OA13144A - Improved process for producing cocoa butter and cocoa powder by liquefied gas extraction. - Google Patents

Improved process for producing cocoa butter and cocoa powder by liquefied gas extraction. Download PDF

Info

Publication number: OA13144A
Authority: OA; OAPI
Prior art keywords: cocoa; solvent; mixing; mass; solids
Prior art date: 2002-10-15

Application number

OA1200500118A

Other languages

English (en)

Inventor

Todd W Gusek

Ian C Purtle

Bassam F Jirjis

Original Assignee

Cargill Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2002-10-15

Filing date

2003-10-15

Publication date

2006-12-13

2003-10-15 Application filed by Cargill Inc filed Critical Cargill Inc

2006-12-13 Publication of OA13144A publication Critical patent/OA13144A/en

Links

244000299461 Theobroma cacao Species 0.000 title claims abstract description 204
235000009470 Theobroma cacao Nutrition 0.000 title claims abstract description 203
235000019868 cocoa butter Nutrition 0.000 title claims abstract description 115
229940110456 cocoa butter Drugs 0.000 title claims abstract description 113
238000000034 method Methods 0.000 title claims abstract description 66
230000008569 process Effects 0.000 title claims abstract description 43
239000000843 powder Substances 0.000 title claims description 87
238000000605 extraction Methods 0.000 title description 29
239000002904 solvent Substances 0.000 claims abstract description 146
238000002156 mixing Methods 0.000 claims abstract description 119
239000007787 solid Substances 0.000 claims abstract description 33
239000002002 slurry Substances 0.000 claims abstract description 23
229930195734 saturated hydrocarbon Natural products 0.000 claims abstract description 20
230000003068 static effect Effects 0.000 claims description 23
238000005406 washing Methods 0.000 claims description 20
IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims description 17
OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 15
239000007788 liquid Substances 0.000 claims description 12
239000001273 butane Substances 0.000 claims description 11
235000014121 butter Nutrition 0.000 claims description 11
238000004064 recycling Methods 0.000 claims description 9
239000004215 Carbon black (E152) Substances 0.000 claims description 4
229930195733 hydrocarbon Natural products 0.000 claims description 4
150000002430 hydrocarbons Chemical class 0.000 claims description 4
238000010924 continuous production Methods 0.000 claims 2
238000004519 manufacturing process Methods 0.000 description 22
239000013557 residual solvent Substances 0.000 description 15
238000000944 Soxhlet extraction Methods 0.000 description 13
239000002245 particle Substances 0.000 description 13
238000003825 pressing Methods 0.000 description 10
239000000047 product Substances 0.000 description 10
239000012530 fluid Substances 0.000 description 9
238000012545 processing Methods 0.000 description 9
230000008901 benefit Effects 0.000 description 8
238000002844 melting Methods 0.000 description 7
230000008018 melting Effects 0.000 description 7
239000007789 gas Substances 0.000 description 6
238000000227 grinding Methods 0.000 description 6
239000000203 mixture Substances 0.000 description 6
244000046052 Phaseolus vulgaris Species 0.000 description 5
235000010627 Phaseolus vulgaris Nutrition 0.000 description 5
238000009826 distribution Methods 0.000 description 5
235000013305 food Nutrition 0.000 description 5
235000004213 low-fat Nutrition 0.000 description 5
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
238000002474 experimental method Methods 0.000 description 4
NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 4
239000004744 fabric Substances 0.000 description 3
239000000706 filtrate Substances 0.000 description 3
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
241000277331 Salmonidae Species 0.000 description 2
IAIWVQXQOWNYOU-BAQGIRSFSA-N [(z)-(5-nitrofuran-2-yl)methylideneamino]urea Chemical compound NC(=O)N\N=C/C1=CC=C([N+]([O-])=O)O1 IAIWVQXQOWNYOU-BAQGIRSFSA-N 0.000 description 2
230000009471 action Effects 0.000 description 2
238000003889 chemical engineering Methods 0.000 description 2
239000011248 coating agent Substances 0.000 description 2
238000000576 coating method Methods 0.000 description 2
238000001816 cooling Methods 0.000 description 2
238000002425 crystallisation Methods 0.000 description 2
230000008025 crystallization Effects 0.000 description 2
238000004821 distillation Methods 0.000 description 2
235000019197 fats Nutrition 0.000 description 2
238000001914 filtration Methods 0.000 description 2
230000004907 flux Effects 0.000 description 2
239000012535 impurity Substances 0.000 description 2
239000001282 iso-butane Substances 0.000 description 2
238000003622 knife milling Methods 0.000 description 2
239000007791 liquid phase Substances 0.000 description 2
238000003801 milling Methods 0.000 description 2
229910052757 nitrogen Inorganic materials 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
-1 /or Species 0.000 description 1
XUKUURHRXDUEBC-KAYWLYCHSA-N Atorvastatin Chemical compound C=1C=CC=CC=1C1=C(C=2C=CC(F)=CC=2)N(CC[C@@H](O)C[C@@H](O)CC(O)=O)C(C(C)C)=C1C(=O)NC1=CC=CC=C1 XUKUURHRXDUEBC-KAYWLYCHSA-N 0.000 description 1
241000196324 Embryophyta Species 0.000 description 1
238000004566 IR spectroscopy Methods 0.000 description 1
150000001335 aliphatic alkanes Chemical class 0.000 description 1
238000013459 approach Methods 0.000 description 1
238000011021 bench scale process Methods 0.000 description 1
231100000357 carcinogen Toxicity 0.000 description 1
239000003183 carcinogenic agent Substances 0.000 description 1
150000001768 cations Chemical class 0.000 description 1
235000019219 chocolate Nutrition 0.000 description 1
235000009508 confectionery Nutrition 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
238000013461 design Methods 0.000 description 1
238000005265 energy consumption Methods 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
239000002360 explosive Substances 0.000 description 1
235000013861 fat-free Nutrition 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000010419 fine particle Substances 0.000 description 1
239000000796 flavoring agent Substances 0.000 description 1
235000019634 flavors Nutrition 0.000 description 1
239000000463 material Substances 0.000 description 1
238000005259 measurement Methods 0.000 description 1
239000012528 membrane Substances 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
230000008450 motivation Effects 0.000 description 1
229920000728 polyester Polymers 0.000 description 1
239000001294 propane Substances 0.000 description 1
238000000646 scanning calorimetry Methods 0.000 description 1
239000011265 semifinished product Substances 0.000 description 1
238000003756 stirring Methods 0.000 description 1
238000002604 ultrasonography Methods 0.000 description 1
238000010977 unit operation Methods 0.000 description 1
229930195735 unsaturated hydrocarbon Natural products 0.000 description 1

