NO992929L - Salte ut fremgangsmÕte for krystallisering av 2,4,6,8,10,12-heksanitro-2,4,6,8,10,12-heksaazatetracyklo(5.5.0.05,903,11)-dodecan - Google Patents

Salte ut fremgangsmÕte for krystallisering av 2,4,6,8,10,12-heksanitro-2,4,6,8,10,12-heksaazatetracyklo(5.5.0.05,903,11)-dodecan

Info

Publication number
NO992929L
NO992929L NO992929A NO992929A NO992929L NO 992929 L NO992929 L NO 992929L NO 992929 A NO992929 A NO 992929A NO 992929 A NO992929 A NO 992929A NO 992929 L NO992929 L NO 992929L
Authority
NO
Norway
Prior art keywords
hexaazatetracyclo
hexanitro
dodecane
crystallization
out process
Prior art date
Application number
NO992929A
Other languages
English (en)
Other versions
NO313698B1 (no
NO992929D0 (no
Inventor
Eugene H Johnston
Robert B Wardle
Original Assignee
Cordant Tech Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cordant Tech Inc filed Critical Cordant Tech Inc
Publication of NO992929L publication Critical patent/NO992929L/no
Publication of NO992929D0 publication Critical patent/NO992929D0/no
Publication of NO313698B1 publication Critical patent/NO313698B1/no

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D259/00—Heterocyclic compounds containing rings having more than four nitrogen atoms as the only ring hetero atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/22—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains four or more hetero rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
NO19992929A 1996-12-17 1999-06-16 Fremgangsmåte for krystallisering av 2,4,6,8,10,12-heksanitro- 2,4,6,8,10,12-heksaazatetracyklo(5.5.0.05,903,11)-dodecan NO313698B1 (no)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US3339296P 1996-12-17 1996-12-17
PCT/US1997/022298 WO1998027072A1 (en) 1996-12-17 1997-12-12 Salting-out process of crystallizing 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0?5,903,11¿]-dodecane

Publications (3)

Publication Number Publication Date
NO992929L true NO992929L (no) 1999-06-16
NO992929D0 NO992929D0 (no) 1999-06-16
NO313698B1 NO313698B1 (no) 2002-11-18

Family

ID=21870159

Family Applications (1)

Application Number Title Priority Date Filing Date
NO19992929A NO313698B1 (no) 1996-12-17 1999-06-16 Fremgangsmåte for krystallisering av 2,4,6,8,10,12-heksanitro- 2,4,6,8,10,12-heksaazatetracyklo(5.5.0.05,903,11)-dodecan

Country Status (10)

Country Link
US (1) US5874574A (no)
EP (1) EP0946527B1 (no)
JP (1) JP2001510465A (no)
KR (1) KR20000069513A (no)
AU (1) AU5374398A (no)
CA (1) CA2275317A1 (no)
DE (1) DE69727963T2 (no)
IL (1) IL130308A0 (no)
NO (1) NO313698B1 (no)
WO (1) WO1998027072A1 (no)

