NL8900937A - Werkwijze voor de condensatie van imiden en alkoholen of aminen. - Google Patents

Werkwijze voor de condensatie van imiden en alkoholen of aminen. Download PDF

Info

Publication number: NL8900937A
Authority: NL; Netherlands
Prior art keywords: lactam; grams; condensation; hours; acyl
Prior art date: 1989-04-14

Application number

NL8900937A

Other languages

English (en)

Dutch (nl)

Original Assignee

Stamicarbon

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1989-04-14

Filing date

1989-04-14

Publication date

1990-11-01

1989-04-14 Application filed by Stamicarbon filed Critical Stamicarbon

1989-04-14 Priority to NL8900937A priority Critical patent/NL8900937A/nl

1990-04-11 Priority to EP90200888A priority patent/EP0392633B1/de

1990-04-11 Priority to AT90200888T priority patent/ATE120779T1/de

1990-04-11 Priority to ES90200888T priority patent/ES2071745T3/es

1990-04-11 Priority to DE69018298T priority patent/DE69018298T2/de

1990-04-11 Priority to DK90200888.7T priority patent/DK0392633T3/da

1990-04-12 Priority to CA002014480A priority patent/CA2014480A1/en

1990-04-12 Priority to US07/507,851 priority patent/US5059687A/en

1990-04-13 Priority to KR1019900005265A priority patent/KR930005149B1/ko

1990-04-16 Priority to JP2097822A priority patent/JPH03115326A/ja

1990-11-01 Publication of NL8900937A publication Critical patent/NL8900937A/nl

Links

238000000034 method Methods 0.000 title claims abstract description 23
238000009833 condensation Methods 0.000 title claims abstract description 10
230000005494 condensation Effects 0.000 title claims abstract description 10
150000003949 imides Chemical class 0.000 title claims abstract description 8
150000001412 amines Chemical class 0.000 title claims abstract description 5
-1 ester acyl lactams Chemical class 0.000 claims abstract description 46
229920000768 polyamine Polymers 0.000 claims abstract description 19
229920005862 polyol Polymers 0.000 claims abstract description 12
150000003077 polyols Chemical class 0.000 claims abstract description 12
150000001298 alcohols Chemical class 0.000 claims abstract description 4
238000006243 chemical reaction Methods 0.000 claims description 21
150000003951 lactams Chemical class 0.000 claims description 15
150000002596 lactones Chemical class 0.000 claims description 7
HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 claims description 7
YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical compound O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 claims description 6
150000001875 compounds Chemical class 0.000 claims description 6
AHEGXLOBOVFTHG-UHFFFAOYSA-N 1-[3-(2-oxopyrrolidine-1-carbonyl)benzoyl]pyrrolidin-2-one Chemical compound C=1C=CC(C(=O)N2C(CCC2)=O)=CC=1C(=O)N1CCCC1=O AHEGXLOBOVFTHG-UHFFFAOYSA-N 0.000 claims description 4
239000007788 liquid Substances 0.000 claims description 4
229930188620 butyrolactone Natural products 0.000 claims description 3
XUWHAWMETYGRKB-UHFFFAOYSA-N piperidin-2-one Chemical compound O=C1CCCCN1 XUWHAWMETYGRKB-UHFFFAOYSA-N 0.000 claims description 3
125000006413 ring segment Chemical group 0.000 claims description 3
PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 claims description 3
AOCWQPKHSMJWPL-UHFFFAOYSA-N 3-methylpyrrolidin-2-one Chemical compound CC1CCNC1=O AOCWQPKHSMJWPL-UHFFFAOYSA-N 0.000 claims description 2
SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims description 2
230000003197 catalytic effect Effects 0.000 claims description 2
239000007791 liquid phase Substances 0.000 abstract 1
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 10
XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical compound ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 10
229920001451 polypropylene glycol Polymers 0.000 description 10
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 9
ZBFCSRYSLRPAOY-UHFFFAOYSA-M sodium;hydroxy(phenyl)methanesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C(O)C1=CC=CC=C1 ZBFCSRYSLRPAOY-UHFFFAOYSA-M 0.000 description 9
239000004721 Polyphenylene oxide Substances 0.000 description 5
150000002430 hydrocarbons Chemical class 0.000 description 5
229920000570 polyether Polymers 0.000 description 5
239000005062 Polybutadiene Substances 0.000 description 4
150000004985 diamines Chemical class 0.000 description 4
125000002887 hydroxy group Chemical group [H]O* 0.000 description 4
229920002857 polybutadiene Polymers 0.000 description 4
239000004952 Polyamide Substances 0.000 description 3
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
229920001400 block copolymer Polymers 0.000 description 3
230000000052 comparative effect Effects 0.000 description 3
125000001033 ether group Chemical group 0.000 description 3
229930195733 hydrocarbon Natural products 0.000 description 3
229920001778 nylon Polymers 0.000 description 3
229920002647 polyamide Polymers 0.000 description 3
229920000642 polymer Polymers 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
239000004215 Carbon black (E152) Substances 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
