NO892713L - Fremgangsmaate og anordning for regulering/oppfoelging av aktiveringsreaksjoner for ziegler-natta-katalysatorbaerere, og deres anvendelse. - Google Patents

Fremgangsmaate og anordning for regulering/oppfoelging av aktiveringsreaksjoner for ziegler-natta-katalysatorbaerere, og deres anvendelse.

Info

Publication number: NO892713L
Authority: NO; Norway
Prior art keywords: reaction; container; hydrochloric acid; absorption; solution
Prior art date: 1988-06-30

Application number

NO89892713A

Other languages

English (en)

Norwegian (no)

Other versions

NO892713D0 (no

Inventor

Thomas Garoff

Original Assignee

Neste Oy

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1988-06-30

Filing date

1989-06-29

Publication date

1990-01-02

1989-06-29 Application filed by Neste Oy filed Critical Neste Oy

1989-06-29 Publication of NO892713D0 publication Critical patent/NO892713D0/no

1990-01-02 Publication of NO892713L publication Critical patent/NO892713L/no

Links

238000006243 chemical reaction Methods 0.000 title claims description 149
238000000034 method Methods 0.000 title claims description 43
230000004913 activation Effects 0.000 title claims description 8
239000000969 carrier Substances 0.000 title claims description 8
239000011954 Ziegler–Natta catalyst Substances 0.000 title claims description 6
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 168
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 99
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 58
229910001868 water Inorganic materials 0.000 claims description 57
238000010521 absorption reaction Methods 0.000 claims description 41
239000007789 gas Substances 0.000 claims description 40
XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims description 39
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 23
239000003054 catalyst Substances 0.000 claims description 22
238000011161 development Methods 0.000 claims description 17
229910052757 nitrogen Inorganic materials 0.000 claims description 11
238000004519 manufacturing process Methods 0.000 claims description 10
125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 9
150000001875 compounds Chemical class 0.000 claims description 7
230000001105 regulatory effect Effects 0.000 claims description 5
150000001732 carboxylic acid derivatives Chemical class 0.000 claims description 4
RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 2
150000003141 primary amines Chemical class 0.000 claims description 2
150000003335 secondary amines Chemical class 0.000 claims description 2
150000003573 thiols Chemical class 0.000 claims description 2
238000009792 diffusion process Methods 0.000 claims 2
238000007743 anodising Methods 0.000 claims 1
238000007086 side reaction Methods 0.000 claims 1
235000019441 ethanol Nutrition 0.000 description 69
TWRXJAOTZQYOKJ-UHFFFAOYSA-L magnesium chloride Substances [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 58
239000013078 crystal Substances 0.000 description 43
150000003839 salts Chemical class 0.000 description 39
238000012360 testing method Methods 0.000 description 39
235000011147 magnesium chloride Nutrition 0.000 description 27
239000000243 solution Substances 0.000 description 26
239000000203 mixture Substances 0.000 description 17
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 14
239000011777 magnesium Substances 0.000 description 13
229910001629 magnesium chloride Inorganic materials 0.000 description 13
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 12
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
229910003074 TiCl4 Inorganic materials 0.000 description 12
230000015572 biosynthetic process Effects 0.000 description 12
229910052749 magnesium Inorganic materials 0.000 description 11
238000004448 titration Methods 0.000 description 11
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 9
238000002156 mixing Methods 0.000 description 9
238000003786 synthesis reaction Methods 0.000 description 9
239000002585 base Substances 0.000 description 8
238000001994 activation Methods 0.000 description 7
239000003960 organic solvent Substances 0.000 description 7
239000000377 silicon dioxide Substances 0.000 description 7
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
150000001298 alcohols Chemical class 0.000 description 6
239000003153 chemical reaction reagent Substances 0.000 description 6
235000012239 silicon dioxide Nutrition 0.000 description 6
239000012876 carrier material Substances 0.000 description 5
238000002474 experimental method Methods 0.000 description 5
239000010936 titanium Substances 0.000 description 5
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 4
239000007795 chemical reaction product Substances 0.000 description 4
238000005755 formation reaction Methods 0.000 description 4
238000012544 monitoring process Methods 0.000 description 4
239000002244 precipitate Substances 0.000 description 4
238000001556 precipitation Methods 0.000 description 4
229920002545 silicone oil Polymers 0.000 description 4
239000000126 substance Substances 0.000 description 4
229910052719 titanium Inorganic materials 0.000 description 4
125000003158 alcohol group Chemical group 0.000 description 3
238000001354 calcination Methods 0.000 description 3
239000003795 chemical substances by application Substances 0.000 description 3
230000000694 effects Effects 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
239000000395 magnesium oxide Substances 0.000 description 3
CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 3
159000000003 magnesium salts Chemical class 0.000 description 3
AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 3
210000003739 neck Anatomy 0.000 description 3
239000003921 oil Substances 0.000 description 3
239000011541 reaction mixture Substances 0.000 description 3
230000035484 reaction time Effects 0.000 description 3
239000000725 suspension Substances 0.000 description 3
238000005406 washing Methods 0.000 description 3
-1 MgCl2 salt Chemical class 0.000 description 2
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
239000002253 acid Substances 0.000 description 2
239000003513 alkali Substances 0.000 description 2
238000009835 boiling Methods 0.000 description 2
238000005352 clarification Methods 0.000 description 2
238000010411 cooking Methods 0.000 description 2
230000007423 decrease Effects 0.000 description 2
238000001035 drying Methods 0.000 description 2
238000000921 elemental analysis Methods 0.000 description 2
150000002148 esters Chemical class 0.000 description 2
VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 2
239000000347 magnesium hydroxide Substances 0.000 description 2
229910001862 magnesium hydroxide Inorganic materials 0.000 description 2
239000000463 material Substances 0.000 description 2
239000001301 oxygen Substances 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
238000005192 partition Methods 0.000 description 2
229920000642 polymer Polymers 0.000 description 2
239000000047 product Substances 0.000 description 2
229910052710 silicon Inorganic materials 0.000 description 2
239000010703 silicon Substances 0.000 description 2
239000002904 solvent Substances 0.000 description 2
229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
238000004566 IR spectroscopy Methods 0.000 description 1
238000003109 Karl Fischer titration Methods 0.000 description 1
229910003910 SiCl4 Inorganic materials 0.000 description 1
229910004298 SiO 2 Inorganic materials 0.000 description 1
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
229910007932 ZrCl4 Inorganic materials 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
230000003213 activating effect Effects 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
238000002048 anodisation reaction Methods 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
239000012298 atmosphere Substances 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
230000005587 bubbling Effects 0.000 description 1
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
238000001311 chemical methods and process Methods 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
MGWAVDBGNNKXQV-UHFFFAOYSA-N diisobutyl phthalate Chemical compound CC(C)COC(=O)C1=CC=CC=C1C(=O)OCC(C)C MGWAVDBGNNKXQV-UHFFFAOYSA-N 0.000 description 1
229910001873 dinitrogen Inorganic materials 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
229920001971 elastomer Polymers 0.000 description 1
IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 1
238000000227 grinding Methods 0.000 description 1
238000013101 initial test Methods 0.000 description 1
238000012886 linear function Methods 0.000 description 1
ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
239000001095 magnesium carbonate Substances 0.000 description 1
229910000021 magnesium carbonate Inorganic materials 0.000 description 1
238000010297 mechanical methods and process Methods 0.000 description 1
230000005226 mechanical processes and functions Effects 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
239000012299 nitrogen atmosphere Substances 0.000 description 1
TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
125000004430 oxygen atom Chemical group O* 0.000 description 1
239000007793 ph indicator Substances 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
239000000376 reactant Substances 0.000 description 1
239000012429 reaction media Substances 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
238000010517 secondary reaction Methods 0.000 description 1
FDNAPBUWERUEDA-UHFFFAOYSA-N silicon tetrachloride Chemical compound Cl[Si](Cl)(Cl)Cl FDNAPBUWERUEDA-UHFFFAOYSA-N 0.000 description 1
238000010561 standard procedure Methods 0.000 description 1
238000003756 stirring Methods 0.000 description 1
WEQHQGJDZLDFID-UHFFFAOYSA-J thorium(iv) chloride Chemical compound Cl[Th](Cl)(Cl)Cl WEQHQGJDZLDFID-UHFFFAOYSA-J 0.000 description 1
108010063955 thrombin receptor peptide (42-47) Proteins 0.000 description 1
150000003609 titanium compounds Chemical class 0.000 description 1
OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
238000000954 titration curve Methods 0.000 description 1
230000004580 weight loss Effects 0.000 description 1
DUNKXUFBGCUVQW-UHFFFAOYSA-J zirconium tetrachloride Chemical compound Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond

