NL8503443A - Werkwijze voor de bereiding van een magnesiumnitraat bevattende oplossing, die geschikt is voor toepassing bij de vervaardiging van technisch stabiele ammoniumnitraat bevattende meststofkorrels. - Google Patents

Werkwijze voor de bereiding van een magnesiumnitraat bevattende oplossing, die geschikt is voor toepassing bij de vervaardiging van technisch stabiele ammoniumnitraat bevattende meststofkorrels. Download PDF

Info

Publication number: NL8503443A
Authority: NL; Netherlands
Prior art keywords: ammonium nitrate; magnesium; reaction; nitrate; aqueous
Prior art date: 1985-12-13

Application number

NL8503443A

Other languages

English (en)

Dutch (nl)

Original Assignee

Nl Stikstof

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-12-13

Filing date

1985-12-13

Publication date

1987-07-01

1985-12-13 Application filed by Nl Stikstof filed Critical Nl Stikstof

1985-12-13 Priority to NL8503443A priority Critical patent/NL8503443A/nl

1986-12-12 Priority to DE8686202261T priority patent/DE3669491D1/de

1986-12-12 Priority to ES86202261T priority patent/ES2013597B3/es

1986-12-12 Priority to AT86202261T priority patent/ATE50969T1/de

1986-12-12 Priority to EP86202261A priority patent/EP0229421B1/de

1987-07-01 Publication of NL8503443A publication Critical patent/NL8503443A/nl

1990-03-15 Priority to GR89400319T priority patent/GR3000383T3/el

Links

YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical compound [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 title claims abstract description 52
PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 title claims abstract description 36
239000003337 fertilizer Substances 0.000 title claims abstract description 6
239000008187 granular material Substances 0.000 title claims abstract description 6
238000004519 manufacturing process Methods 0.000 title claims abstract description 6
238000000034 method Methods 0.000 title claims description 17
239000000395 magnesium oxide Substances 0.000 claims abstract description 34
CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 34
AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims abstract description 25
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 21
229910017604 nitric acid Inorganic materials 0.000 claims abstract description 21
238000006243 chemical reaction Methods 0.000 claims description 28
239000011541 reaction mixture Substances 0.000 claims description 17
239000000203 mixture Substances 0.000 claims description 14
238000003860 storage Methods 0.000 claims description 8
238000002360 preparation method Methods 0.000 claims description 5
239000011777 magnesium Substances 0.000 claims description 3
238000003756 stirring Methods 0.000 claims description 3
UUZZMWZGAZGXSF-UHFFFAOYSA-N peroxynitric acid Chemical compound OON(=O)=O UUZZMWZGAZGXSF-UHFFFAOYSA-N 0.000 claims description 2
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
229910052749 magnesium Inorganic materials 0.000 claims 1
239000000243 solution Substances 0.000 abstract description 19
239000007864 aqueous solution Substances 0.000 abstract description 5
239000012429 reaction media Substances 0.000 abstract description 2
239000000047 product Substances 0.000 description 11
238000012360 testing method Methods 0.000 description 9
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
238000002156 mixing Methods 0.000 description 5
238000001816 cooling Methods 0.000 description 4
238000002425 crystallisation Methods 0.000 description 4
230000008025 crystallization Effects 0.000 description 4
238000009835 boiling Methods 0.000 description 3
238000005469 granulation Methods 0.000 description 3
230000003179 granulation Effects 0.000 description 3
VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 3
239000000347 magnesium hydroxide Substances 0.000 description 3
229910001862 magnesium hydroxide Inorganic materials 0.000 description 3
230000015572 biosynthetic process Effects 0.000 description 2
ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 2
239000001095 magnesium carbonate Substances 0.000 description 2
235000014380 magnesium carbonate Nutrition 0.000 description 2
229910000021 magnesium carbonate Inorganic materials 0.000 description 2
101000713585 Homo sapiens Tubulin beta-4A chain Proteins 0.000 description 1
229910017897 NH4 NO3 Inorganic materials 0.000 description 1
229910002651 NO3 Inorganic materials 0.000 description 1
NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
IOVCWXUNBOPUCH-UHFFFAOYSA-N Nitrous acid Chemical compound ON=O IOVCWXUNBOPUCH-UHFFFAOYSA-N 0.000 description 1
102100036788 Tubulin beta-4A chain Human genes 0.000 description 1
239000002826 coolant Substances 0.000 description 1
238000012937 correction Methods 0.000 description 1
238000011161 development Methods 0.000 description 1
238000009826 distribution Methods 0.000 description 1
230000007613 environmental effect Effects 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
238000011049 filling Methods 0.000 description 1
238000001914 filtration Methods 0.000 description 1
230000036571 hydration Effects 0.000 description 1
238000006703 hydration reaction Methods 0.000 description 1
239000012535 impurity Substances 0.000 description 1
FYYHWMGAXLPEAU-OUBTZVSYSA-N magnesium-25 atom Chemical compound [25Mg] FYYHWMGAXLPEAU-OUBTZVSYSA-N 0.000 description 1
239000000463 material Substances 0.000 description 1
238000012544 monitoring process Methods 0.000 description 1
239000002245 particle Substances 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
239000002994 raw material Substances 0.000 description 1
239000003507 refrigerant Substances 0.000 description 1
238000005057 refrigeration Methods 0.000 description 1
239000007787 solid Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/38—Magnesium nitrates
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C1/00—Ammonium nitrate fertilisers
- C05C1/02—Granulation; Pelletisation; Stabilisation; Colouring