239000004677 Nylon Substances 0.000 description 2
125000002252 acyl group Chemical group 0.000 description 2
125000002877 alkyl aryl group Chemical group 0.000 description 2
125000000217 alkyl group Chemical group 0.000 description 2
125000003277 amino group Chemical group 0.000 description 2
125000003710 aryl alkyl group Chemical group 0.000 description 2
125000003118 aryl group Chemical group 0.000 description 2
150000002009 diols Chemical class 0.000 description 2
JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 description 2
230000009477 glass transition Effects 0.000 description 2
WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
239000002184 metal Substances 0.000 description 2
229910052751 metal Inorganic materials 0.000 description 2
VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
239000000203 mixture Substances 0.000 description 2
238000010107 reaction injection moulding Methods 0.000 description 2
239000002904 solvent Substances 0.000 description 2
238000003756 stirring Methods 0.000 description 2
LFAAJNRMQQCJTH-UHFFFAOYSA-N 1,2-bis(7-oxoazepan-2-yl)ethane-1,2-dione Chemical compound C1CCCC(=O)NC1C(=O)C(=O)C1CCCCC(=O)N1 LFAAJNRMQQCJTH-UHFFFAOYSA-N 0.000 description 1
AGEILULECXEYHO-UHFFFAOYSA-N 1,6-bis(7-oxoazepan-2-yl)hexane-1,6-dione Chemical compound C1CCCC(=O)NC1C(=O)CCCCC(=O)C1CCCCC(=O)N1 AGEILULECXEYHO-UHFFFAOYSA-N 0.000 description 1
OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
239000005715 Fructose Substances 0.000 description 1
229930091371 Fructose Natural products 0.000 description 1
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
DJOWTWWHMWQATC-KYHIUUMWSA-N Karpoxanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1(O)C(C)(C)CC(O)CC1(C)O)C=CC=C(/C)C=CC2=C(C)CC(O)CC2(C)C DJOWTWWHMWQATC-KYHIUUMWSA-N 0.000 description 1
229920000459 Nitrile rubber Polymers 0.000 description 1
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
229930006000 Sucrose Natural products 0.000 description 1
239000012190 activator Substances 0.000 description 1
125000002947 alkylene group Chemical group 0.000 description 1
WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
NTXGQCSETZTARF-UHFFFAOYSA-N buta-1,3-diene;prop-2-enenitrile Chemical compound C=CC=C.C=CC#N NTXGQCSETZTARF-UHFFFAOYSA-N 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
238000004587 chromatography analysis Methods 0.000 description 1
238000003776 cleavage reaction Methods 0.000 description 1
125000004122 cyclic group Chemical group 0.000 description 1
125000000753 cycloalkyl group Chemical group 0.000 description 1
238000000113 differential scanning calorimetry Methods 0.000 description 1
235000013870 dimethyl polysiloxane Nutrition 0.000 description 1
238000007046 ethoxylation reaction Methods 0.000 description 1
239000008103 glucose Substances 0.000 description 1
239000012442 inert solvent Substances 0.000 description 1
238000012693 lactam polymerization Methods 0.000 description 1
150000002736 metal compounds Chemical class 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
125000006353 oxyethylene group Chemical group 0.000 description 1
125000004430 oxygen atom Chemical group O* 0.000 description 1
230000000737 periodic effect Effects 0.000 description 1
229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
238000006116 polymerization reaction Methods 0.000 description 1
229920001296 polysiloxane Polymers 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
239000000376 reactant Substances 0.000 description 1
230000007017 scission Effects 0.000 description 1
239000005720 sucrose Substances 0.000 description 1
YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
AGGKEGLBGGJEBZ-UHFFFAOYSA-N tetramethylenedisulfotetramine Chemical compound C1N(S2(=O)=O)CN3S(=O)(=O)N1CN2C3 AGGKEGLBGGJEBZ-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F216/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/32—Polymers modified by chemical after-treatment
- C08G65/329—Polymers modified by chemical after-treatment with organic compounds
- C08G65/333—Polymers modified by chemical after-treatment with organic compounds containing nitrogen
- C08G65/3332—Polymers modified by chemical after-treatment with organic compounds containing nitrogen containing carboxamide group
- C08G65/33327—Polymers modified by chemical after-treatment with organic compounds containing nitrogen containing carboxamide group cyclic
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D227/00—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00
- C07D227/02—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00 with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D227/06—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00 with only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D227/08—Oxygen atoms
- C07D227/087—One doubly-bound oxygen atom in position 2, e.g. lactams
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/14—Lactams
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/48—Polymers modified by chemical after-treatment

