MY185625A - Method of extracting and concentrating phytosterol from palm oil by-product - Google Patents

Method of extracting and concentrating phytosterol from palm oil by-product

Info

Publication number
MY185625A
MY185625A MYPI2015001728A MYPI2015001728A MY185625A MY 185625 A MY185625 A MY 185625A MY PI2015001728 A MYPI2015001728 A MY PI2015001728A MY PI2015001728 A MYPI2015001728 A MY PI2015001728A MY 185625 A MY185625 A MY 185625A
Authority
MY
Malaysia
Prior art keywords
product
phytosterol
solvent
feed material
extracting
Prior art date
Application number
MYPI2015001728A
Inventor
Hasamudin Wan Hassan Wan
Faizah Jalani Nor
Astimar Abd Aziz Dr
Abd Wahab Noorshamsiana
Dr Choo Yuen May Datuk
Hamzah Iskandarshah
Abd Gapor Md Top Dr
Original Assignee
Malaysian Palm Oil Board Mpob
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Malaysian Palm Oil Board Mpob filed Critical Malaysian Palm Oil Board Mpob
Priority to MYPI2015001728A priority Critical patent/MY185625A/en
Priority to PCT/MY2016/000037 priority patent/WO2017003279A2/en
Publication of MY185625A publication Critical patent/MY185625A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J9/00—Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Steroid Compounds (AREA)

Abstract

A method of extracting and concentrating phytosterol from phytosterol-rich by-products (100) is disclosed, wherein the method (100) includes the steps of (a) selecting a feed material (102); (b) subjecting the feed material to a solid-liquid extraction process at a temperature in a range of 35?C to 40?C to yield an extracted product (104); (c) subjecting the extracted product to a reaction process in a 10% ethanolic basic solution(106) at a reflux temperature in a range of 60?C to 80?C for a duration of 30 to 90 minutes; (d) extracting unsaponifiable material by conducting a liquid extraction using non-polar solvent (108); (e) conducting a neutralization process using a non-reacting liquid such as water until neutral pH is obtained (110); and (f) conducting a product purification process via crystallization of product as obtained from step (e) using single solvent wherein ratio between a solvent to the feed material is 10:1 (mass to volume ratio) and the feed material to basic reactant is 2:1 (mass ratio), further wherein a solvent used is a hydrocarbon solvent at a minimum 5 extraction cycles. Most illustrative drawing is FIG. 1.
MYPI2015001728A 2015-07-02 2015-07-02 Method of extracting and concentrating phytosterol from palm oil by-product MY185625A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
MYPI2015001728A MY185625A (en) 2015-07-02 2015-07-02 Method of extracting and concentrating phytosterol from palm oil by-product
PCT/MY2016/000037 WO2017003279A2 (en) 2015-07-02 2016-06-28 Method of extracting and concentrating phytosterol from palm oil by-product

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
MYPI2015001728A MY185625A (en) 2015-07-02 2015-07-02 Method of extracting and concentrating phytosterol from palm oil by-product

Publications (1)

Publication Number Publication Date
MY185625A true MY185625A (en) 2021-05-26

Family

ID=57609391

Family Applications (1)

Application Number Title Priority Date Filing Date
MYPI2015001728A MY185625A (en) 2015-07-02 2015-07-02 Method of extracting and concentrating phytosterol from palm oil by-product

Country Status (2)

Country Link
MY (1) MY185625A (en)
WO (1) WO2017003279A2 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107383138A (en) * 2017-06-27 2017-11-24 广西南宁桂知科技有限公司 A kind of method that natural phytosterin is extracted from dragon fruit bough
CN108485817B (en) * 2018-06-08 2021-07-23 白山市科学技术研究所 Method for extracting herba Filipendulae extract

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0333472B1 (en) * 1988-03-16 1997-10-08 PALM OIL RESEARCH & DEVELOPMENT BOARD Production of high concentration tocopherols and tocotrienols from palm oil by-products
US20030144536A1 (en) * 2002-01-28 2003-07-31 Forbes Medi-Tech Inc. Process of extracting and purifying phytosterols and phytostanols from tall oil pitch
MY142319A (en) * 2002-08-20 2010-11-15 Malaysian Palm Oil Board Mpob Extraction of palm vitamin e, phytosterols and squalene from palm oil
MY160111A (en) * 2009-07-30 2017-02-28 Chiang Mai Univ System and method for extracting vitamin e from fatty acid distillates
PL2635592T5 (en) * 2010-11-03 2025-09-08 Verbio Se Method for obtaining phytosterols and/or tocopherols from residues after distillation of vegetable oil esters, preferably from residues after distillation of transesterification of vegetable oils

Also Published As

Publication number Publication date
WO2017003279A3 (en) 2017-02-16
WO2017003279A2 (en) 2017-01-05

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