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Geology (AREA)
Inorganic Chemistry (AREA)
Fertilizers (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

NL8503443A 1985-12-13 1985-12-13 Werkwijze voor de bereiding van een magnesiumnitraat bevattende oplossing, die geschikt is voor toepassing bij de vervaardiging van technisch stabiele ammoniumnitraat bevattende meststofkorrels. NL8503443A (nl)

Priority Applications (6)

Application Number	Priority Date	Filing Date	Title
NL8503443A NL8503443A (nl)	1985-12-13	1985-12-13	Werkwijze voor de bereiding van een magnesiumnitraat bevattende oplossing, die geschikt is voor toepassing bij de vervaardiging van technisch stabiele ammoniumnitraat bevattende meststofkorrels.
DE8686202261T DE3669491D1 (de)	1985-12-13	1986-12-12	Verfahren zur herstellung einer magnesiumnitrat enthaltenden loesung, verwendbar in der herstellung von thermisch stabiles ammoniumnitrat enthaltendem duengemittel.
ES86202261T ES2013597B3 (es)	1985-12-13	1986-12-12	Producción de una solución que contiene nitrato magnésico.
AT86202261T ATE50969T1 (de)	1985-12-13	1986-12-12	Verfahren zur herstellung einer magnesiumnitrat enthaltenden loesung, verwendbar in der herstellung von thermisch stabiles ammoniumnitrat enthaltendem duengemittel.
EP86202261A EP0229421B1 (de)	1985-12-13	1986-12-12	Verfahren zur Herstellung einer Magnesiumnitrat enthaltenden Lösung, verwendbar in der Herstellung von thermisch stabiles Ammoniumnitrat enthaltendem Düngemittel
GR89400319T GR3000383T3 (en)	1985-12-13	1990-03-15	A process for the production of a magnesium nitrate containing solution suitable for use in making thermally stable ammonium nitrate containing fertilizers

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
NL8503443A NL8503443A (nl)	1985-12-13	1985-12-13	Werkwijze voor de bereiding van een magnesiumnitraat bevattende oplossing, die geschikt is voor toepassing bij de vervaardiging van technisch stabiele ammoniumnitraat bevattende meststofkorrels.
NL8503443		1985-12-13

Publications (1)

Publication Number	Publication Date
NL8503443A true NL8503443A (nl)	1987-07-01

Family

ID=19847015

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL8503443A NL8503443A (nl)	1985-12-13	1985-12-13	Werkwijze voor de bereiding van een magnesiumnitraat bevattende oplossing, die geschikt is voor toepassing bij de vervaardiging van technisch stabiele ammoniumnitraat bevattende meststofkorrels.

Country Status (6)

Country	Link
EP (1)	EP0229421B1 (de)
AT (1)	ATE50969T1 (de)
DE (1)	DE3669491D1 (de)
ES (1)	ES2013597B3 (de)
GR (1)	GR3000383T3 (de)
NL (1)	NL8503443A (de)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
WO2003066795A1 (en) *	2002-02-08	2003-08-14	Sk Corporation	Cleaning agent and method for cleaning heater tubes
US20100012237A1 (en)	2008-07-15	2010-01-21	Honeywell International Inc.	Weakly oxidizing ammonium nitrate composite materials and methods for preparing such compositions
CN104086235B (zh) *	2014-07-22	2016-02-24	路永宽	一种利用钢带造粒机生产全水溶性硝酸铵镁的方法
CN105621461B (zh) *	2015-12-28	2017-10-24	大连百傲化学股份有限公司	一种连续化生产硝酸镁的装置及工艺方法
CN109019645B (zh) *	2018-09-25	2023-07-14	天津华景工程技术有限公司	一种大颗粒硝酸镁的生产系统及生产方法
CN115155493B (zh) *	2022-07-05	2024-07-26	山西金兰化工股份有限公司	一种硝酸镁连续中和装置及制备工艺
CN119954186B (zh) *	2025-04-11	2025-07-01	山东海化骊潍新材料有限公司	一种硝酸镁制备过程中的反应热利用方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US1910807A (en) *	1930-03-04	1933-05-23	Hercules Powder Co Ltd	Method of producing hydrated nitrate double salt
US3173756A (en) *	1960-11-16	1965-03-16	Monsanto Co	Double nitrate salts and methods for their preparation
NL8104284A (nl) *	1981-09-17	1983-04-18	Unie Van Kunstmestfab Bv	Werkwijze voor het bereiden van magnesiumnitraathexahydraat, alsmede voor het thermisch stabiliseren van ammoniumnitraat onder toepassing van een zo verkregen magnesiumnitraathexahydraat.
ES8504079A1 (es) *	1982-10-01	1985-04-01	Stamicarbon	Un procedimiento para producir una solucion de nitrato de magnesio