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Health & Medical Sciences (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
General Chemical & Material Sciences (AREA)
Polyamides (AREA)
Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Hydrogenated Pyridines (AREA)
Indole Compounds (AREA)
Other In-Based Heterocyclic Compounds (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Polyethers (AREA)

NL8900937A 1989-04-14 1989-04-14 Werkwijze voor de condensatie van imiden en alkoholen of aminen. NL8900937A (nl)

Priority Applications (10)

Application Number	Priority Date	Filing Date	Title
NL8900937A NL8900937A (nl)	1989-04-14	1989-04-14	Werkwijze voor de condensatie van imiden en alkoholen of aminen.
EP90200888A EP0392633B1 (de)	1989-04-14	1990-04-11	Verfahren zur Kondensation von Imiden und Alkoholen oder Aminen
AT90200888T ATE120779T1 (de)	1989-04-14	1990-04-11	Verfahren zur kondensation von imiden und alkoholen oder aminen.
ES90200888T ES2071745T3 (es)	1989-04-14	1990-04-11	Procedimiento para la condensacion de imidas y alcoholes o aminas.
DE69018298T DE69018298T2 (de)	1989-04-14	1990-04-11	Verfahren zur Kondensation von Imiden und Alkoholen oder Aminen.
DK90200888.7T DK0392633T3 (da)	1989-04-14	1990-04-11	Fremgangsmåde til kondensation af imider og alkoholer eller aminer
CA002014480A CA2014480A1 (en)	1989-04-14	1990-04-12	Process for the condensation of imides and alcohols or amines
US07/507,851 US5059687A (en)	1989-04-14	1990-04-12	Process for the condensation of imides and alcohols or amines
KR1019900005265A KR930005149B1 (ko)	1989-04-14	1990-04-13	이미드와 알코올 또는 아민의 축합방법
JP2097822A JPH03115326A (ja)	1989-04-14	1990-04-16	イミド類とアルコール類またはアミン類の縮合方法

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
NL8900937		1989-04-14
NL8900937A NL8900937A (nl)	1989-04-14	1989-04-14	Werkwijze voor de condensatie van imiden en alkoholen of aminen.

Publications (1)

Publication Number	Publication Date
NL8900937A true NL8900937A (nl)	1990-11-01

Family

ID=19854477

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL8900937A NL8900937A (nl)	1989-04-14	1989-04-14	Werkwijze voor de condensatie van imiden en alkoholen of aminen.

