NO852837L - Fremgangsmaate ved fremstilling av en vannuloeselig organisk nitrogenbase og natriumkarbonat. - Google Patents
Fremgangsmaate ved fremstilling av en vannuloeselig organisk nitrogenbase og natriumkarbonat.Info
- Publication number
- NO852837L NO852837L NO852837A NO852837A NO852837L NO 852837 L NO852837 L NO 852837L NO 852837 A NO852837 A NO 852837A NO 852837 A NO852837 A NO 852837A NO 852837 L NO852837 L NO 852837L
- Authority
- NO
- Norway
- Prior art keywords
- aqueous solution
- treated
- hydrochloride
- amine
- organic
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 34
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 title description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 title 2
- 229910052757 nitrogen Inorganic materials 0.000 title 1
- 229910000029 sodium carbonate Inorganic materials 0.000 title 1
- -1 nitrogenous organic base Chemical class 0.000 claims description 61
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 52
- 239000007864 aqueous solution Substances 0.000 claims description 49
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 47
- 239000000243 solution Substances 0.000 claims description 42
- 150000001412 amines Chemical class 0.000 claims description 38
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 26
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 26
- 235000002639 sodium chloride Nutrition 0.000 claims description 25
- 239000011780 sodium chloride Substances 0.000 claims description 25
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 23
- 230000005484 gravity Effects 0.000 claims description 21
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 20
- 239000003153 chemical reaction reagent Substances 0.000 claims description 20
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 19
- 238000000926 separation method Methods 0.000 claims description 18
- 238000004519 manufacturing process Methods 0.000 claims description 15
- 229910052783 alkali metal Inorganic materials 0.000 claims description 14
- 239000008346 aqueous phase Substances 0.000 claims description 14
- 239000012452 mother liquor Substances 0.000 claims description 12
- 239000007789 gas Substances 0.000 claims description 11
- 239000001569 carbon dioxide Substances 0.000 claims description 10
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 10
- 150000007530 organic bases Chemical class 0.000 claims description 9
- 230000000295 complement effect Effects 0.000 claims description 8
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims description 8
- 239000007900 aqueous suspension Substances 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 6
- 125000004432 carbon atom Chemical group C* 0.000 claims description 5
- 239000011541 reaction mixture Substances 0.000 claims description 5
- 150000003973 alkyl amines Chemical class 0.000 claims description 4
- 150000007529 inorganic bases Chemical class 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 239000012074 organic phase Substances 0.000 claims description 3
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 description 10
- 239000003960 organic solvent Substances 0.000 description 10
- 229920006395 saturated elastomer Polymers 0.000 description 8
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 6
- 238000002425 crystallisation Methods 0.000 description 6
- 230000008025 crystallization Effects 0.000 description 6
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 5
- 235000015497 potassium bicarbonate Nutrition 0.000 description 4
- 229910000028 potassium bicarbonate Inorganic materials 0.000 description 4
- 239000011736 potassium bicarbonate Substances 0.000 description 4
- 150000003141 primary amines Chemical class 0.000 description 4
- AAIUWVOMXTVLRG-UHFFFAOYSA-N 8,8-dimethylnonan-1-amine Chemical compound CC(C)(C)CCCCCCCN AAIUWVOMXTVLRG-UHFFFAOYSA-N 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 229910001514 alkali metal chloride Inorganic materials 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 150000003840 hydrochlorides Chemical class 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
- 235000011941 Tilia x europaea Nutrition 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 2
- 150000001491 aromatic compounds Chemical class 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 2
- 239000000920 calcium hydroxide Substances 0.000 description 2
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000005868 electrolysis reaction Methods 0.000 description 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 2
- 239000004571 lime Substances 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000008096 xylene Substances 0.000 description 2
