NL1008788C2 - Werkwijze voor het winnen van een 2,3-pyridinedicarbonzuur. - Google Patents

Werkwijze voor het winnen van een 2,3-pyridinedicarbonzuur. Download PDF

Info

Publication number: NL1008788C2
Authority: NL; Netherlands
Prior art keywords: dicarboxylic acid; pyridine dicarboxylic; pyridine; nanofiltration; preparation
Prior art date: 1998-04-02

Application number

NL1008788A

Other languages

English (en)

Dutch (nl)

Inventor

Peter Johannes Dominicus Maas

Veerle Cauwenberg

Franciscus Hendrik P Vergossen

Original Assignee

Dsm Nv

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1998-04-02

Filing date

1998-04-02

Publication date

1999-10-05

1998-04-02 Application filed by Dsm Nv filed Critical Dsm Nv

1998-04-02 Priority to NL1008788A priority Critical patent/NL1008788C2/nl

1999-03-29 Priority to AT99200965T priority patent/ATE221877T1/de

1999-03-29 Priority to DE69902413T priority patent/DE69902413D1/de

1999-03-29 Priority to EP99200965A priority patent/EP0947508B1/de

1999-04-01 Priority to JP11094648A priority patent/JPH11322717A/ja

1999-04-01 Priority to IN379MA1999 priority patent/IN187646B/en

1999-04-01 Priority to CN99106247A priority patent/CN1236777A/zh

1999-04-02 Priority to US09/283,757 priority patent/US6133450A/en

1999-04-02 Priority to CZ991177A priority patent/CZ117799A3/cs

1999-10-05 Application granted granted Critical

1999-10-05 Publication of NL1008788C2 publication Critical patent/NL1008788C2/nl

Links

GJAWHXHKYYXBSV-UHFFFAOYSA-N quinolinic acid Chemical compound OC(=O)C1=CC=CN=C1C(O)=O GJAWHXHKYYXBSV-UHFFFAOYSA-N 0.000 title claims abstract description 84
238000000034 method Methods 0.000 title claims abstract description 42
238000001728 nano-filtration Methods 0.000 claims abstract description 23
238000002360 preparation method Methods 0.000 claims abstract description 14
HPYNZHMRTTWQTB-UHFFFAOYSA-N 2,3-dimethylpyridine Chemical compound CC1=CC=CN=C1C HPYNZHMRTTWQTB-UHFFFAOYSA-N 0.000 claims abstract description 12
SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 claims abstract description 10
239000012452 mother liquor Substances 0.000 claims abstract description 10
239000012141 concentrate Substances 0.000 claims abstract description 5
230000003647 oxidation Effects 0.000 claims description 9
238000007254 oxidation reaction Methods 0.000 claims description 9
239000011541 reaction mixture Substances 0.000 claims description 5
238000011084 recovery Methods 0.000 claims description 5
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims description 4
238000000926 separation method Methods 0.000 claims description 4
LVPMIMZXDYBCDF-UHFFFAOYSA-N isocinchomeronic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)N=C1 LVPMIMZXDYBCDF-UHFFFAOYSA-N 0.000 claims description 2
239000007787 solid Substances 0.000 claims 2
239000011343 solid material Substances 0.000 abstract 1
239000012528 membrane Substances 0.000 description 30
230000014759 maintenance of location Effects 0.000 description 15
239000006227 byproduct Substances 0.000 description 9
PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 description 8
SIOXPEMLGUPBBT-UHFFFAOYSA-N picolinic acid Chemical compound OC(=O)C1=CC=CC=N1 SIOXPEMLGUPBBT-UHFFFAOYSA-N 0.000 description 8
239000012466 permeate Substances 0.000 description 7
239000002994 raw material Substances 0.000 description 5
229960003512 nicotinic acid Drugs 0.000 description 4
235000001968 nicotinic acid Nutrition 0.000 description 4
239000011664 nicotinic acid Substances 0.000 description 4
229940081066 picolinic acid Drugs 0.000 description 4
239000012465 retentate Substances 0.000 description 4
150000003839 salts Chemical class 0.000 description 4
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
239000000919 ceramic Substances 0.000 description 3
239000002131 composite material Substances 0.000 description 3
230000007423 decrease Effects 0.000 description 3
230000004907 flux Effects 0.000 description 3
239000000047 product Substances 0.000 description 3
HNTZKNJGAFJMHQ-UHFFFAOYSA-N 2-methylpyridine-3-carboxylic acid Chemical compound CC1=NC=CC=C1C(O)=O HNTZKNJGAFJMHQ-UHFFFAOYSA-N 0.000 description 2
LMHIBYREWJHKNZ-UHFFFAOYSA-N 3-methylpyridine-2-carboxylic acid Chemical compound CC1=CC=CN=C1C(O)=O LMHIBYREWJHKNZ-UHFFFAOYSA-N 0.000 description 2
