NO312954B1 - Fremgangsmåte for fremstilling av partikler av smeltedyktige driv- og eksplosivstoffer - Google Patents

Fremgangsmåte for fremstilling av partikler av smeltedyktige driv- og eksplosivstoffer Download PDF

Info

Publication number: NO312954B1
Authority: NO; Norway
Prior art keywords: matrix liquid; emulsion; substance; particles; melt
Prior art date: 1998-04-16

Application number

NO19991178A

Other languages

English (en)

Norwegian (no)

Other versions

NO991178D0 (no

NO991178L (no

Inventor

Ulrich Teipel

Horst Krause

Karlfred Leisinger

Thomas Heintz

Original Assignee

Fraunhofer Ges Forschung

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1998-04-16

Filing date

1999-03-10

Publication date

2002-07-22

1999-03-10 Application filed by Fraunhofer Ges Forschung filed Critical Fraunhofer Ges Forschung

1999-03-10 Publication of NO991178D0 publication Critical patent/NO991178D0/no

1999-10-18 Publication of NO991178L publication Critical patent/NO991178L/no

2002-07-22 Publication of NO312954B1 publication Critical patent/NO312954B1/no

Links

238000000034 method Methods 0.000 title claims description 25
239000002245 particle Substances 0.000 title claims description 25
239000002360 explosive Substances 0.000 title claims description 23
239000003380 propellant Substances 0.000 title claims description 10
238000002360 preparation method Methods 0.000 title description 4
BRUFJXUJQKYQHA-UHFFFAOYSA-O ammonium dinitramide Chemical compound [NH4+].[O-][N+](=O)[N-][N+]([O-])=O BRUFJXUJQKYQHA-UHFFFAOYSA-O 0.000 claims description 33
239000000839 emulsion Substances 0.000 claims description 32
239000007788 liquid Substances 0.000 claims description 29
239000011159 matrix material Substances 0.000 claims description 29
239000000126 substance Substances 0.000 claims description 22
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 12
238000002425 crystallisation Methods 0.000 claims description 11
230000008025 crystallization Effects 0.000 claims description 11
238000004519 manufacturing process Methods 0.000 claims description 10
239000007787 solid Substances 0.000 claims description 9
239000000155 melt Substances 0.000 claims description 8
238000001953 recrystallisation Methods 0.000 claims description 8
239000012798 spherical particle Substances 0.000 claims description 8
239000005662 Paraffin oil Substances 0.000 claims description 6
239000000654 additive Substances 0.000 claims description 6
238000002844 melting Methods 0.000 claims description 6
230000008018 melting Effects 0.000 claims description 6
235000012239 silicon dioxide Nutrition 0.000 claims description 6
239000000377 silicon dioxide Substances 0.000 claims description 6
238000004581 coalescence Methods 0.000 claims description 4
238000001816 cooling Methods 0.000 claims description 4
238000002604 ultrasonography Methods 0.000 claims description 4
229920002545 silicone oil Polymers 0.000 claims description 3
239000003921 oil Substances 0.000 claims description 2
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 9
239000012071 phase Substances 0.000 description 7
239000007800 oxidant agent Substances 0.000 description 5
238000000926 separation method Methods 0.000 description 5
239000003995 emulsifying agent Substances 0.000 description 4
230000002209 hydrophobic effect Effects 0.000 description 4
230000015572 biosynthetic process Effects 0.000 description 3
239000000203 mixture Substances 0.000 description 3
244000052616 bacterial pathogen Species 0.000 description 2
238000010924 continuous production Methods 0.000 description 2
239000013078 crystal Substances 0.000 description 2
239000000446 fuel Substances 0.000 description 2
239000000463 material Substances 0.000 description 2
239000000047 product Substances 0.000 description 2
150000003839 salts Chemical class 0.000 description 2
239000002904 solvent Substances 0.000 description 2
239000003381 stabilizer Substances 0.000 description 2
238000003756 stirring Methods 0.000 description 2
238000005496 tempering Methods 0.000 description 2
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
230000000996 additive effect Effects 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
239000000084 colloidal system Substances 0.000 description 1
239000000356 contaminant Substances 0.000 description 1
239000012297 crystallization seed Substances 0.000 description 1
238000005474 detonation Methods 0.000 description 1
238000009826 distribution Methods 0.000 description 1
238000004945 emulsification Methods 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
238000001914 filtration Methods 0.000 description 1
238000010304 firing Methods 0.000 description 1
239000012530 fluid Substances 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
230000001788 irregular Effects 0.000 description 1
238000010899 nucleation Methods 0.000 description 1
239000008385 outer phase Substances 0.000 description 1
239000012188 paraffin wax Substances 0.000 description 1
238000004062 sedimentation Methods 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
239000010703 silicon Substances 0.000 description 1
239000007790 solid phase Substances 0.000 description 1
238000001228 spectrum Methods 0.000 description 1
230000002269 spontaneous effect Effects 0.000 description 1
239000007858 starting material Substances 0.000 description 1
230000003068 static effect Effects 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0033—Shaping the mixture
- C06B21/0066—Shaping the mixture by granulation, e.g. flaking
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0033—Shaping the mixture
- C06B21/005—By a process involving melting at least part of the ingredients
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B31/00—Compositions containing an inorganic nitrogen-oxygen salt

