NL1010880C2 - Werkwijze voor het isoleren van aroma's uit een cafeïne- of theobrominebevattende voedingsmiddelgrondstof. - Google Patents

Werkwijze voor het isoleren van aroma's uit een cafeïne- of theobrominebevattende voedingsmiddelgrondstof. Download PDF

Info

Publication number: NL1010880C2
Authority: NL; Netherlands
Prior art keywords: food; cocoa; extraction; pervaporation; extract
Prior art date: 1998-12-23

Application number

NL1010880A

Other languages

English (en)

Dutch (nl)

Inventor

Hans Robert Kattenberg

Hendrik Derk Hoving

Herman Henk Nijhuis

Jeroen Harold Anton Willemsen

Dick Antonius Johanne Starmans

Miranda Gertruida Mari Winters

Original Assignee

Adm Cocoa B V

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1998-12-23

Filing date

1998-12-23

Publication date

2000-06-26

1998-12-23 Application filed by Adm Cocoa B V filed Critical Adm Cocoa B V

1998-12-23 Priority to NL1010880A priority Critical patent/NL1010880C2/nl

1999-12-23 Priority to DE69917805T priority patent/DE69917805D1/de

1999-12-23 Priority to CA002356198A priority patent/CA2356198A1/en

1999-12-23 Priority to EP99963698A priority patent/EP1139792B1/de

1999-12-23 Priority to AT99963698T priority patent/ATE268125T1/de

1999-12-23 Priority to AU20070/00A priority patent/AU2007000A/en

1999-12-23 Priority to PCT/NL1999/000802 priority patent/WO2000038540A1/en

2000-06-26 Application granted granted Critical

2000-06-26 Publication of NL1010880C2 publication Critical patent/NL1010880C2/nl

2001-06-25 Priority to US09/887,558 priority patent/US6506433B2/en

Links

235000013305 food Nutrition 0.000 title claims abstract description 61
238000000034 method Methods 0.000 title claims abstract description 51
YAPQBXQYLJRXSA-UHFFFAOYSA-N theobromine Chemical compound CN1C(=O)NC(=O)C2=C1N=CN2C YAPQBXQYLJRXSA-UHFFFAOYSA-N 0.000 title claims description 30
RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 title claims description 28
239000002994 raw material Substances 0.000 title claims description 22
229960004559 theobromine Drugs 0.000 title claims description 15
LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 title claims description 14
229960001948 caffeine Drugs 0.000 title claims description 14
VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 title claims description 14
244000299461 Theobroma cacao Species 0.000 claims abstract description 102
235000009470 Theobroma cacao Nutrition 0.000 claims abstract description 100
238000000605 extraction Methods 0.000 claims abstract description 74
238000005373 pervaporation Methods 0.000 claims abstract description 51
239000000284 extract Substances 0.000 claims abstract description 48
239000012528 membrane Substances 0.000 claims abstract description 32
239000012466 permeate Substances 0.000 claims abstract description 23
239000012141 concentrate Substances 0.000 claims abstract description 17
239000000463 material Substances 0.000 claims abstract description 12
244000269722 Thea sinensis Species 0.000 claims abstract description 5
235000016213 coffee Nutrition 0.000 claims abstract description 4
235000013353 coffee beverage Nutrition 0.000 claims abstract description 4
239000000796 flavoring agent Substances 0.000 claims description 57
235000019634 flavors Nutrition 0.000 claims description 57
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 47
239000000843 powder Substances 0.000 claims description 30
239000007788 liquid Substances 0.000 claims description 25
239000012510 hollow fiber Substances 0.000 claims description 16
ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 claims description 11
235000005487 catechin Nutrition 0.000 claims description 11
150000001765 catechin Chemical class 0.000 claims description 9
239000004205 dimethyl polysiloxane Substances 0.000 claims description 9
239000012465 retentate Substances 0.000 claims description 8
229920002943 EPDM rubber Polymers 0.000 claims description 7
230000015572 biosynthetic process Effects 0.000 claims description 2
235000013870 dimethyl polysiloxane Nutrition 0.000 claims 1
235000019568 aromas Nutrition 0.000 abstract description 14
230000002209 hydrophobic effect Effects 0.000 abstract 1
239000002245 particle Substances 0.000 description 16
239000003925 fat Substances 0.000 description 13
235000019197 fats Nutrition 0.000 description 13
238000009833 condensation Methods 0.000 description 12