241000272194 Ciconiiformes Species 0.000 description 2
238000002425 crystallisation Methods 0.000 description 2
230000008025 crystallization Effects 0.000 description 2
229910052500 inorganic mineral Inorganic materials 0.000 description 2
239000011707 mineral Substances 0.000 description 2
229920002492 poly(sulfone) Polymers 0.000 description 2
238000000746 purification Methods 0.000 description 2
239000002033 PVDF binder Substances 0.000 description 1
239000004952 Polyamide Substances 0.000 description 1
239000004695 Polyether sulfone Substances 0.000 description 1
239000004697 Polyetherimide Substances 0.000 description 1
239000004642 Polyimide Substances 0.000 description 1
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 1
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
238000009825 accumulation Methods 0.000 description 1
239000002253 acid Substances 0.000 description 1
239000003905 agrochemical Substances 0.000 description 1
230000001476 alcoholic effect Effects 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
230000006315 carbonylation Effects 0.000 description 1
238000005810 carbonylation reaction Methods 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
229920002678 cellulose Polymers 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
150000001470 diamides Chemical class 0.000 description 1
150000005690 diesters Chemical class 0.000 description 1
239000003814 drug Substances 0.000 description 1
239000000975 dye Substances 0.000 description 1
238000006056 electrooxidation reaction Methods 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
230000008014 freezing Effects 0.000 description 1
238000007710 freezing Methods 0.000 description 1
239000012510 hollow fiber Substances 0.000 description 1
230000007062 hydrolysis Effects 0.000 description 1
238000006460 hydrolysis reaction Methods 0.000 description 1
238000009434 installation Methods 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
239000000203 mixture Substances 0.000 description 1
150000004767 nitrides Chemical class 0.000 description 1
229910052755 nonmetal Inorganic materials 0.000 description 1
239000007800 oxidant agent Substances 0.000 description 1
230000035699 permeability Effects 0.000 description 1
229920002239 polyacrylonitrile Polymers 0.000 description 1
229920002647 polyamide Polymers 0.000 description 1
229920006393 polyether sulfone Polymers 0.000 description 1
229920001601 polyetherimide Polymers 0.000 description 1
229920001721 polyimide Polymers 0.000 description 1
229920002981 polyvinylidene fluoride Polymers 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
230000000717 retained effect Effects 0.000 description 1
239000002904 solvent Substances 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1
229910052719 titanium Inorganic materials 0.000 description 1
239000010936 titanium Substances 0.000 description 1
238000000108 ultra-filtration Methods 0.000 description 1
238000010626 work up procedure Methods 0.000 description 1
229910052726 zirconium Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/79—Acids; Esters
- C07D213/80—Acids; Esters in position 3

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Pyridine Compounds (AREA)
Separation Using Semi-Permeable Membranes (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)

NL1008788A 1998-04-02 1998-04-02 Werkwijze voor het winnen van een 2,3-pyridinedicarbonzuur. NL1008788C2 (nl)

Priority Applications (9)

Application Number	Priority Date	Filing Date	Title
NL1008788A NL1008788C2 (nl)	1998-04-02	1998-04-02	Werkwijze voor het winnen van een 2,3-pyridinedicarbonzuur.
AT99200965T ATE221877T1 (de)	1998-04-02	1999-03-29	Verfahren zur rückgewinnung von 2,3- pyridindicarbonsäure
DE69902413T DE69902413D1 (de)	1998-04-02	1999-03-29	Verfahren zur Rückgewinnung von 2,3-Pyridindicarbonsäure
EP99200965A EP0947508B1 (de)	1998-04-02	1999-03-29	Verfahren zur Rückgewinnung von 2,3-Pyridindicarbonsäure
JP11094648A JPH11322717A (ja)	1998-04-02	1999-04-01	ピリジン―２，３―ジカルボン酸の回収法
IN379MA1999 IN187646B (de)	1998-04-02	1999-04-01
CN99106247A CN1236777A (zh)	1998-04-02	1999-04-01	回收吡啶－2,3－二羧酸的方法
US09/283,757 US6133450A (en)	1998-04-02	1999-04-02	Process for recovery of pyridine-2,3-dicarboxylic acid
CZ991177A CZ117799A3 (cs)	1998-04-02	1999-04-02	Způsob zpětného získávání kyseliny pyridin-2,3-dikarboxylové

