NO841623L - Framgangsmaate for bearbeiding av metalliske diboridpulvere - Google Patents

Framgangsmaate for bearbeiding av metalliske diboridpulvere

Info

Publication number: NO841623L
Authority: NO; Norway
Prior art keywords: titanium; powder; reaction; gaseous; trichloride
Prior art date: 1983-04-26

Application number

NO841623A

Other languages

English (en)

Norwegian (no)

Inventor

Jorulf Brynestad

Carlos E Bamberger

Original Assignee

Us Energy

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-04-26

Filing date

1984-04-25

Publication date

1984-10-29

1984-04-25 Application filed by Us Energy filed Critical Us Energy

1984-10-29 Publication of NO841623L publication Critical patent/NO841623L/no

Links

239000000843 powder Substances 0.000 title claims description 37
238000000034 method Methods 0.000 title claims description 19
QYEXBYZXHDUPRC-UHFFFAOYSA-N B#[Ti]#B Chemical compound B#[Ti]#B QYEXBYZXHDUPRC-UHFFFAOYSA-N 0.000 claims description 28
229910033181 TiB2 Inorganic materials 0.000 claims description 28
239000010936 titanium Substances 0.000 claims description 20
229910052719 titanium Inorganic materials 0.000 claims description 15
FAQYAMRNWDIXMY-UHFFFAOYSA-N trichloroborane Chemical compound ClB(Cl)Cl FAQYAMRNWDIXMY-UHFFFAOYSA-N 0.000 claims description 15
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 14
YONPGGFAJWQGJC-UHFFFAOYSA-K titanium(iii) chloride Chemical compound Cl[Ti](Cl)Cl YONPGGFAJWQGJC-UHFFFAOYSA-K 0.000 claims description 13
ZWYDDDAMNQQZHD-UHFFFAOYSA-L titanium(ii) chloride Chemical compound [Cl-].[Cl-].[Ti+2] ZWYDDDAMNQQZHD-UHFFFAOYSA-L 0.000 claims description 12
229910007948 ZrB2 Inorganic materials 0.000 claims description 5
VWZIXVXBCBBRGP-UHFFFAOYSA-N boron;zirconium Chemical compound B#[Zr]#B VWZIXVXBCBBRGP-UHFFFAOYSA-N 0.000 claims description 5
239000000463 material Substances 0.000 claims description 5
229910052845 zircon Inorganic materials 0.000 claims description 4
GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 claims description 4
238000006243 chemical reaction Methods 0.000 description 27
239000002245 particle Substances 0.000 description 23
229910052751 metal Inorganic materials 0.000 description 15
239000002184 metal Substances 0.000 description 15
239000007787 solid Substances 0.000 description 15
239000000047 product Substances 0.000 description 12
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 10
XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 9
238000002474 experimental method Methods 0.000 description 8
229910003074 TiCl4 Inorganic materials 0.000 description 6
238000004519 manufacturing process Methods 0.000 description 6
229910015844 BCl3 Inorganic materials 0.000 description 5
229910010068 TiCl2 Inorganic materials 0.000 description 5
229910052796 boron Inorganic materials 0.000 description 5
229910052759 nickel Inorganic materials 0.000 description 5
ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 4
238000002441 X-ray diffraction Methods 0.000 description 4
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
239000007795 chemical reaction product Substances 0.000 description 4
239000001301 oxygen Substances 0.000 description 4
229910052760 oxygen Inorganic materials 0.000 description 4
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 3
230000015572 biosynthetic process Effects 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
239000007789 gas Substances 0.000 description 3
239000007788 liquid Substances 0.000 description 3
238000005096 rolling process Methods 0.000 description 3
238000005245 sintering Methods 0.000 description 3
239000000126 substance Substances 0.000 description 3
238000003786 synthesis reaction Methods 0.000 description 3
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