230000005494 condensation Effects 0.000 description 12
239000000126 substance Substances 0.000 description 12
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 11
239000002253 acid Substances 0.000 description 10
238000004108 freeze drying Methods 0.000 description 10
238000002474 experimental method Methods 0.000 description 8
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238000000926 separation method Methods 0.000 description 7
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
235000013336 milk Nutrition 0.000 description 6
239000008267 milk Substances 0.000 description 6
210000004080 milk Anatomy 0.000 description 6
239000000047 product Substances 0.000 description 6
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244000290333 Vanilla fragrans Species 0.000 description 5
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235000019636 bitter flavor Nutrition 0.000 description 5
230000015556 catabolic process Effects 0.000 description 5
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238000006731 degradation reaction Methods 0.000 description 5
238000004128 high performance liquid chromatography Methods 0.000 description 5
230000002906 microbiologic effect Effects 0.000 description 5
238000001256 steam distillation Methods 0.000 description 5
238000000194 supercritical-fluid extraction Methods 0.000 description 5
YGHRJJRRZDOVPD-UHFFFAOYSA-N 3-methylbutanal Chemical compound CC(C)CC=O YGHRJJRRZDOVPD-UHFFFAOYSA-N 0.000 description 4
239000011248 coating agent Substances 0.000 description 4
238000000576 coating method Methods 0.000 description 4
XMOCLSLCDHWDHP-IUODEOHRSA-N epi-Gallocatechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@H]2O)=CC(O)=C(O)C(O)=C1 XMOCLSLCDHWDHP-IUODEOHRSA-N 0.000 description 4
235000013861 fat-free Nutrition 0.000 description 4
239000000203 mixture Substances 0.000 description 4
108090000623 proteins and genes Proteins 0.000 description 4
102000004169 proteins and genes Human genes 0.000 description 4
238000003908 quality control method Methods 0.000 description 4
MIDXCONKKJTLDX-UHFFFAOYSA-N 3,5-dimethylcyclopentane-1,2-dione Chemical compound CC1CC(C)C(=O)C1=O MIDXCONKKJTLDX-UHFFFAOYSA-N 0.000 description 3
241000202807 Glycyrrhiza Species 0.000 description 3
235000001453 Glycyrrhiza echinata Nutrition 0.000 description 3
235000006200 Glycyrrhiza glabra Nutrition 0.000 description 3
235000017382 Glycyrrhiza lepidota Nutrition 0.000 description 3
239000006286 aqueous extract Substances 0.000 description 3
235000020289 caffè mocha Nutrition 0.000 description 3
235000013736 caramel Nutrition 0.000 description 3
230000001419 dependent effect Effects 0.000 description 3
238000006073 displacement reaction Methods 0.000 description 3
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238000001471 micro-filtration Methods 0.000 description 3
230000036651 mood Effects 0.000 description 3
239000003960 organic solvent Substances 0.000 description 3
238000005325 percolation Methods 0.000 description 3
238000000746 purification Methods 0.000 description 3
238000001223 reverse osmosis Methods 0.000 description 3
239000002904 solvent Substances 0.000 description 3
235000013616 tea Nutrition 0.000 description 3
238000007738 vacuum evaporation Methods 0.000 description 3
PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 description 2
PFTAWBLQPZVEMU-ZFWWWQNUSA-N (+)-epicatechin Natural products C1([C@@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-ZFWWWQNUSA-N 0.000 description 2
PFTAWBLQPZVEMU-UKRRQHHQSA-N (-)-epicatechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-UKRRQHHQSA-N 0.000 description 2
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
240000007154 Coffea arabica Species 0.000 description 2
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Natural products CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
XMOCLSLCDHWDHP-UHFFFAOYSA-N L-Epigallocatechin Natural products OC1CC2=C(O)C=C(O)C=C2OC1C1=CC(O)=C(O)C(O)=C1 XMOCLSLCDHWDHP-UHFFFAOYSA-N 0.000 description 2
244000141359 Malus pumila Species 0.000 description 2
239000003963 antioxidant agent Substances 0.000 description 2
235000006708 antioxidants Nutrition 0.000 description 2
235000021016 apples Nutrition 0.000 description 2
HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 2
235000014121 butter Nutrition 0.000 description 2
238000012512 characterization method Methods 0.000 description 2
235000019219 chocolate Nutrition 0.000 description 2