Country Status (10)

Country	Link
US (1)	US5059687A (de)
EP (1)	EP0392633B1 (de)
JP (1)	JPH03115326A (de)
KR (1)	KR930005149B1 (de)
AT (1)	ATE120779T1 (de)
CA (1)	CA2014480A1 (de)
DE (1)	DE69018298T2 (de)
DK (1)	DK0392633T3 (de)
ES (1)	ES2071745T3 (de)
NL (1)	NL8900937A (de)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5461157A (en) *	1992-06-19	1995-10-24	Daiichi Pharmaceutical Co., Ltd.	Process for preparing pyrrolidinylacetamide derivatives
US7450138B2 (en) *	2005-02-09	2008-11-11	Ricoh Company, Ltd.	Controlling timing for starting image formation

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3944629A (en) *	1974-06-24	1976-03-16	Monsanto Company	Polyester initiated anionic catalyzed polymerization of lactam
US3993709A (en) *	1974-06-24	1976-11-23	Monsanto Company	Polyester initiated anionic catalyzed polymerization of lactam
US3922254A (en) *	1974-07-22	1975-11-25	Monsanto Co	Catalytic process for imide-alcohol condensation
US4678839A (en) *	1985-07-08	1987-07-07	General Electric Company	Mixtures including polyphenylene ethers and lactams and resinous compositions prepared therefrom
JPS62182378A (ja) *	1986-02-03	1987-08-10	トヨタ自動車株式会社	車両のラゲ−ジドアロツク装置

1989
- 1989-04-14 NL NL8900937A patent/NL8900937A/nl not_active Application Discontinuation
1990
- 1990-04-11 EP EP90200888A patent/EP0392633B1/de not_active Expired - Lifetime
- 1990-04-11 ES ES90200888T patent/ES2071745T3/es not_active Expired - Lifetime
- 1990-04-11 AT AT90200888T patent/ATE120779T1/de not_active IP Right Cessation
- 1990-04-11 DK DK90200888.7T patent/DK0392633T3/da active
- 1990-04-11 DE DE69018298T patent/DE69018298T2/de not_active Expired - Fee Related
- 1990-04-12 US US07/507,851 patent/US5059687A/en not_active Expired - Fee Related
- 1990-04-12 CA CA002014480A patent/CA2014480A1/en not_active Abandoned
- 1990-04-13 KR KR1019900005265A patent/KR930005149B1/ko not_active Expired - Fee Related
- 1990-04-16 JP JP2097822A patent/JPH03115326A/ja active Pending

Also Published As

Publication number	Publication date
DK0392633T3 (da)	1995-07-31
KR900016288A (ko)	1990-11-13
CA2014480A1 (en)	1990-10-14
ATE120779T1 (de)	1995-04-15
DE69018298T2 (de)	1996-01-11
JPH03115326A (ja)	1991-05-16
ES2071745T3 (es)	1995-07-01
KR930005149B1 (ko)	1993-06-16
EP0392633B1 (de)	1995-04-05
US5059687A (en)	1991-10-22
EP0392633A1 (de)	1990-10-17
DE69018298D1 (de)	1995-05-11

Legal Events

Date	Code	Title	Description
1990-11-01	A1B	A search report has been drawn up
1993-01-18	CNR	Transfer of rights (patent application after its laying open for public inspection)	Free format text: DSM N.V.
1996-01-02	BV	The patent application has lapsed

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NL8900937A (nl)	1990-11-01	Werkwijze voor de condensatie van imiden en alkoholen of aminen.
KR900015870A (ko)	1990-11-10	단량체 성형 방법에 의한 슬라이딩 커플링 제조방법
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KR910003843B1 (ko)	1991-06-12	락탐중합개시제 및 그 제조방법
DE4033165A1 (de)	1992-04-23	Verfahren zur kondensation von imiden und alkoholen oder aminen
Rahman et al.	1979	Block Polymers Derived from Poly (ethylene Oxide) and Hydroxy-Terminated Polybutadiene
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JPS60240727A (ja)	1985-11-29	ポリアミドブロツク共重合体