NL1009218C2 - Bereiding van een polymeer onder toepassing van een anorganisch membraan met een kleine gemiddelde poriegrootte. - Google Patents
Bereiding van een polymeer onder toepassing van een anorganisch membraan met een kleine gemiddelde poriegrootte. Download PDFInfo
- Publication number
- NL1009218C2 NL1009218C2 NL1009218A NL1009218A NL1009218C2 NL 1009218 C2 NL1009218 C2 NL 1009218C2 NL 1009218 A NL1009218 A NL 1009218A NL 1009218 A NL1009218 A NL 1009218A NL 1009218 C2 NL1009218 C2 NL 1009218C2
- Authority
- NL
- Netherlands
- Prior art keywords
- membrane
- reaction
- reaction mixture
- polymer
- average pore
- Prior art date
Links
- 239000012528 membrane Substances 0.000 title claims abstract description 78
- 239000011148 porous material Substances 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 229920000642 polymer Polymers 0.000 title claims description 10
- 239000011541 reaction mixture Substances 0.000 claims abstract description 40
- 238000006243 chemical reaction Methods 0.000 claims abstract description 36
- 238000000034 method Methods 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 239000000376 reactant Substances 0.000 claims description 12
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 239000000919 ceramic Substances 0.000 claims description 3
- 150000002894 organic compounds Chemical class 0.000 abstract 2
- 238000006482 condensation reaction Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 description 7
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 6
- 229920000180 alkyd Polymers 0.000 description 5
- 238000002474 experimental method Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000006116 polymerization reaction Methods 0.000 description 4
- 108020005351 Isochores Proteins 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 230000004907 flux Effects 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000004642 Polyimide Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 230000003197 catalytic effect Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 239000012466 permeate Substances 0.000 description 2
- 238000006068 polycondensation reaction Methods 0.000 description 2
- 229920001721 polyimide Polymers 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 1
- TXBCBTDQIULDIA-UHFFFAOYSA-N 2-[[3-hydroxy-2,2-bis(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)(CO)COCC(CO)(CO)CO TXBCBTDQIULDIA-UHFFFAOYSA-N 0.000 description 1
- BWMXRNGZUDOSJR-UHFFFAOYSA-N 3,3,5-trimethylhexanoic acid Chemical compound CC(C)CC(C)(C)CC(O)=O BWMXRNGZUDOSJR-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 150000008065 acid anhydrides Chemical class 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000000071 blow moulding Methods 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000010097 foam moulding Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000002638 heterogeneous catalyst Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000002808 molecular sieve Substances 0.000 description 1
- DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- 238000005373 pervaporation Methods 0.000 description 1
- ZWLUXSQADUDCSB-UHFFFAOYSA-N phthalaldehyde Chemical compound O=CC1=CC=CC=C1C=O ZWLUXSQADUDCSB-UHFFFAOYSA-N 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2475—Membrane reactors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2455—Stationary reactors without moving elements inside provoking a loop type movement of the reactants
- B01J19/2465—Stationary reactors without moving elements inside provoking a loop type movement of the reactants externally, i.e. the mixture leaving the vessel and subsequently re-entering it
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/04—Feed or outlet devices; Feed or outlet control devices using osmotic pressure using membranes, porous plates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
- B01J2219/0011—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling involving reactant liquids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Saccharide Compounds (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Polyoxymethylene Polymers And Polymers With Carbon-To-Carbon Bonds (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL1009218A NL1009218C2 (nl) | 1998-05-20 | 1998-05-20 | Bereiding van een polymeer onder toepassing van een anorganisch membraan met een kleine gemiddelde poriegrootte. |
| AT99925010T ATE222797T1 (de) | 1998-05-20 | 1999-05-15 | Verfahren zur herstellung einer organischen verbindung durch eine kondensationsreaktion |
| DE69902667T DE69902667T2 (de) | 1998-05-20 | 1999-05-15 | Verfahren zur herstellung einer organischen verbindung durch eine kondensationsreaktion |
| JP2000549368A JP2002515325A (ja) | 1998-05-20 | 1999-05-15 | 縮合反応による有機化合物の調製 |
| PCT/EP1999/003435 WO1999059711A1 (en) | 1998-05-20 | 1999-05-15 | Preparation of an organic compound by a condensation reaction |
| ES99925010T ES2183560T3 (es) | 1998-05-20 | 1999-05-15 | Preparacion de un compuesto organico por una raccion de condensacion. |
| EP99925010A EP1094891B1 (de) | 1998-05-20 | 1999-05-15 | Verfahren zur herstellung einer organischen verbindung durch eine kondensationsreaktion |