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Colloid Chemistry (AREA)
Silicon Compounds (AREA)
Medicinal Preparation (AREA)

NO19991178A 1998-04-16 1999-03-10 Fremgangsmåte for fremstilling av partikler av smeltedyktige driv- og eksplosivstoffer NO312954B1 (no)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE1998116853 DE19816853A1 (de)	1998-04-16	1998-04-16	Verfahren zur Herstellung von Partikeln schmelzfähiger Treib- und Explosivstoffe

Publications (3)

Publication Number	Publication Date
NO991178D0 NO991178D0 (no)	1999-03-10
NO991178L NO991178L (no)	1999-10-18
NO312954B1 true NO312954B1 (no)	2002-07-22

Family

ID=7864703

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO19991178A NO312954B1 (no)	1998-04-16	1999-03-10	Fremgangsmåte for fremstilling av partikler av smeltedyktige driv- og eksplosivstoffer

Country Status (3)

Country	Link
EP (1)	EP0953555B1 (de)
DE (2)	DE19816853A1 (de)
NO (1)	NO312954B1 (de)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE10201937B4 (de) *	2002-01-19	2005-08-04	Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V.	Verfahren zur Herstellung von mit Additiven versetztem Ammoniumdinitramid (ADN)
FR2884244B1 (fr) *	2005-04-12	2007-07-06	Snpe Materiaux Energetiques Sa	Obtention de cristaux de dinitroamidure d'ammonium (adn); cristaux d'adn et les composites energetiques en contenant.
FR3081864B1 (fr) *	2018-05-30	2022-03-18	Arianegroup Sas	Obtention de cristaux de dinitroamidure d'ammmonium (adn) ; cristaux d'adn et les composites energetiques en contenant
DE102020122328B3 (de)	2020-08-26	2021-08-12	Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung eingetragener Verein	Verfahren zur Herstellung von Partikeln aus Ammoniumdinitramid (ADN)

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
NL85445C (de) *	1955-02-23
US3522334A (en) *	1961-05-09	1970-07-28	Exxon Research Engineering Co	Preparation of spherical solid oxidizer pellets from nitronium perchlorate-lithium perchlorate mixture
DE1467203B2 (de) *	1964-09-09	1974-03-28	Bundesrepublik Deutschland Vertr. Durch Den Bundesminister Der Verteidigung, 5300 Bonn	Verfahren zum Herstellen von kugeligem Ammoniumnitrat
US3468986A (en) *	1966-11-15	1969-09-23	David J Watanabe	Method for producing a solid particulate material
US4118797A (en) *	1977-10-25	1978-10-03	Energy And Minerals Research Co.	Ultrasonic emulsifier and method
IT1096661B (it) *	1978-06-13	1985-08-26	Montedison Spa	Procedimento per la preparazione di prodotti in forma sferoidale solidi a temperatura ambiente
EP0238210A3 (en) *	1986-03-14	1989-05-24	Imperial Chemical Industries Plc	Solid explosive composition
BE1002001A4 (fr) *	1988-02-18	1990-05-15	Mitsubishi Mining & Cement Co	Procede de preparation de microspheres ceramiques.
JPH07503798A (ja) *	1992-02-14	1995-04-20	リサーチ　ラボラトリース　オブ　オーストラリア　プロプライエタリー　リミテッド	静電写真法に有用な球形粒子
US5688742A (en) *	1995-08-18	1997-11-18	Rohm And Haas Company	Water based formation of a beaded product
US5801453A (en) *	1996-06-11	1998-09-01	United Technologies Corporation	Process for preparing spherical energetic compounds