Landscapes

Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Catalysts (AREA)
Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

NO89892713A 1988-06-30 1989-06-29 Fremgangsmaate og anordning for regulering/oppfoelging av aktiveringsreaksjoner for ziegler-natta-katalysatorbaerere, og deres anvendelse. NO892713L (no)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
FI883128A FI81812C (fi)	1988-06-30	1988-06-30	Foerfarande och anordning foer kontroll av aktiveringsreaktioner foer ziegler-natta katalysatorbaerare samt anvaendning av dessa.

Publications (2)

Publication Number	Publication Date
NO892713D0 NO892713D0 (no)	1989-06-29
NO892713L true NO892713L (no)	1990-01-02

Family

ID=8526746

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO89892713A NO892713L (no)	1988-06-30	1989-06-29	Fremgangsmaate og anordning for regulering/oppfoelging av aktiveringsreaksjoner for ziegler-natta-katalysatorbaerere, og deres anvendelse.

Country Status (4)

Country	Link
EP (1)	EP0352911A3 (fr)
JP (1)	JPH0286605A (fr)
FI (1)	FI81812C (fr)
NO (1)	NO892713L (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2801673B1 (fr)	1999-11-26	2001-12-28	Pechiney Aluminium	Procede de mesure du degre et de l'homogeneite de calcination des alumines
US6855655B2 (en)	2002-07-15	2005-02-15	Univation Technologies, Llc	Supported polymerization catalyst

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CS184648B1 (en) *	1976-09-29	1978-08-31	Vladimir Vojir	Checking of course and ending of condensation reactions and device for making this method
PL99745B1 (pl) *	1976-10-27	1978-08-31		Urzadzenie do kontroli kinetyki procesow wydzielania silnie kwasowych produktow gazowych,zwlaszcza podczas destrukcji polichlorku winylu

1988
- 1988-06-30 FI FI883128A patent/FI81812C/fi not_active IP Right Cessation
1989
- 1989-06-29 NO NO89892713A patent/NO892713L/no unknown
- 1989-06-29 EP EP19890306624 patent/EP0352911A3/fr not_active Withdrawn
- 1989-06-30 JP JP1169689A patent/JPH0286605A/ja active Pending

Also Published As

Publication number	Publication date
EP0352911A2 (fr)	1990-01-31
FI883128L (fi)	1989-12-31
FI81812B (fi)	1990-08-31
JPH0286605A (ja)	1990-03-27
EP0352911A3 (fr)	1991-06-19
NO892713D0 (no)	1989-06-29
FI81812C (fi)	1990-12-10
FI883128A0 (fi)	1988-06-30

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