NO831000L - Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblandinger - Google Patents

Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblandinger

Info

Publication number: NO831000L
Authority: NO; Norway
Prior art keywords: amine; sulfuric acid; paraffin; acid; weight
Prior art date: 1982-03-23

Application number

NO831000A

Other languages

English (en)

Norwegian (no)

Inventor

Bernhard Mees

Herbert Ramloch

Original Assignee

Hoechst Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1982-03-23

Filing date

1983-03-22

Publication date

1983-09-26

1983-03-22 Application filed by Hoechst Ag filed Critical Hoechst Ag

1983-09-26 Publication of NO831000L publication Critical patent/NO831000L/no

Links

QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title claims description 104
238000000034 method Methods 0.000 title claims description 22
239000011541 reaction mixture Substances 0.000 title claims description 6
150000001412 amines Chemical class 0.000 claims description 49
239000012188 paraffin wax Substances 0.000 claims description 29
-1 amine sulfate Chemical class 0.000 claims description 24
239000002253 acid Substances 0.000 claims description 23
239000000203 mixture Substances 0.000 claims description 20
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
150000003839 salts Chemical class 0.000 claims description 5
229910021653 sulphate ion Inorganic materials 0.000 claims description 5
238000009835 boiling Methods 0.000 claims description 3
238000000605 extraction Methods 0.000 claims description 3
238000001256 steam distillation Methods 0.000 claims description 3
239000003513 alkali Substances 0.000 claims description 2
229910001854 alkali hydroxide Inorganic materials 0.000 claims description 2
150000008044 alkali metal hydroxides Chemical class 0.000 claims description 2
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 18
238000000926 separation method Methods 0.000 description 18
239000012071 phase Substances 0.000 description 17
JQVDAXLFBXTEQA-UHFFFAOYSA-N dibutylamine Chemical compound CCCCNCCCC JQVDAXLFBXTEQA-UHFFFAOYSA-N 0.000 description 10
235000011121 sodium hydroxide Nutrition 0.000 description 6
239000000243 solution Substances 0.000 description 4
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
125000000217 alkyl group Chemical group 0.000 description 3
150000003863 ammonium salts Chemical class 0.000 description 3
229910052739 hydrogen Inorganic materials 0.000 description 3
239000001257 hydrogen Substances 0.000 description 3
CDULGHZNHURECF-UHFFFAOYSA-N 2,3-dimethylaniline 2,4-dimethylaniline 2,5-dimethylaniline 2,6-dimethylaniline 3,4-dimethylaniline 3,5-dimethylaniline Chemical group CC1=CC=C(N)C(C)=C1.CC1=CC=C(C)C(N)=C1.CC1=CC(C)=CC(N)=C1.CC1=CC=C(N)C=C1C.CC1=CC=CC(N)=C1C.CC1=CC=CC(C)=C1N CDULGHZNHURECF-UHFFFAOYSA-N 0.000 description 2
MLPVBIWIRCKMJV-UHFFFAOYSA-N 2-ethylaniline Chemical compound CCC1=CC=CC=C1N MLPVBIWIRCKMJV-UHFFFAOYSA-N 0.000 description 2
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
OJGMBLNIHDZDGS-UHFFFAOYSA-N N-Ethylaniline Chemical compound CCNC1=CC=CC=C1 OJGMBLNIHDZDGS-UHFFFAOYSA-N 0.000 description 2
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
125000001931 aliphatic group Chemical group 0.000 description 2
125000002947 alkylene group Chemical group 0.000 description 2
125000004432 carbon atom Chemical group C* 0.000 description 2
PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 description 2
230000000694 effects Effects 0.000 description 2
239000003350 kerosene Substances 0.000 description 2
238000002156 mixing Methods 0.000 description 2
JACMPVXHEARCBO-UHFFFAOYSA-N n-pentylpentan-1-amine Chemical compound CCCCCNCCCCC JACMPVXHEARCBO-UHFFFAOYSA-N 0.000 description 2
RNVCVTLRINQCPJ-UHFFFAOYSA-N o-toluidine Chemical compound CC1=CC=CC=C1N RNVCVTLRINQCPJ-UHFFFAOYSA-N 0.000 description 2
239000012266 salt solution Substances 0.000 description 2
239000002904 solvent Substances 0.000 description 2
238000003756 stirring Methods 0.000 description 2