1998
- 1998-04-16 DE DE1998116853 patent/DE19816853A1/de not_active Withdrawn
1999
- 1999-03-10 NO NO19991178A patent/NO312954B1/no unknown
- 1999-03-23 DE DE59912567T patent/DE59912567D1/de not_active Expired - Lifetime
- 1999-03-23 EP EP19990105812 patent/EP0953555B1/de not_active Expired - Lifetime

Also Published As

Publication number	Publication date
DE59912567D1 (de)	2006-02-02
EP0953555B1 (de)	2005-09-21
DE19816853A1 (de)	1999-10-21
NO991178D0 (no)	1999-03-10
NO991178L (no)	1999-10-18
EP0953555A1 (de)	1999-11-03

Publication	Publication Date	Title
Lu et al.	2012	Crystallization of an active pharmaceutical ingredient that oils out
US5360478A (en)	1994-11-01	Gas anti-solvent recrystallization process
Teipel	1999	Production of particles of explosives
US4746380A (en)	1988-05-24	Explosive compound comprising ammonium nitrate and glycine
US5801453A (en)	1998-09-01	Process for preparing spherical energetic compounds
NO312954B1 (no)	2002-07-22	Fremgangsmåte for fremstilling av partikler av smeltedyktige driv- og eksplosivstoffer
Jin et al.	2024	Spherical core-shell CL-20@ LLM-105 composites with excellent mechanical sensibility obtained by Pickering emulsion
US4997494A (en)	1991-03-05	Chemically gassed emulsion explosive
EP1256558A2 (de)	2002-11-13	Verfahren zur Herstellung von Kristallen aus in einem Lösungsmittel gelösten Treib-, Explosivstoffen und Oxidatoren
US4600451A (en)	1986-07-15	Perchlorate based microknit composite explosives and processes for making same
US8491736B2 (en)	2013-07-23	Method for obtaining ADN crystals through crystallization in a viscous medium
US4994124A (en)	1991-02-19	Sensitized explosive
KR101573616B1 (ko)	2015-12-01	구아닐우레아 디니트라미드의 재결정에 의한 형상 및 입도 조절방법
DE69224230T2 (de)	1998-05-28	Geschäumten Sensibilisator enthaltender Sprengstoff
US5700970A (en)	1997-12-23	Broken-emulsion and process for recycling emulsion explosives
Yang et al.	2024	Formation of flake-like DAAF crystals with tunable size realized on a microfluidic platform for binder-free initiator explosives
DE102004004964A1 (de)	2005-08-18	Verfahren zur Herstellung von Komposit-Partikeln aus kristallinen Explosivstoffen
EP0493638A1 (de)	1992-07-08	Compositsprengstoffe und Verfahren zu ihrer Herstellung
DE10201937A1 (de)	2003-08-07	Verfahren zur Herstellung von mit Additiven versetztem Ammoniumdinitramid (ADN)
DE102004002318A1 (de)	2005-08-11	Verfahren zur Herstellung feindisperser kristallinger Treib-, Explosivstoffe und Oxidatoren
Li et al.	2025	Controlled fabrication of spherical HNS with Micro/Nano secondary structure for performance augmentation
CA2183010A1 (en)	1998-02-10	Waste emulsion recycling process
CZ9902408A3 (cs)	2000-10-11	Výbušná emulze pro náložky
Radulescu et al.	2018	Formation of ADN-prills in microfluidic droplet generators
Heintz et al.	2010	Continuous production of spherical ammonium dinitramide particles (ADN-prills) by microreaction technology