Classifications

- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/30—Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/56—Liquid products; Solid products in the form of powders, flakes or granules for making liquid products, e.g. for making chocolate milk, drinks and the products for their preparation, pastes for spreading or milk crumb
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/0003—Processes of manufacture not relating to composition or compounding ingredients
- A23G1/0006—Processes specially adapted for manufacture or treatment of cocoa or cocoa products
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/0003—Processes of manufacture not relating to composition or compounding ingredients
- A23G1/0006—Processes specially adapted for manufacture or treatment of cocoa or cocoa products
- A23G1/0009—Manufacture or treatment of liquids, creams, pastes, granules, shreds or powders
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/0003—Processes of manufacture not relating to composition or compounding ingredients
- A23G1/0006—Processes specially adapted for manufacture or treatment of cocoa or cocoa products
- A23G1/0009—Manufacture or treatment of liquids, creams, pastes, granules, shreds or powders
- A23G1/0016—Transformation of liquids, pastes, creams, lumps, powders, granules or shreds into powders, granules or shreds; Manufacture or treatment of powders

Landscapes

Life Sciences & Earth Sciences (AREA)
Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Food Science & Technology (AREA)
Polymers & Plastics (AREA)
Confectionery (AREA)

OA1200500118A 2002-10-15 2003-10-15 Improved process for producing cocoa butter and cocoa powder by liquefied gas extraction. OA13144A (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US10/272,486 US20040071848A1 (en)	2002-10-15	2002-10-15	Process for producing cocoa butter and cocoa powder by liquefied gas extraction

Publications (1)

Publication Number	Publication Date
OA13144A true OA13144A (en)	2006-12-13

Family

ID=32069266

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
OA1200500118A OA13144A (en)	2002-10-15	2003-10-15	Improved process for producing cocoa butter and cocoa powder by liquefied gas extraction.

Country Status (9)

Country	Link
US (1)	US20040071848A1 (de)
EP (1)	EP1565060B1 (de)
CN (1)	CN1725956A (de)
AT (1)	ATE388638T1 (de)
AU (1)	AU2003287149A1 (de)
BR (1)	BR0315313A (de)
DE (1)	DE60319730T2 (de)
OA (1)	OA13144A (de)
WO (1)	WO2004034801A2 (de)

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CN103298355A (zh)	2011-01-12	2013-09-11	卡吉尔公司	可可粉组合物
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2002
- 2002-10-15 US US10/272,486 patent/US20040071848A1/en not_active Abandoned
2003
- 2003-10-15 OA OA1200500118A patent/OA13144A/en unknown
- 2003-10-15 EP EP03781326A patent/EP1565060B1/de not_active Expired - Lifetime
- 2003-10-15 BR BR0315313-4A patent/BR0315313A/pt not_active IP Right Cessation
- 2003-10-15 CN CN200380106144.5A patent/CN1725956A/zh active Pending
- 2003-10-15 AU AU2003287149A patent/AU2003287149A1/en not_active Abandoned
- 2003-10-15 AT AT03781326T patent/ATE388638T1/de not_active IP Right Cessation
- 2003-10-15 WO PCT/US2003/032636 patent/WO2004034801A2/en not_active Ceased
- 2003-10-15 DE DE60319730T patent/DE60319730T2/de not_active Expired - Lifetime

Also Published As

Publication number	Publication date
BR0315313A (pt)	2005-09-06
CN1725956A (zh)	2006-01-25
EP1565060B1 (de)	2008-03-12
ATE388638T1 (de)	2008-03-15
DE60319730D1 (de)	2008-04-24
DE60319730T2 (de)	2009-04-16
EP1565060A2 (de)	2005-08-24
AU2003287149A1 (en)	2004-05-04
WO2004034801A2 (en)	2004-04-29
US20040071848A1 (en)	2004-04-15
WO2004034801A3 (en)	2004-09-23

Publication	Publication Date	Title
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