229950001002 cianidanol Drugs 0.000 description 2
150000001875 compounds Chemical class 0.000 description 2
239000013078 crystal Substances 0.000 description 2
235000005911 diet Nutrition 0.000 description 2
230000037213 diet Effects 0.000 description 2
238000001035 drying Methods 0.000 description 2
235000013399 edible fruits Nutrition 0.000 description 2
229920001971 elastomer Polymers 0.000 description 2
239000000806 elastomer Substances 0.000 description 2
LPTRNLNOHUVQMS-UHFFFAOYSA-N epicatechin Natural products Cc1cc(O)cc2OC(C(O)Cc12)c1ccc(O)c(O)c1 LPTRNLNOHUVQMS-UHFFFAOYSA-N 0.000 description 2
235000012734 epicatechin Nutrition 0.000 description 2
DZYNKLUGCOSVKS-UHFFFAOYSA-N epigallocatechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3cc(O)c(O)c(O)c3 DZYNKLUGCOSVKS-UHFFFAOYSA-N 0.000 description 2
238000011156 evaluation Methods 0.000 description 2
235000011389 fruit/vegetable juice Nutrition 0.000 description 2
PHTQWCKDNZKARW-UHFFFAOYSA-N isoamylol Chemical compound CC(C)CCO PHTQWCKDNZKARW-UHFFFAOYSA-N 0.000 description 2
229960004592 isopropanol Drugs 0.000 description 2
238000002156 mixing Methods 0.000 description 2
229920001296 polysiloxane Polymers 0.000 description 2
238000010992 reflux Methods 0.000 description 2
239000004576 sand Substances 0.000 description 2
238000004062 sedimentation Methods 0.000 description 2
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238000003756 stirring Methods 0.000 description 2
CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 description 1
XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 description 1
235000011293 Brassica napus Nutrition 0.000 description 1
240000008100 Brassica rapa Species 0.000 description 1
235000000540 Brassica rapa subsp rapa Nutrition 0.000 description 1
101100481408 Danio rerio tie2 gene Proteins 0.000 description 1
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241000196324 Embryophyta Species 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
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101100481410 Mus musculus Tek gene Proteins 0.000 description 1
241000533293 Sesbania emerus Species 0.000 description 1
229930006000 Sucrose Natural products 0.000 description 1
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
239000005862 Whey Substances 0.000 description 1
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NEHMKBQYUWJMIP-UHFFFAOYSA-N anhydrous methyl chloride Natural products ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 description 1
230000003078 antioxidant effect Effects 0.000 description 1
230000000903 blocking effect Effects 0.000 description 1
238000009835 boiling Methods 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
238000004140 cleaning Methods 0.000 description 1
239000008199 coating composition Substances 0.000 description 1
229940119429 cocoa extract Drugs 0.000 description 1
235000019864 coconut oil Nutrition 0.000 description 1
239000003240 coconut oil Substances 0.000 description 1
244000221110 common millet Species 0.000 description 1
238000010276 construction Methods 0.000 description 1
239000003431 cross linking reagent Substances 0.000 description 1
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238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
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239000004615 ingredient Substances 0.000 description 1
230000001788 irregular Effects 0.000 description 1
239000008101 lactose Substances 0.000 description 1
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239000003921 oil Substances 0.000 description 1
235000019198 oils Nutrition 0.000 description 1
238000005457 optimization Methods 0.000 description 1
230000020477 pH reduction Effects 0.000 description 1
QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 1
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235000014214 soft drink Nutrition 0.000 description 1
239000007858 starting material Substances 0.000 description 1
238000003860 storage Methods 0.000 description 1
239000005720 sucrose Substances 0.000 description 1
235000000346 sugar Nutrition 0.000 description 1
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239000008399 tap water Substances 0.000 description 1
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MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 1
235000019222 white chocolate Nutrition 0.000 description 1

