554A
Inventor
Hans Joachim Hasselbach
Martin Korfer
Christof P Gruner
Franz H Hanrath
Jurgen Stock
Jignesh Gangadwala
Horst Krull
Original Assignee
Evonik Operations Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Operations Gmbh filed Critical Evonik Operations Gmbh
Publication of MY171361A publication Critical patent/MY171361A/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/26—Separation; Purification; Stabilisation; Use of additives
    • C07C319/28—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/50—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton
    • C07C323/51—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C323/57—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C323/58—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups with amino groups bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/66—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D233/72—Two oxygen atoms, e.g. hydantoin
    • C07D233/76—Two oxygen atoms, e.g. hydantoin with substituted hydrocarbon radicals attached to the third ring carbon atom
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention relates to a method of production of a methionine salt, in particular the production of a methionine salt starting from the precursors 3-methylmercaptopropionaldehyde (MMP) and hydrogen cyanide (HCN) or starting from at least one component that can be prepared from these raw materials such as methylmercaptopropionaldehyde-cyanohydrin (MMP-CN). In particular the invention relates to the alkaline hydrolysis of 5-(2-methylmercapto)-hydantoin in a column. The invention further relates to a reaction system suitable for this method, which comprises a reactive-rectification column and the use of the reaction system. (No suitable figure)
MYPI2014000554A 2011-08-30 2012-08-23 Method for producing a methionine salt MY171361A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US201161529013P 2011-08-30 2011-08-30

Publications (1)

Publication Number Publication Date
MY171361A true MY171361A (en) 2019-10-10

Family

ID=46717855

Family Applications (1)

Application Number Title Priority Date Filing Date
MYPI2014000554A MY171361A (en) 2011-08-30 2012-08-23 Method for producing a methionine salt

Country Status (11)

Country Link
US (2) US9023284B2 (en)
EP (1) EP2750775B1 (en)
JP (1) JP6120854B2 (en)
KR (1) KR101944569B1 (en)
CN (1) CN103764240B (en)
BR (1) BR112014003602B1 (en)
MX (1) MX2014002250A (en)
MY (1) MY171361A (en)
RU (1) RU2618042C2 (en)
SG (1) SG2014012819A (en)
WO (1) WO2013030068A2 (en)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010064250A1 (en) 2010-12-28 2012-06-28 Evonik Degussa Gmbh Process for the preparation of methylmercaptopropionaldehyde
EP2678312B1 (en) 2011-02-23 2017-10-11 Evonik Degussa GmbH Method for producing 2-hydroxy-4-(methylthio)butanenitrile from 3-(methylthio)propanal and hydrogen cyanide
DE102011081828A1 (en) 2011-08-30 2013-02-28 Evonik Degussa Gmbh Process for the reaction of methylmercaptopropionaldehyde from crude acrolein and crude methylmercaptan
EP2679579A1 (en) 2012-06-27 2014-01-01 Evonik Industries AG Integrated method for producing acrolein and 3-Methylmercapto propionaldehyde
CN103408498B (en) * 2013-08-28 2016-02-17 重庆紫光化工股份有限公司 Thick hydrocyanic acid gas is utilized to prepare 5-(2-methylmercaptoethyl) method of-glycolylurea
EP2848607A1 (en) 2013-09-17 2015-03-18 Evonik Industries AG Method for extracting methionine
CN106714923B (en) * 2014-09-24 2020-04-24 国际壳牌研究有限公司 Method and device for preparing alkanediol
EP3475248B1 (en) 2016-06-27 2020-08-05 Evonik Operations GmbH Granules containing dipeptide
US10919848B2 (en) 2017-05-15 2021-02-16 Evonik Operations Gmbh Process for preparing methionine
EP3431465A1 (en) 2017-07-21 2019-01-23 Evonik Degussa GmbH Process for preparing methionine
EP3404018A1 (en) 2017-05-15 2018-11-21 Evonik Degussa GmbH Process for preparing methionine
EP3406593A1 (en) 2017-05-24 2018-11-28 Evonik Degussa GmbH Method for manufacturing methionine
EP3461803A1 (en) 2017-10-02 2019-04-03 Evonik Degussa GmbH Method for the production of granules containing dipeptide
FR3123068B1 (en) 2021-05-20 2024-05-10 Adisseo France Sas PROCESS FOR MANUFACTURING METHIONINE
CN114685603A (en) * 2022-05-07 2022-07-01 宁夏紫光天化蛋氨酸有限责任公司 Method for preparing methionine