238000006277 sulfonation reaction Methods 0.000 description 2
229910052717 sulfur Inorganic materials 0.000 description 2
239000011593 sulfur Substances 0.000 description 2
150000003467 sulfuric acid derivatives Chemical class 0.000 description 2
125000005270 trialkylamine group Chemical group 0.000 description 2
IMFACGCPASFAPR-UHFFFAOYSA-N tributylamine Chemical compound CCCCN(CCCC)CCCC IMFACGCPASFAPR-UHFFFAOYSA-N 0.000 description 2
GEYOCULIXLDCMW-UHFFFAOYSA-N 1,2-phenylenediamine Chemical compound NC1=CC=CC=C1N GEYOCULIXLDCMW-UHFFFAOYSA-N 0.000 description 1
BMVXCPBXGZKUPN-UHFFFAOYSA-N 1-hexanamine Chemical compound CCCCCCN BMVXCPBXGZKUPN-UHFFFAOYSA-N 0.000 description 1
NJBCRXCAPCODGX-UHFFFAOYSA-N 2-methyl-n-(2-methylpropyl)propan-1-amine Chemical compound CC(C)CNCC(C)C NJBCRXCAPCODGX-UHFFFAOYSA-N 0.000 description 1
FDECURPHVMNAKO-UHFFFAOYSA-N 4-nonylaniline Chemical compound CCCCCCCCCC1=CC=C(N)C=C1 FDECURPHVMNAKO-UHFFFAOYSA-N 0.000 description 1
PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 1
LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
XBPCUCUWBYBCDP-UHFFFAOYSA-N Dicyclohexylamine Chemical compound C1CCCCC1NC1CCCCC1 XBPCUCUWBYBCDP-UHFFFAOYSA-N 0.000 description 1
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
WJYIASZWHGOTOU-UHFFFAOYSA-N Heptylamine Chemical compound CCCCCCCN WJYIASZWHGOTOU-UHFFFAOYSA-N 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
150000001408 amides Chemical class 0.000 description 1
239000008346 aqueous phase Substances 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
150000004982 aromatic amines Chemical class 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
OCPOLAAAWHQKCX-UHFFFAOYSA-N dipentylazanium sulfate Chemical compound [O-]S([O-])(=O)=O.CCCCC[NH2+]CCCCC.CCCCC[NH2+]CCCCC OCPOLAAAWHQKCX-UHFFFAOYSA-N 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000012467 final product Substances 0.000 description 1
239000012458 free base Substances 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
150000002431 hydrogen Chemical class 0.000 description 1
150000002576 ketones Chemical class 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000004530 micro-emulsion Substances 0.000 description 1
FRQONEWDWWHIPM-UHFFFAOYSA-N n,n-dicyclohexylcyclohexanamine Chemical compound C1CCCCC1N(C1CCCCC1)C1CCCCC1 FRQONEWDWWHIPM-UHFFFAOYSA-N 0.000 description 1
DIAIBWNEUYXDNL-UHFFFAOYSA-N n,n-dihexylhexan-1-amine Chemical compound CCCCCCN(CCCCCC)CCCCCC DIAIBWNEUYXDNL-UHFFFAOYSA-N 0.000 description 1
OOHAUGDGCWURIT-UHFFFAOYSA-N n,n-dipentylpentan-1-amine Chemical compound CCCCCN(CCCCC)CCCCC OOHAUGDGCWURIT-UHFFFAOYSA-N 0.000 description 1
MTHFROHDIWGWFD-UHFFFAOYSA-N n-butyl-n-methylbutan-1-amine Chemical compound CCCCN(C)CCCC MTHFROHDIWGWFD-UHFFFAOYSA-N 0.000 description 1
238000006386 neutralization reaction Methods 0.000 description 1
IOQPZZOEVPZRBK-UHFFFAOYSA-N octan-1-amine Chemical compound CCCCCCCCN IOQPZZOEVPZRBK-UHFFFAOYSA-N 0.000 description 1
239000012074 organic phase Substances 0.000 description 1
RZXMPPFPUUCRFN-UHFFFAOYSA-N p-toluidine Chemical compound CC1=CC=C(N)C=C1 RZXMPPFPUUCRFN-UHFFFAOYSA-N 0.000 description 1
229940100684 pentylamine Drugs 0.000 description 1
238000005191 phase separation Methods 0.000 description 1
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 description 1
239000003495 polar organic solvent Substances 0.000 description 1
239000002798 polar solvent Substances 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
159000000000 sodium salts Chemical class 0.000 description 1
229910052938 sodium sulfate Inorganic materials 0.000 description 1
235000011152 sodium sulphate Nutrition 0.000 description 1
RPACBEVZENYWOL-XFULWGLBSA-M sodium;(2r)-2-[6-(4-chlorophenoxy)hexyl]oxirane-2-carboxylate Chemical compound [Na+].C=1C=C(Cl)C=CC=1OCCCCCC[C@]1(C(=O)[O-])CO1 RPACBEVZENYWOL-XFULWGLBSA-M 0.000 description 1
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/42—Separation; Purification; Stabilisation; Use of additives