Classifications

- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/46—Coffee flavour; Coffee oil; Flavouring of coffee or coffee extract
- A23F5/48—Isolation or recuperation of coffee flavour or coffee oil
- A23F5/50—Isolation or recuperation of coffee flavour or coffee oil from coffee extract
- A23F5/505—Isolation or recuperation of coffee flavour or coffee oil from coffee extract by distillation, e.g. stripping the extract; Recovering volatile gases, e.g. during concentration
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/40—Tea flavour; Tea oil; Flavouring of tea or tea extract
- A23F3/42—Isolation or recuperation of tea flavour or tea oil
- A23F3/426—Isolation or recuperation of tea flavour or tea oil by distillation, e.g. stripping leaves; Recovering volatile gases
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/115—Natural spices, flavouring agents or condiments; Extracts thereof obtained by distilling, stripping, or recovering of volatiles

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Food Science & Technology (AREA)
Polymers & Plastics (AREA)
Oil, Petroleum & Natural Gas (AREA)
Health & Medical Sciences (AREA)
Nutrition Science (AREA)
Seasonings (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Tea And Coffee (AREA)

NL1010880A 1998-12-23 1998-12-23 Werkwijze voor het isoleren van aroma's uit een cafeïne- of theobrominebevattende voedingsmiddelgrondstof. NL1010880C2 (nl)

Priority Applications (8)

Application Number	Priority Date	Filing Date	Title
NL1010880A NL1010880C2 (nl)	1998-12-23	1998-12-23	Werkwijze voor het isoleren van aroma's uit een cafeïne- of theobrominebevattende voedingsmiddelgrondstof.
DE69917805T DE69917805D1 (de)	1998-12-23	1999-12-23	Verfahren zum gewinnen eines aromakonzentrats aus coffein oder theobromin enthaltenden nahrungsmitteln
CA002356198A CA2356198A1 (en)	1998-12-23	1999-12-23	Method for recovering aroma concentrate from a caffeine- or theobromine-comprising food base material
EP99963698A EP1139792B1 (de)	1998-12-23	1999-12-23	Verfahren zum gewinnen eines aromakonzentrats aus coffein oder theobromin enthaltenden nahrungsmitteln
AT99963698T ATE268125T1 (de)	1998-12-23	1999-12-23	Verfahren zum gewinnen eines aromakonzentrats aus coffein oder theobromin enthaltenden nahrungsmitteln
AU20070/00A AU2007000A (en)	1998-12-23	1999-12-23	Method for recovering aroma concentrate from a caffeine- or theobromine-comprising food base material
PCT/NL1999/000802 WO2000038540A1 (en)	1998-12-23	1999-12-23	Method for recovering aroma concentrate from a caffeine- or theobromine-comprising food base material
US09/887,558 US6506433B2 (en)	1998-12-23	2001-06-25	Method for recovering aroma concentrate from a caffeine- or theobromine-comprising food base material

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
NL1010880A NL1010880C2 (nl)	1998-12-23	1998-12-23	Werkwijze voor het isoleren van aroma's uit een cafeïne- of theobrominebevattende voedingsmiddelgrondstof.
NL1010880		1998-12-23

Publications (1)

Publication Number	Publication Date
NL1010880C2 true NL1010880C2 (nl)	2000-06-26

Family

ID=19768359

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL1010880A NL1010880C2 (nl)	1998-12-23	1998-12-23	Werkwijze voor het isoleren van aroma's uit een cafeïne- of theobrominebevattende voedingsmiddelgrondstof.