229910010062 TiCl3 Inorganic materials 0.000 description 2
-1 boron halide Chemical class 0.000 description 2
239000000460 chlorine Substances 0.000 description 2
239000013078 crystal Substances 0.000 description 2
230000003628 erosive effect Effects 0.000 description 2
229910002804 graphite Inorganic materials 0.000 description 2
239000010439 graphite Substances 0.000 description 2
238000002844 melting Methods 0.000 description 2
230000008018 melting Effects 0.000 description 2
239000012071 phase Substances 0.000 description 2
239000000376 reactant Substances 0.000 description 2
239000007858 starting material Substances 0.000 description 2
238000004627 transmission electron microscopy Methods 0.000 description 2
YPSXFMHXRZAGTG-UHFFFAOYSA-N 4-methoxy-2-[2-(5-methoxy-2-nitrosophenyl)ethyl]-1-nitrosobenzene Chemical compound COC1=CC=C(N=O)C(CCC=2C(=CC=C(OC)C=2)N=O)=C1 YPSXFMHXRZAGTG-UHFFFAOYSA-N 0.000 description 1
102100021569 Apoptosis regulator Bcl-2 Human genes 0.000 description 1
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
229910003862 HfB2 Inorganic materials 0.000 description 1
101000971171 Homo sapiens Apoptosis regulator Bcl-2 Proteins 0.000 description 1
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
238000007630 basic procedure Methods 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
229910052801 chlorine Inorganic materials 0.000 description 1
238000002485 combustion reaction Methods 0.000 description 1
238000010960 commercial process Methods 0.000 description 1
239000004035 construction material Substances 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 1
238000004821 distillation Methods 0.000 description 1
238000010891 electric arc Methods 0.000 description 1
239000012467 final product Substances 0.000 description 1
239000010419 fine particle Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
229910052735 hafnium Inorganic materials 0.000 description 1
VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
239000012535 impurity Substances 0.000 description 1
239000005300 metallic glass Substances 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
239000000203 mixture Substances 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
150000004767 nitrides Chemical class 0.000 description 1
230000006911 nucleation Effects 0.000 description 1
238000010899 nucleation Methods 0.000 description 1
239000008188 pellet Substances 0.000 description 1
238000003825 pressing Methods 0.000 description 1
230000002035 prolonged effect Effects 0.000 description 1
230000005855 radiation Effects 0.000 description 1
239000011819 refractory material Substances 0.000 description 1
230000000717 retained effect Effects 0.000 description 1
238000010301 surface-oxidation reaction Methods 0.000 description 1
238000012360 testing method Methods 0.000 description 1
GBECUEIQVRDUKB-UHFFFAOYSA-M thallium monochloride Chemical compound [Tl]Cl GBECUEIQVRDUKB-UHFFFAOYSA-M 0.000 description 1
239000012808 vapor phase Substances 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
229910052726 zirconium Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B35/00—Boron; Compounds thereof
- C01B35/02—Boron; Borides
- C01B35/04—Metal borides
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S977/00—Nanotechnology
- Y10S977/70—Nanostructure
- Y10S977/773—Nanoparticle, i.e. structure having three dimensions of 100 nm or less
- Y10S977/775—Nanosized powder or flake, e.g. nanosized catalyst
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S977/00—Nanotechnology
- Y10S977/84—Manufacture, treatment, or detection of nanostructure
- Y10S977/895—Manufacture, treatment, or detection of nanostructure having step or means utilizing chemical property
- Y10S977/896—Chemical synthesis, e.g. chemical bonding or breaking