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Catalysts (AREA)

NO831000A 1982-03-23 1983-03-22 Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblandinger NO831000L (no)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE19823210573 DE3210573A1 (de)	1982-03-23	1982-03-23	Verfahren zum abtrennen von schwefelsaeure aus dem bei der sulfoxidation von paraffinen anfallenden reaktionsgemisch

Publications (1)

Publication Number	Publication Date
NO831000L true NO831000L (no)	1983-09-26

Family

ID=6159035

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO831000A NO831000L (no)	1982-03-23	1983-03-22	Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblandinger

Country Status (12)

Country	Link
EP (1)	EP0089653A3 (cs)
JP (1)	JPS58172363A (cs)
AR (1)	AR229069A1 (cs)
AU (1)	AU1270683A (cs)
BR (1)	BR8301442A (cs)
CS (1)	CS195783A2 (cs)
DD (1)	DD209441A5 (cs)
DE (1)	DE3210573A1 (cs)
ES (1)	ES8402564A1 (cs)
NO (1)	NO831000L (cs)
YU (1)	YU67983A (cs)
ZA (1)	ZA831993B (cs)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE3801942A1 (de) *	1988-01-23	1989-07-27	Basf Ag	Verfahren zur herstellung von alkalisalzen der biphenyl-4,4'-disulfonsaeure

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE1593860B1 (de) *	1967-03-15	1971-02-11	Hoechst Ag	Verfahren zur Herstellung von Aminsalzen von n-Paraffinsulfonsaeuren
US3719703A (en) *	1969-04-29	1973-03-06	Atomic Energy Commission	Separation of sulfonic acids from sulfuric acid
US3720707A (en) *	1970-02-27	1973-03-13	Labofina Sa	Process for reducing the sulfuric acid content of alkylarylsulfonic acids
CH534670A (fr) *	1970-08-07	1973-03-15	Aquitaine Petrole	Procédé pour la séparation des acides sulfoniques contenus dans une solution sulfonique brute
IT1074825B (it) *	1977-01-11	1985-04-20	Euteco Spa	Procedimento per la purificazione di acidi alchilsolfonici
DE3048058C2 (de) *	1980-12-19	1983-04-28	Hoechst Ag, 6230 Frankfurt	Verfahren zur Abtrennung von Schwefelsäure aus dem bei der Sulfoxidation von n-Paraffinen anfallenden rohen Sulfonierungsgemisch

