MY176013A - A method for treating free fatty acids of crude plant-derived oils to obtain fatty acid alkyl esters - Google Patents
A method for treating free fatty acids of crude plant-derived oils to obtain fatty acid alkyl estersInfo
- Publication number
- MY176013A MY176013A MYUI2012700051A MYUI2012700051A MY176013A MY 176013 A MY176013 A MY 176013A MY UI2012700051 A MYUI2012700051 A MY UI2012700051A MY UI2012700051 A MYUI2012700051 A MY UI2012700051A MY 176013 A MY176013 A MY 176013A
- Authority
- MY
- Malaysia
- Prior art keywords
- fatty acid
- oil
- acid alkyl
- alcohol
- crude plant
- Prior art date
Links
- 235000014113 dietary fatty acids Nutrition 0.000 title abstract 5
- 229930195729 fatty acid Natural products 0.000 title abstract 5
- 239000000194 fatty acid Substances 0.000 title abstract 5
- 235000021588 free fatty acids Nutrition 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 2
- 239000003921 oil Substances 0.000 title 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract 6
- 239000000203 mixture Substances 0.000 abstract 4
- 239000003377 acid catalyst Substances 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Fats And Perfumes (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The present invention relates to a method for reducing free fatty acids content in crude plant-derived oil, comprising esterifying and transesterifying the crude plant-derived oil, and characterized by the steps of: heating the crude plant-derived oil; mixing an alcohol comprising 1-4 carbon chain length with the heated oil at a molar ratio of the alcohol to the heated oil of 8: 1 to 20: 1; reacting solid sulphonic acid catalyst with the heated oil containing the alcohol to form treated oil having free fatty acids content of maximum 1% by weight at a temperature in a range of 40-70?C for a time in a range of 3-150 minutes; removing excess alcohol and the solid sulphonic acid catalyst from the treated oil; wherein said catalyst is recycled for further free fatty acid reduction in a fresh crude plant-derived oil; reacting the alkali catalyst and the alcohol with the treated oil to produce a mixture comprising fatty acid alkyl ester and crude glycerol; evaporating the excess alcohol and separating the crude glycerol from the mixture comprising fatty acid alkyl ester; and purifying the mixture comprising fatty acid alkyl ester with water and dehydrating the purified mixture comprising fatty acid alkyl ester.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MYUI2012700051A MY176013A (en) | 2012-03-05 | 2012-03-05 | A method for treating free fatty acids of crude plant-derived oils to obtain fatty acid alkyl esters |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MYUI2012700051A MY176013A (en) | 2012-03-05 | 2012-03-05 | A method for treating free fatty acids of crude plant-derived oils to obtain fatty acid alkyl esters |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MY176013A true MY176013A (en) | 2020-07-21 |
Family
ID=81329792
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MYUI2012700051A MY176013A (en) | 2012-03-05 | 2012-03-05 | A method for treating free fatty acids of crude plant-derived oils to obtain fatty acid alkyl esters |
Country Status (1)
| Country | Link |
|---|---|
| MY (1) | MY176013A (en) |
-
2012
- 2012-03-05 MY MYUI2012700051A patent/MY176013A/en unknown
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