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FR2770216B1 (fr) * 1997-10-29 1999-12-03 Poudres & Explosifs Ste Nale Procede d'obtention de la forme polymorphe epsilon de l'hexanitrohexaazaisowurtzitane
US6214988B1 (en) 1999-01-03 2001-04-10 Schlumberger Technology Corporation Process for making an HMX product
JP2002538160A (ja) 1999-02-16 2002-11-12 アライアント・テクシステムズ・インコーポレーテッド ２，４，６，８，１０，１２−ヘキサニトロ−２，４，６，８，１０，１２−ヘキサアザテトラシクロ［５．５．０．０５，９．０３，１１］−ドデカンの製造方法
US6428724B1 (en) 1999-05-26 2002-08-06 Schlumberger Technology Corporation Granulation process
US6201117B1 (en) 1999-05-26 2001-03-13 Schlumberger Technology Corporation Process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane
US6265573B1 (en) 1999-05-26 2001-07-24 Schlumberger Technology Corporation Purification process
US6194571B1 (en) 1999-05-26 2001-02-27 Schlumberger Technology Corporation HMX compositions and processes for their preparation
US6841016B1 (en) * 2000-03-02 2005-01-11 Nederlandse Organisatie Voor Toegepast-Natuurwetenschappelijk Onderzoek Tno Process for the production of crystalline energetic materials
US6350871B1 (en) 2000-03-31 2002-02-26 Alliant Techsystems Inc. Crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
US7288648B2 (en) * 2000-10-06 2007-10-30 Alliant Techsystems Inc. High temperature crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
US6884436B2 (en) * 2000-12-22 2005-04-26 Baxter International Inc. Method for preparing submicron particle suspensions
US20030096013A1 (en) * 2000-12-22 2003-05-22 Jane Werling Preparation of submicron sized particles with polymorph control
US20050048126A1 (en) * 2000-12-22 2005-03-03 Barrett Rabinow Formulation to render an antimicrobial drug potent against organisms normally considered to be resistant to the drug
WO2002076911A2 (en) * 2001-02-09 2002-10-03 Alliant Techsystems Inc. Reformulation of composition c-4 explosive
EP1412308A2 (en) * 2001-08-01 2004-04-28 Alliant Techsystems Inc. Low sensitivity explosive compositions and method for making explosive compositions
JP2005504090A (ja) * 2001-09-26 2005-02-10 バクスター・インターナショナル・インコーポレイテッド 分散体および溶媒相または液相の除去によるサブミクロンサイズ−ナノ粒子の調製
US7112340B2 (en) * 2001-10-19 2006-09-26 Baxter International Inc. Compositions of and method for preparing stable particles in a frozen aqueous matrix
US6992185B2 (en) 2002-01-09 2006-01-31 Alliant Techsystems Inc. Crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
US20060280786A1 (en) * 2005-06-14 2006-12-14 Rabinow Barrett E Pharmaceutical formulations for minimizing drug-drug interactions
BRPI0618661A2 (pt) * 2005-11-15 2011-09-06 Baxter Int composições de inibidores de lipoxigenase
US20090152176A1 (en) * 2006-12-23 2009-06-18 Baxter International Inc. Magnetic separation of fine particles from compositions
US8426467B2 (en) * 2007-05-22 2013-04-23 Baxter International Inc. Colored esmolol concentrate
US20080293814A1 (en) * 2007-05-22 2008-11-27 Deepak Tiwari Concentrate esmolol
US8722736B2 (en) * 2007-05-22 2014-05-13 Baxter International Inc. Multi-dose concentrate esmolol with benzyl alcohol
FR2950623B1 (fr) * 2009-09-29 2011-10-21 Snpe Materiaux Energetiques Suspension de cristaux d'hexanitrohexaazaisowurtzitane, obtention desdites suspensions et fabrication d'objets pyrotechniques.
RU2447075C9 (ru) * 2011-01-11 2012-11-20 Открытое акционерное общество "Федеральный научно-производственный центр "Алтай" Способ получения гамма-полиморфной модификации 2,4,6,8,10,12-гексанитро-2,4,6,8,10,12-гексаазатетрацикло[5,5,0,03,11,05,9]додекана
CZ303686B6 (cs) 2011-09-29 2013-03-06 Univerzita Pardubice Zpusob prípravy epsilon-2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitanu se snízenou citlivostí k nárazu
CN105418619B (zh) * 2015-12-29 2017-12-12 山西北化关铝化工有限公司 一种特质六硝基六氮杂异伍兹烷的制备方法
CN105693734B (zh) * 2016-03-15 2018-11-09 北京理工大学 一种特质ε-HNIW晶体及其制备方法
US10626061B2 (en) * 2017-08-03 2020-04-21 National Technology & Engineering Solutions Of Sandia, Llc Synthesis of energetic material particles with controlled morphology
CN119425143A (zh) * 2024-10-11 2025-02-14 西安近代化学研究所 一种基于微流控技术的ε-HNIW粒度调控方法

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SE451718B (sv) * 1984-04-04 1987-10-26 Nobel Kemi Ab Sett att omkristallisera sprengemnena oktogen och hexogen
DE3617408C1 (de) * 1986-05-23 1987-06-11 Dynamit Nobel Ag Verfahren zur Herstellung von feinkoernigem beta-Oktogen
US4785094A (en) * 1986-09-26 1988-11-15 Morton Thiokol, Inc. Crystallization of beta HMX
US5132409A (en) * 1987-01-12 1992-07-21 Bracco Industria Chimica S.P.A. Macrocyclic chelating agents and chelates thereof
US5693794A (en) * 1988-09-30 1997-12-02 The United States Of America As Represented By The Secretary Of The Navy Caged polynitramine compound
HU209603B (en) * 1988-10-05 1994-09-28 Upjohn Co Process for production of solid powders in finalydivided microcristallin form
US5707634A (en) * 1988-10-05 1998-01-13 Pharmacia & Upjohn Company Finely divided solid crystalline powders via precipitation into an anti-solvent
DE4200743C2 (de) * 1991-09-18 1994-04-07 Wasagchemie Sythen Gmbh Verfahren und Vorrichtung zur Verringerung der Korngröße von kristallinem Explosivstoff
US5124493A (en) * 1991-10-15 1992-06-23 The United States Of America As Represented By The Secretary Of The Army Process of producing XMX in 100% yield and purity
US5268469A (en) * 1991-10-15 1993-12-07 The United States Of America As Represented By The Secretary Of The Army Process of making impact insensitive Alpha-HMX
US5723604A (en) * 1995-06-22 1998-03-03 Thiokol Corporation Synthesis of 2,4,6,8,10,12-hexabenzyl-2,4,6,8,10,12-hexaazatetracyclo 5.5.0.05,9.03,11!dodecane
US5739325A (en) * 1995-12-07 1998-04-14 Thiokol Corporation Hydrogenolysis of 2,4,6,8,10,12-Hexabenzyl-2,4,6,8,10,12-Hexaazatetracyclo 5.5.0.05,9.03,11 !dodecane

Also Published As

Publication number Publication date
CA2275317A1 (en) 1998-06-25
DE69727963T2 (de) 2004-07-22
DE69727963D1 (de) 2004-04-08
NO313698B1 (no) 2002-11-18
EP0946527B1 (en) 2004-03-03
JP2001510465A (ja) 2001-07-31
IL130308A0 (en) 2000-06-01
KR20000069513A (ko) 2000-11-25
US5874574A (en) 1999-02-23
AU5374398A (en) 1998-07-15
WO1998027072A1 (en) 1998-06-25
NO992929D0 (no) 1999-06-16
EP0946527A1 (en) 1999-10-06

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