Country Status (8)

Country	Link
US (1)	US6506433B2 (de)
EP (1)	EP1139792B1 (de)
AT (1)	ATE268125T1 (de)
AU (1)	AU2007000A (de)
CA (1)	CA2356198A1 (de)
DE (1)	DE69917805D1 (de)
NL (1)	NL1010880C2 (de)
WO (1)	WO2000038540A1 (de)

Cited By (1)

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Publication number	Priority date	Publication date	Assignee	Title
WO2002002213A1 (en) *	2000-07-04	2002-01-10	Zylepsis Limited	Separation method

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Publication number	Priority date	Publication date	Assignee	Title
US20030099752A1 (en)	2001-10-19	2003-05-29	The Procter & Gamble Co.	Liquid coffee concentrates
US7303773B2 (en) *	2003-10-21	2007-12-04	The Procter & Gamble Company	Process for enriching extracts of natural theanine
ES2336901T3 (es) *	2003-10-27	2010-04-19	Nestec S.A.	Bebida a base de cafe fermentado.
PT103657B (pt) *	2007-02-12	2009-08-25	Univ Do Porto	Processo de enriquecimento aromático de uma bebida obtida por desalcoolização
WO2012155889A1 (de) *	2011-05-17	2012-11-22	Innodrying Gmbh	Verfahren zur herstellung von löslichen aromakonzentraten
CN103385338B (zh) *	2013-06-09	2015-04-22	南京工业大学	一种速溶茶粉生产工艺中香气成分的回收方法
GB201402745D0 (en) *	2014-02-17	2014-04-02	Givaudan Sa	Product
CN104207083B (zh) *	2014-09-10	2016-04-13	娄尤来	一种天然玫瑰花有效香气成分的提取方法
CN109198574A (zh) *	2018-10-15	2019-01-15	深圳市深宝技术中心有限公司	一种茶叶香气物质富集方法及制得的茶叶香气物质

Citations (3)

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Publication number	Priority date	Publication date	Assignee	Title
JPH0549840A (ja) *	1991-08-19	1993-03-02	Hitachi Zosen Corp	膜を用いるお茶成分濃縮方法
SE500579C2 (sv) *	1992-09-25	1994-07-18	V & S Vin & Sprit Ab Tillverkn	Metod för reglering av den relativa permeatsammansättningen
DE4421682A1 (de) *	1993-06-23	1995-02-23	Geesthacht Gkss Forschung	Verfahren und Vorrichtung zur Trennung von flüchtigen Aromastoffen

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1999
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- 1999-12-23 AU AU20070/00A patent/AU2007000A/en not_active Abandoned
- 1999-12-23 AT AT99963698T patent/ATE268125T1/de not_active IP Right Cessation
- 1999-12-23 EP EP99963698A patent/EP1139792B1/de not_active Expired - Lifetime
- 1999-12-23 WO PCT/NL1999/000802 patent/WO2000038540A1/en not_active Ceased
- 1999-12-23 CA CA002356198A patent/CA2356198A1/en not_active Abandoned
2001
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Also Published As

Publication number	Publication date
AU2007000A (en)	2000-07-31
EP1139792B1 (de)	2004-06-02
EP1139792A1 (de)	2001-10-10
US20020058092A1 (en)	2002-05-16
DE69917805D1 (de)	2004-07-08
CA2356198A1 (en)	2000-07-06
US6506433B2 (en)	2003-01-14
WO2000038540A1 (en)	2000-07-06
ATE268125T1 (de)	2004-06-15

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Date	Code	Title	Description
2000-09-01	PD2B	A search report has been drawn up
2005-09-01	VD1	Lapsed due to non-payment of the annual fee	Effective date: 20050701

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NL1010880C2 - Werkwijze voor het isoleren van aroma's uit een cafeïne- of theobrominebevattende voedingsmiddelgrondstof. - Google Patents

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