- HYFLWBNQFMXCPA-UHFFFAOYSA-N 1-ethyl-2-methylbenzene Chemical class CCC1=CC=CC=C1C HYFLWBNQFMXCPA-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 150000007824 aliphatic compounds Chemical class 0.000 description 1
- 229910001617 alkaline earth metal chloride Inorganic materials 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000002152 aqueous-organic solution Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- OCKPCBLVNKHBMX-UHFFFAOYSA-N butylbenzene Chemical class CCCCC1=CC=CC=C1 OCKPCBLVNKHBMX-UHFFFAOYSA-N 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 150000002466 imines Chemical class 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M potassium chloride Inorganic materials [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 150000003335 secondary amines Chemical class 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
- 229910001948 sodium oxide Inorganic materials 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/16—Preparation from compounds of sodium or potassium with amines and carbon dioxide
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Removal Of Specific Substances (AREA)
- Treatment Of Water By Oxidation Or Reduction (AREA)
- Fertilizers (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8411424A FR2567878B1 (fr) | 1984-07-17 | 1984-07-17 | Procede pour l'obtention d'une base organique azotee insoluble dans l'eau, au depart d'une solution aqueuse de bicarbonate de metal alcalin et de chlorhydrate de ladite base, et procede de fabrication de bicarbonate de sodium |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO852837L true NO852837L (no) | 1986-01-20 |
Family
ID=9306264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO852837A NO852837L (no) | 1984-07-17 | 1985-07-16 | Fremgangsmaate ved fremstilling av en vannuloeselig organisk nitrogenbase og natriumkarbonat. |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US4677229A (fr) |
| JP (1) | JPS6156157A (fr) |
| AT (1) | AT383591B (fr) |
| AU (1) | AU4485785A (fr) |
| BE (1) | BE902854A (fr) |
| BR (1) | BR8503385A (fr) |
| DE (1) | DE3525573A1 (fr) |
| ES (1) | ES8607208A1 (fr) |
| FR (1) | FR2567878B1 (fr) |
| GB (1) | GB2162176A (fr) |
| IL (1) | IL75759A0 (fr) |
| IT (1) | IT1187690B (fr) |
| LU (1) | LU86005A1 (fr) |
| MA (1) | MA20489A1 (fr) |
| NL (1) | NL8502060A (fr) |
| NO (1) | NO852837L (fr) |
| PT (1) | PT80814B (fr) |
| SE (1) | SE8503478L (fr) |
| ZA (1) | ZA855161B (fr) |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3443889A (en) * | 1964-08-17 | 1969-05-13 | Kaiser Aluminium Chem Corp | Method of synthesis of alkali metal salts |
| JPS5734020A (en) * | 1980-08-06 | 1982-02-24 | Toyo Soda Mfg Co Ltd | Recovery of ammonia |
-
1984
- 1984-07-17 FR FR8411424A patent/FR2567878B1/fr not_active Expired
-
1985
- 1985-07-09 ZA ZA855161A patent/ZA855161B/xx unknown
- 1985-07-10 IL IL75759A patent/IL75759A0/xx unknown
- 1985-07-11 BE BE1/011295A patent/BE902854A/fr not_active IP Right Cessation
- 1985-07-12 AU AU44857/85A patent/AU4485785A/en not_active Abandoned
- 1985-07-15 PT PT80814A patent/PT80814B/fr unknown
- 1985-07-15 SE SE8503478A patent/SE8503478L/ not_active Application Discontinuation
- 1985-07-15 LU LU86005A patent/LU86005A1/fr unknown
- 1985-07-15 US US06/754,972 patent/US4677229A/en not_active Expired - Fee Related
- 1985-07-16 GB GB08517879A patent/GB2162176A/en not_active Withdrawn
- 1985-07-16 NO NO852837A patent/NO852837L/no unknown
- 1985-07-16 BR BR8503385A patent/BR8503385A/pt unknown
- 1985-07-16 ES ES545249A patent/ES8607208A1/es not_active Expired
- 1985-07-16 AT AT0210085A patent/AT383591B/de not_active IP Right Cessation
- 1985-07-16 JP JP60156847A patent/JPS6156157A/ja active Pending
- 1985-07-16 MA MA20714A patent/MA20489A1/fr unknown
- 1985-07-17 DE DE19853525573 patent/DE3525573A1/de not_active Withdrawn
- 1985-07-17 IT IT21613/85A patent/IT1187690B/it active
- 1985-07-17 NL NL8502060A patent/NL8502060A/nl not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| US4677229A (en) | 1987-06-30 |
| IL75759A0 (en) | 1985-11-29 |
| FR2567878B1 (fr) | 1986-12-05 |
| IT1187690B (it) | 1987-12-23 |
| GB2162176A (en) | 1986-01-29 |
| AU4485785A (en) | 1986-01-23 |
| IT8521613A0 (it) | 1985-07-17 |
| PT80814B (fr) | 1987-03-23 |
| JPS6156157A (ja) | 1986-03-20 |
| DE3525573A1 (de) | 1986-01-23 |
| PT80814A (fr) | 1985-08-01 |
| ES545249A0 (es) | 1986-05-16 |
| BR8503385A (pt) | 1986-04-08 |
| ES8607208A1 (es) | 1986-05-16 |
| ZA855161B (en) | 1986-03-26 |
| AT383591B (de) | 1987-07-27 |
| BE902854A (fr) | 1986-01-13 |
| MA20489A1 (fr) | 1986-04-01 |
| NL8502060A (nl) | 1986-02-17 |
| GB8517879D0 (en) | 1985-08-21 |
| LU86005A1 (fr) | 1986-02-12 |
| FR2567878A1 (fr) | 1986-01-24 |
| ATA210085A (de) | 1986-12-15 |
| SE8503478D0 (sv) | 1985-07-15 |
| SE8503478L (sv) | 1986-01-18 |
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