| US09/713,167 US6476185B1 (en) | 1998-05-20 | 2000-11-15 | Preparation of an organic compound by a condensation reaction |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL1009218A NL1009218C2 (nl) | 1998-05-20 | 1998-05-20 | Bereiding van een polymeer onder toepassing van een anorganisch membraan met een kleine gemiddelde poriegrootte. |
| NL1009218 | 1998-05-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NL1009218C2 true NL1009218C2 (nl) | 1999-11-24 |
Family
ID=19767174
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NL1009218A NL1009218C2 (nl) | 1998-05-20 | 1998-05-20 | Bereiding van een polymeer onder toepassing van een anorganisch membraan met een kleine gemiddelde poriegrootte. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US6476185B1 (de) |
| EP (1) | EP1094891B1 (de) |
| JP (1) | JP2002515325A (de) |
| AT (1) | ATE222797T1 (de) |
| DE (1) | DE69902667T2 (de) |
| ES (1) | ES2183560T3 (de) |
| NL (1) | NL1009218C2 (de) |
| WO (1) | WO1999059711A1 (de) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1316577B1 (de) | 2001-11-30 | 2005-02-23 | Akzo Nobel N.V. | Verfahren zur Herstellung von Polymeren aus Glycerin mit einem Saponit-Katalysator |
| AU2003273998A1 (en) * | 2002-10-22 | 2004-05-13 | Akzo Nobel N.V. | Dewatering of peroxygen formulations using pervaporation |
| US20040211729A1 (en) * | 2003-04-25 | 2004-10-28 | Sunkara Hari Babu | Processes for recovering oligomers of glycols and polymerization catalysts from waste streams |
| US7329720B2 (en) * | 2005-11-29 | 2008-02-12 | General Electric Company | Methods for increasing the mean particle size of 2-hydrocarbyl-3,3-bis(hydroxyaryl)phthalimidines |
| US7579498B2 (en) | 2005-11-29 | 2009-08-25 | E. I. Du Pont De Nemours And Company | Process for preparing fluorinated alkyl carboxylate esters |
| WO2009088785A1 (en) * | 2007-12-31 | 2009-07-16 | Chevron U.S.A. Inc. | Membrane reactor with in-situ dehydration and method for using the same |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6296453A (ja) * | 1985-10-24 | 1987-05-02 | Japan Organo Co Ltd | アミノ酸エステル化反応装置 |
| US5009789A (en) * | 1987-01-19 | 1991-04-23 | Eka Nobel | Method and plant for separation of synthetic water soluble polymers |
| EP0512736A2 (de) * | 1991-05-06 | 1992-11-11 | Rohm And Haas Company | Ultrafiltrationsverfahren und -anlage für Gewinnung von Polymelatices aus einer frischen Mutterlauge |
| US5434315A (en) * | 1994-02-22 | 1995-07-18 | E. I. Du Pont De Nemours And Company | Reducing molecular weight polydispersity of polyether glycols by membrane fractionation |
| US5545829A (en) * | 1993-02-12 | 1996-08-13 | Hoechst Aktiengesellschaft | Process for preparing cycloolefin copolymers |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4329449A (en) * | 1978-09-01 | 1982-05-11 | A. E. Staley Manufacturing Company | Method of using recycled mother liquors to produce aldosides |
| US5717081A (en) | 1993-09-17 | 1998-02-10 | Unichema Chemie B.V. | Process for producing an alkylglycoside using a pervaporation membrane to remove reaction water |
| DE4423355A1 (de) | 1994-07-04 | 1996-01-11 | Bayer Ag | Verfahren zur Herstellung von Maleinsäuredialkylestern |
-
1998
- 1998-05-20 NL NL1009218A patent/NL1009218C2/nl not_active IP Right Cessation
-
1999
- 1999-05-15 EP EP99925010A patent/EP1094891B1/de not_active Revoked
- 1999-05-15 DE DE69902667T patent/DE69902667T2/de not_active Revoked
- 1999-05-15 AT AT99925010T patent/ATE222797T1/de not_active IP Right Cessation
- 1999-05-15 JP JP2000549368A patent/JP2002515325A/ja not_active Withdrawn
- 1999-05-15 WO PCT/EP1999/003435 patent/WO1999059711A1/en not_active Ceased
- 1999-05-15 ES ES99925010T patent/ES2183560T3/es not_active Expired - Lifetime
-
2000
- 2000-11-15 US US09/713,167 patent/US6476185B1/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6296453A (ja) * | 1985-10-24 | 1987-05-02 | Japan Organo Co Ltd | アミノ酸エステル化反応装置 |
| US5009789A (en) * | 1987-01-19 | 1991-04-23 | Eka Nobel | Method and plant for separation of synthetic water soluble polymers |
| EP0512736A2 (de) * | 1991-05-06 | 1992-11-11 | Rohm And Haas Company | Ultrafiltrationsverfahren und -anlage für Gewinnung von Polymelatices aus einer frischen Mutterlauge |
| US5545829A (en) * | 1993-02-12 | 1996-08-13 | Hoechst Aktiengesellschaft | Process for preparing cycloolefin copolymers |
| US5434315A (en) * | 1994-02-22 | 1995-07-18 | E. I. Du Pont De Nemours And Company | Reducing molecular weight polydispersity of polyether glycols by membrane fractionation |
Non-Patent Citations (2)
| Title |
|---|
| DATABASE WPI Section Ch Week 8723, Derwent World Patents Index; Class B05, AN 87-160967, XP002090331 * |
| PATENT ABSTRACTS OF JAPAN vol. 11, no. 307 (C - 450) 7 October 1987 (1987-10-07) * |
Also Published As
| Publication number | Publication date |
|---|---|
| ES2183560T3 (es) | 2003-03-16 |
| WO1999059711A1 (en) | 1999-11-25 |
| JP2002515325A (ja) | 2002-05-28 |
| ATE222797T1 (de) | 2002-09-15 |
| US6476185B1 (en) | 2002-11-05 |
| DE69902667D1 (de) | 2002-10-02 |
| EP1094891B1 (de) | 2002-08-28 |
| DE69902667T2 (de) | 2004-04-08 |
| EP1094891A1 (de) | 2001-05-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PD2B | A search report has been drawn up | ||
| VD1 | Lapsed due to non-payment of the annual fee |
Effective date: 20061201 |