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
NL1008788A NL1008788C2 (nl)	1998-04-02	1998-04-02	Werkwijze voor het winnen van een 2,3-pyridinedicarbonzuur.
NL1008788		1998-04-02

Publications (1)

Publication Number	Publication Date
NL1008788C2 true NL1008788C2 (nl)	1999-10-05

Family

ID=19766881

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL1008788A NL1008788C2 (nl)	1998-04-02	1998-04-02	Werkwijze voor het winnen van een 2,3-pyridinedicarbonzuur.

Country Status (9)

Country	Link
US (1)	US6133450A (de)
EP (1)	EP0947508B1 (de)
JP (1)	JPH11322717A (de)
CN (1)	CN1236777A (de)
AT (1)	ATE221877T1 (de)
CZ (1)	CZ117799A3 (de)
DE (1)	DE69902413D1 (de)
IN (1)	IN187646B (de)
NL (1)	NL1008788C2 (de)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US7795439B2 (en) *	2004-06-25	2010-09-14	Basf Aktiengesellschaft	In-situ treatment of pyridine 2,3-dicarboxylic acid esters with an oxidizing agent
US20100071836A1 (en) *	2008-09-19	2010-03-25	Roy Watson	Sealing of Mica Wnidows for Geiger-Muller Tubes
WO2013036998A1 (en) *	2011-09-13	2013-03-21	The University Of Sydney	Treatment of bone diseases

Citations (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4537971A (en) *	1981-05-06	1985-08-27	The Hilton-Davis Chemical Co.	Process for preparing quinolinic acid
US5635071A (en) *	1995-01-20	1997-06-03	Zenon Airport Enviromental, Inc.	Recovery of carboxylic acids from chemical plant effluents
EP0780152A1 (de) *	1995-12-21	1997-06-25	Stork Friesland B.V.	Halbdurchlässige, zusammengesetzte Membran, Verfahren zur Herstellung einer derartigen Membran, und ihre Verwendung

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5028336A (en) *	1989-03-03	1991-07-02	Texaco Inc.	Separation of water-soluble organic electrolytes

1998
- 1998-04-02 NL NL1008788A patent/NL1008788C2/nl not_active IP Right Cessation
1999
- 1999-03-29 EP EP99200965A patent/EP0947508B1/de not_active Expired - Lifetime
- 1999-03-29 AT AT99200965T patent/ATE221877T1/de not_active IP Right Cessation
- 1999-03-29 DE DE69902413T patent/DE69902413D1/de not_active Expired - Lifetime
- 1999-04-01 IN IN379MA1999 patent/IN187646B/en unknown
- 1999-04-01 CN CN99106247A patent/CN1236777A/zh active Pending
- 1999-04-01 JP JP11094648A patent/JPH11322717A/ja active Pending
- 1999-04-02 US US09/283,757 patent/US6133450A/en not_active Expired - Fee Related
- 1999-04-02 CZ CZ991177A patent/CZ117799A3/cs unknown

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4537971A (en) *	1981-05-06	1985-08-27	The Hilton-Davis Chemical Co.	Process for preparing quinolinic acid
US5635071A (en) *	1995-01-20	1997-06-03	Zenon Airport Enviromental, Inc.	Recovery of carboxylic acids from chemical plant effluents
EP0780152A1 (de) *	1995-12-21	1997-06-25	Stork Friesland B.V.	Halbdurchlässige, zusammengesetzte Membran, Verfahren zur Herstellung einer derartigen Membran, und ihre Verwendung

Also Published As

Publication number	Publication date
ATE221877T1 (de)	2002-08-15
US6133450A (en)	2000-10-17
JPH11322717A (ja)	1999-11-24
CZ117799A3 (cs)	1999-10-13
EP0947508B1 (de)	2002-08-07
EP0947508A1 (de)	1999-10-06
CN1236777A (zh)	1999-12-01
IN187646B (de)	2002-06-01
DE69902413D1 (de)	2002-09-12

Legal Events

Date	Code	Title	Description
1999-12-01	PD2B	A search report has been drawn up
2003-01-06	VD1	Lapsed due to non-payment of the annual fee	Effective date: 20021101

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