1982
- 1982-03-23 DE DE19823210573 patent/DE3210573A1/de not_active Withdrawn
1983
- 1983-03-19 EP EP83102734A patent/EP0089653A3/de not_active Withdrawn
- 1983-03-21 ES ES520801A patent/ES8402564A1/es not_active Expired
- 1983-03-21 DD DD83249010A patent/DD209441A5/de unknown
- 1983-03-21 YU YU00679/83A patent/YU67983A/xx unknown
- 1983-03-21 AR AR292452A patent/AR229069A1/es active
- 1983-03-22 JP JP58046088A patent/JPS58172363A/ja active Pending
- 1983-03-22 CS CS831957A patent/CS195783A2/cs unknown
- 1983-03-22 BR BR8301442A patent/BR8301442A/pt unknown
- 1983-03-22 AU AU12706/83A patent/AU1270683A/en not_active Abandoned
- 1983-03-22 ZA ZA831993A patent/ZA831993B/xx unknown
- 1983-03-22 NO NO831000A patent/NO831000L/no unknown

Also Published As

Publication number	Publication date
CS195783A2 (en)	1985-07-16
AU1270683A (en)	1983-09-29
BR8301442A (pt)	1983-11-29
ES520801A0 (es)	1984-02-01
JPS58172363A (ja)	1983-10-11
DE3210573A1 (de)	1983-10-06
ZA831993B (en)	1983-11-30
AR229069A1 (es)	1983-05-31
EP0089653A2 (de)	1983-09-28
ES8402564A1 (es)	1984-02-01
YU67983A (en)	1986-02-28
EP0089653A3 (de)	1984-05-23
DD209441A5 (de)	1984-05-09

Publication	Publication Date	Title
JP2017533883A (ja)	2017-11-16	アルカリイセチオン酸塩およびアルカリビニルスルホン酸塩からタウリンを生産するための循環プロセス
US4251671A (en)	1981-02-17	Extraction of citric acid
NO831000L (no)	1983-09-26	Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblandinger
BR112016026310B1 (pt)	2021-11-16	Processo para a reação de compostos químicos
US2820056A (en)	1958-01-14	Alkaryl sulfonates
NO814347L (no)	1982-06-21	Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblanding
US3063806A (en)	1962-11-13	Process for the production of anhydrous hydrazine
US2127495A (en)	1938-08-23	Manufacture of nitrogen base salts of acid alkyl esters
EP0593551B1 (en)	1997-10-15	Process for making alkyl naphthalene sulfonate surfactants
PT91757B (pt)	1995-05-31	Processo de preparacao de gama-butirobetaina
US2497130A (en)	1950-02-14	Manufacture of sulfoaryl-amides of aromatic carboxylic acids
US3577456A (en)	1971-05-04	Process for the manufacture of aqueous alkali paraffin sulphonate solutions containing small amounts of alkali sulfate
JPS6038356A (ja)	1985-02-27	パラフインのスルホキシド化の際に得られる反応混合物からパラフイン‐スルホン酸またはパラフイン‐スルホナートを穏やかな条件下で単離する方法
JPS60146854A (ja)	1985-08-02	ニトリロ三酢酸塩の製造方法
JP5463839B2 (ja)	2014-04-09	２−ヒドロキシ−４−メチルチオブタン酸の製造方法
US1406745A (en)	1922-02-14	Manufacture of resorcinol
Blood et al.	1930	LXXI.—The reactivity of halogen atoms in compounds of the pyridine series. Part I. The halides of 2-stilbazole
SU48139A1 (ru)	1936-08-31	Способ выделени солей кислых сернокислых эфиров лейко-соединений кубовых красителей
SU148808A1 (ru)	1961-11-30	Способ получени третичных ароматических алкиламинов
US2407351A (en)	1946-09-10	Process for the manufacture of o-sulphobenzoic acids
Robson et al.	1952	The direct isolation of arginine and lysine picrates from gelatin hydrolysates
JP2731816B2 (ja)	1998-03-25	クレゾールの精製方法
US1863676A (en)	1932-06-21	Amino-hydroxy pyridine and process of preparing the same
SU614104A1 (ru)	1978-07-05	Способ получени 1,8-нафтсультама
DE707029C (de)	1941-06-11	Verfahren zur Herstellung als Druckhilfsstoffe geeigneter quartaerer Ammoniumverbindungen