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4235295A1 (en) * 1992-10-20 1994-04-21 Degussa Continuously feasible process for the preparation of methionine or methionine derivatives
DE19547236A1 (en) 1995-12-18 1997-07-03 Degussa Process for the preparation of D, L-methionine or its salt
DE19548538C2 (en) 1995-12-23 1997-12-18 Degussa Process for recovering 2-hydroxy-4-methylthiobutyric acid (MHA)
EP0907393A1 (en) * 1996-05-24 1999-04-14 Basf Aktiengesellschaft Column and process for deodorising dispersions
DE69709526T2 (en) 1996-10-31 2002-08-01 Sumitomo Chemical Co., Ltd. Process for the production of methionine
DE19707380A1 (en) 1997-02-25 1998-08-27 Degussa Process for producing a free-flowing animal feed supplement based on methionine salt and the granules obtainable in this way
DE19735332A1 (en) 1997-08-14 1999-02-18 Degussa Aliphatic alkanals with improved storage stability and process for improving storage stability
DE19822099A1 (en) 1998-05-16 1999-11-18 Degussa Process for the preparation of aqueous sodium methioninate solutions and use of these solutions for the production of granules
WO2001060788A1 (en) * 2000-02-15 2001-08-23 Rhone-Poulenc Animal Nutrition Process for the production of methionine
RU2230593C2 (en) * 2000-07-25 2004-06-20 Юоп Ллк Rectifying column containing a panel of fractionating trays, a complete set of fractionating trays for installation in a column of fractional distillation and a method of installation of the fractionating trays in the column of fractional distillation
DE10160358A1 (en) 2001-12-08 2003-06-18 Degussa Process for the production of methionine
DE10238212A1 (en) 2002-08-21 2004-03-04 Degussa Ag Process for the preparation of α-amino acids by hydrolysis of hydantoins at elevated pressure and temperature
DE10359636A1 (en) * 2003-12-18 2005-07-28 Degussa Ag Process for the separation of methylmercaptan from reaction mixtures
EP1564208B1 (en) 2004-02-14 2011-05-18 Evonik Degussa GmbH Process for producing methionine
DE102004035465A1 (en) * 2004-07-22 2006-02-16 Degussa Ag Process for the purification of CO2 gas streams
JP4792754B2 (en) 2005-01-31 2011-10-12 住友化学株式会社 Method for removing ammonia from a solution containing an ammonium salt
TWI327998B (en) * 2006-01-26 2010-08-01 Asahi Kasei Chemicals Corp Industrial process for production of diol
JP2009292795A (en) 2008-06-09 2009-12-17 Sumitomo Chemical Co Ltd Method for producing methionine
DE102008040544A1 (en) 2008-07-18 2010-01-21 Evonik Degussa Gmbh Reaction vessel and method of use
JP5307512B2 (en) 2008-11-07 2013-10-02 住友化学株式会社 Method for producing methionine
DE102010064250A1 (en) 2010-12-28 2012-06-28 Evonik Degussa Gmbh Process for the preparation of methylmercaptopropionaldehyde
EP2678312B1 (en) 2011-02-23 2017-10-11 Evonik Degussa GmbH Method for producing 2-hydroxy-4-(methylthio)butanenitrile from 3-(methylthio)propanal and hydrogen cyanide
SG192908A1 (en) 2011-02-23 2013-09-30 Evonik Degussa Gmbh Storage-stable 2-hydroxy-4-(methylthio) butyric acid nitrile
DE102011081828A1 (en) 2011-08-30 2013-02-28 Evonik Degussa Gmbh Process for the reaction of methylmercaptopropionaldehyde from crude acrolein and crude methylmercaptan

Also Published As

Publication number Publication date
JP6120854B2 (en) 2017-04-26
CN103764240A (en) 2014-04-30
WO2013030068A2 (en) 2013-03-07
US9023284B2 (en) 2015-05-05
MX2014002250A (en) 2014-04-25
KR101944569B1 (en) 2019-01-31
RU2618042C2 (en) 2017-05-02
BR112014003602B1 (en) 2021-05-18
EP2750775A2 (en) 2014-07-09
KR20140070538A (en) 2014-06-10
US20130231501A1 (en) 2013-09-05
WO2013030068A4 (en) 2013-12-27
US20150175535A1 (en) 2015-06-25
US9403764B2 (en) 2016-08-02
CN103764240B (en) 2016-04-20
JP2014529615A (en) 2014-11-13
WO2013030068A3 (en) 2013-11-07
SG2014012819A (en) 2014-06-27
RU2014111964A (en) 2015-10-10
EP2750775B1 (en) 2020-12-09
BR112014003602A2 (en) 2017-03-14

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