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Ceramic Products (AREA)
Inorganic Compounds Of Heavy Metals (AREA)

NO841623A 1983-04-26 1984-04-25 Framgangsmaate for bearbeiding av metalliske diboridpulvere NO841623L (no)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US06/488,870 US4503021A (en)	1983-04-26	1983-04-26	Preparation of titanium diboride powder

Publications (1)

Publication Number	Publication Date
NO841623L true NO841623L (no)	1984-10-29

Family

ID=23941456

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO841623A NO841623L (no)	1983-04-26	1984-04-25	Framgangsmaate for bearbeiding av metalliske diboridpulvere

Country Status (8)

Country	Link
US (1)	US4503021A (it)
JP (1)	JPS59207835A (it)
CA (1)	CA1209786A (it)
DE (1)	DE3415611A1 (it)
FR (1)	FR2545077A1 (it)
GB (1)	GB2138794B (it)
IT (1)	IT1176115B (it)
NO (1)	NO841623L (it)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4888166A (en) *	1986-09-03	1989-12-19	Georgia Tech Research Corporation	Process for making highly reactive sub-micron amorphous titanium diboride powder
JPH0643248B2 (ja) *	1987-09-18	1994-06-08	科学技術庁金属材料技術研究所長	遷移金属ほう化物繊維の製造法
US5169832A (en) *	1988-07-12	1992-12-08	The Dow Chemical Company	Synthesis of refractory metal boride powders of predetermined particle size
US5227195A (en) *	1989-04-04	1993-07-13	Sri International	Low temperature method of forming materials using one or more metal reactants and a halogen-containing reactant to form one or more reactive intermediates
US5149514A (en) *	1989-04-04	1992-09-22	Sri International	Low temperature method of forming materials using one or more metal reactants and a halogen-containing reactant to form one or more reactive intermediates
WO1991003423A1 (en) *	1989-08-28	1991-03-21	Logan Kathryn V	Process for making highly reactive sub-micron amorphous titanium diboride power and products made therefrom
US5171734A (en) *	1991-04-22	1992-12-15	Sri International	Coating a substrate in a fluidized bed maintained at a temperature below the vaporization temperature of the resulting coating composition
JP3122436B1 (ja) *	1999-09-09	2001-01-09	三菱重工業株式会社	アルミニウム複合材およびその製造方法、並びにそれを用いたバスケットおよびキャスク
EP1517858A1 (en) *	2002-03-28	2005-03-30	Council Of Scientific And Industrial Research	Process for the production of zirconium boride powder
US8142749B2 (en) *	2008-11-17	2012-03-27	Kennametal Inc.	Readily-densified titanium diboride and process for making same
CN105040027B (zh) *	2009-07-28	2018-06-22	美铝美国公司	用于制造铝熔炼中的可润湿阴极的组合物
EP2423164A1 (en) *	2010-08-25	2012-02-29	Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V.	General synthesis of metal borides in liquid salt melts
RU2684381C1 (ru) *	2018-01-09	2019-04-08	федеральное государственное бюджетное образовательное учреждение высшего образования "Санкт-Петербургский горный университет"	Способ получения порошка диборида титана
CN109019625B (zh) *	2018-09-30	2021-07-20	成都先进金属材料产业技术研究院有限公司	硼化钛粉末的制备方法
US11066308B2 (en)	2019-02-05	2021-07-20	United Technologies Corporation	Preparation of metal diboride and boron-doped powders
RU2723859C1 (ru) *	2019-09-13	2020-06-17	Евгений Сергеевич Горланов	Способ низкотемпературного синтеза диборида титана

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB632564A (en) *	1938-07-11	1949-11-28	Wilhelm Kroll	Improvements in or relating to the manufacture of titanium in a cold-malleable form
FR1152241A (fr) *	1956-06-06	1958-02-13		Procédé de préparation d'alliages contenant du bore
US3244482A (en) *	1961-05-03	1966-04-05	Union Carbide Corp	Ultrafine titanium boride
US3253886A (en) *	1961-05-09	1966-05-31	Union Carbide Corp	Process for producing ultrafine powders of refractory materials
FR1471238A (fr) *	1966-01-19	1967-03-03	France Ministre Des Armees	Méthode permettant de préparer avec une très grande pureté du bore, des borures et de nouveaux composés du bore
SE347765B (it) *	1970-05-27	1972-08-14	Nordstjernan Rederi Ab
US3979500A (en) *	1973-05-02	1976-09-07	Ppg Industries, Inc.	Preparation of finely-divided refractory powders of groups III-V metal borides, carbides, nitrides, silicides and sulfides
US4282195A (en) *	1975-02-03	1981-08-04	Ppg Industries, Inc.	Submicron titanium boride powder and method for preparing same
US4233277A (en) *	1975-02-03	1980-11-11	Ppg Industries, Inc.	Preparing refractory metal boride powder

1983
- 1983-04-26 US US06/488,870 patent/US4503021A/en not_active Expired - Fee Related
1984
- 1984-04-17 GB GB08409883A patent/GB2138794B/en not_active Expired
- 1984-04-17 CA CA000452219A patent/CA1209786A/en not_active Expired
- 1984-04-19 JP JP59079301A patent/JPS59207835A/ja active Pending
- 1984-04-20 IT IT20664/84A patent/IT1176115B/it active
- 1984-04-25 FR FR8406485A patent/FR2545077A1/fr not_active Withdrawn
- 1984-04-25 NO NO841623A patent/NO841623L/no unknown
- 1984-04-26 DE DE19843415611 patent/DE3415611A1/de not_active Withdrawn

Also Published As

Publication number	Publication date
US4503021A (en)	1985-03-05
GB8409883D0 (en)	1984-05-31
GB2138794A (en)	1984-10-31
IT1176115B (it)	1987-08-12
JPS59207835A (ja)	1984-11-26
CA1209786A (en)	1986-08-19
GB2138794B (en)	1986-12-03
IT8420664A1 (it)	1985-10-20
DE3415611A1 (de)	1984-10-31
FR2545077A1 (fr)	1984-11-02
IT8420664A0 (it)	1984-04-20

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US4957884A (en)	1990-09-18	Titanium diboride/boron carbide composites with high hardness and toughness
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US5234674A (en)	1993-08-10	Process for the preparation of metal carbides
WO1993000293A1 (en)	1993-01-07	Method for the preparation of niobium nitride
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US2698221A (en)	1954-12-28	Preparing titanium compounds
US5211921A (en)	1993-05-18	Process of making niobium oxide
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