1985
- 1985-12-13 NL NL8503443A patent/NL8503443A/nl not_active Application Discontinuation
1986
- 1986-12-12 EP EP86202261A patent/EP0229421B1/de not_active Expired - Lifetime
- 1986-12-12 AT AT86202261T patent/ATE50969T1/de not_active IP Right Cessation
- 1986-12-12 ES ES86202261T patent/ES2013597B3/es not_active Expired - Lifetime
- 1986-12-12 DE DE8686202261T patent/DE3669491D1/de not_active Expired - Lifetime
1990
- 1990-03-15 GR GR89400319T patent/GR3000383T3/el unknown

Also Published As

Publication number	Publication date
DE3669491D1 (de)	1990-04-19
ATE50969T1 (de)	1990-03-15
EP0229421A3 (en)	1987-08-05
GR3000383T3 (en)	1991-06-07
ES2013597B3 (es)	1990-05-16
EP0229421A2 (de)	1987-07-22
EP0229421B1 (de)	1990-03-14

Legal Events

Date	Code	Title	Description
1987-07-01	A1B	A search report has been drawn up
1989-08-01	BV	The patent application has lapsed

Publication	Publication Date	Title
SK282502B6 (sk)	2002-10-08	Spôsob výroby výrobkov, obsahujúcich disoli kyseliny mravčej a výrobky týmto spôsobom vyrobené
DK155879B (da)	1989-05-29	Fremgangsmaade til fremstilling af granulerede metalsaeber
US5985236A (en)	1999-11-16	Ammonium octamolybdate composition and method for producing the same
US3966853A (en)	1976-06-29	Process for preparing prilled porous ammonium nitrate
RU2522353C2 (ru)	2014-07-10	Способ получения композиций, содержащих двойные соли нитрата аммония
US3962329A (en)	1976-06-08	Manufacture of granular isobutylidenediurea
US4010245A (en)	1977-03-01	Production of hydrogen fluoride and calcium sulfate
US4028088A (en)	1977-06-07	Soil amendment and method
US4438083A (en)	1984-03-20	Process for preparing magnesium nitrate hexahydrate and for thermally stabilizing ammonium nitrate using magnesium nitrate hexahydrate
EP0229421B1 (de)	1990-03-14	Verfahren zur Herstellung einer Magnesiumnitrat enthaltenden Lösung, verwendbar in der Herstellung von thermisch stabiles Ammoniumnitrat enthaltendem Düngemittel
US3154545A (en)	1964-10-27	Process for preparing cyanuric acid
US4461913A (en)	1984-07-24	Production of urea phosphate
US3107145A (en)	1963-10-15	Process for defluorinating phosphatic materials
CA1044256A (en)	1978-12-12	Production of addition products of lower fatty acids or halogenated fatty acids
US2856278A (en)	1958-10-14	Making fertilizer-grade ammonium acid sulfate
US3640697A (en)	1972-02-08	Noncaking grained ammonium nitrate
US3097064A (en)	1963-07-09	Recovery of values from pickling liquor
CA1041117A (en)	1978-10-24	Production of salts of chlorinated acetic acids
RU2157366C1 (ru)	2000-10-10	Способ производства метилмеркаптана, способ получения катализатора для производства метилмеркаптана и способ получения сероводорода для производства метилмеркаптана
JPS6134429B2 (de)	1986-08-07
US4337228A (en)	1982-06-29	Process for the production of sulfates
US2350575A (en)	1944-06-06	Manufacture of aluminum sulphate products
EP0278562A2 (de)	1988-08-17	Verfahren zur Herstellung von Calciumnitrat-Harnstoff
US4268490A (en)	1981-05-19	Processes of making prilled ammonium nitrate compositions
RU2182144C1 (ru)	2002-05-10	Способ получения комплексного n:k удобрения