PL129512B2 - Matt glaze - Google Patents

Matt glaze Download PDF

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Publication number
PL129512B2
PL129512B2 PL23814282A PL23814282A PL129512B2 PL 129512 B2 PL129512 B2 PL 129512B2 PL 23814282 A PL23814282 A PL 23814282A PL 23814282 A PL23814282 A PL 23814282A PL 129512 B2 PL129512 B2 PL 129512B2
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PL
Poland
Prior art keywords
amount
weight
parts
glaze
matt
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Application number
PL23814282A
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Polish (pl)
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PL238142A2 (en
Inventor
Zdzislaw Dziob
Alfred Czyzewski
Ireneusz Gorski
Zbigniew Rak
Tadeusz Sobotowski
Original Assignee
Akad Gorniczo Hutnicza
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Akad Gorniczo Hutnicza filed Critical Akad Gorniczo Hutnicza
Priority to PL23814282A priority Critical patent/PL129512B2/en
Publication of PL238142A2 publication Critical patent/PL238142A2/en
Publication of PL129512B2 publication Critical patent/PL129512B2/en

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Description

Przedmiotem wynalazku jest szkliwo matowe, znajdujace zastosowanie do pokrywania plytek ceramicznych podlogowych i sciennych oraz wyrobów ceramiki szlachetnej.Powstawanie szkliw matowych polega na wywolaniu krystalizacji w szklistej masie podczas jej studzenia. Krystalizacje w szkliwach mozna wywolac poprzez: — dodatek zwiazków metali ziem alkalicznych celem wywolania krystalizacji krzemianów wapnia lub baru; na przyklad wprowadzenie 0,4-0,5 mola CaO, a BaO w ilosci 0,2 mola wywoluje matowosc szkliw, — dodatek rytylu — Ti02 wprowadzony w ilosci 3-15% wywoluje matowosc szkliw, — przesycenie szkliwa kwarcem, dajacym przy ochlodzeniu trydymit, — zmniejszenie zawartosci SiC2 lub zwiekszenie zawartosci AI2O3 w celu wywolania krystali¬ zacji mulitu podczas studzenia, przy czym stosunek AI2O3 i Si02 okreslajacy lepkosc szkliwa w stanie plynnym pozwalajacy osiagnac znaczna liczbe drobnych krysztalów zawarty jest zwykle w granicach 1:3 do 1:6.Szkliwa matowe powinny sie charakteryzowac duza szybkoscia tworzenia zarodków krystali¬ zacji i mala szybkoscia wzrostu krysztalów, co zalezne jest od takich czynnikówjak sklad chemi¬ czny i krzywa wypalania. Szkliwa matowe sa trudne do otrzymania, gdyz wszelkie wahania skladu chemicznego, lepkosci szkliwa i temperatury wypalania powoduja' utrate matowosci.Szkliwo matowe wedlug wynalazku zawiera tuf porfirowy w ilosci 15-30 czesci wagowych, fryte ceramiczna transparentna lub zmetniona w ilosci 60-80czesci wagowych, chalcedonit w ilosci 2-12 czesci wagowych oraz talk w ilosci 3-15 czesci wagowych.Tufporfirowy i chalcedonit wprowadzaja do zestawu drobne ilosci kwarcu, który nie ulega Calkowitemu stopieniu, tworzac matowa powierzchnie szkliwa.Dodatek talku do szkliwa zapobiega jego sedymentacji, polepsza odpornosc termiczna i obniza wspólczynnik rozszerzalnosci cieplnej. Ponadto taki sklad szkliwa wg wynalazku zapewnia korzystny stosunek AI2O3 do Si02 ulatwiajacy powstanie matowosci.Szkliwo wedlug wynalazku charakteryzuje sie nastepujacymi wlasnosciami technologicznymi: wspólczynnik rozszerzalnosci cieplnej cl***io 50-55-10 61/°C2 129512 mikrotwardosc 450-550 kG/mm2 scieralnosc 50-55 mg odpornosc na pekniecia wloskowate 160-180°C Przyklad. Fryte ceramiczna borowo-olowiowa w ilosci 67,5 kg miele sie na mokro wspólnie z tufem porfirowym w ilosci 22,5 kg, chalcedonitem w ilosci 4,5 kg i talkiem w ilosci 5,5 kg do pozostalosci na sicie 10000 oczek/cm2 rzedu 0,1%. Nastepnie zawiesine szkliwa o gestosci 1,52 g/cm2 nanosi sie na kamionkowe plytki podlogowe wypalone wstepnie w temperaturze 1080°C. Szkliwo podsusza sie do wilgotnosci rzedu 1-3%, po czym wypala sie poszkliwione plytki w tempetaturze 980°C.Szkliwo charakteryzuje sie nastepujacymi wlasnosciami: wspólczynnik rozszerzalnosci cieplnej a60°2o -5,25-10~6l/°C mikrotwardosc 480 kG/mm2 scieralnosc 50 mg odpornosc na pekniecia wloskowate 160°C Zastrzezenie patentowe Szkliwo matowe, znamienne tym, ze zawiera fryte ceramiczna transparentna lub zmetniona w ilosci 60-80 czesci wagowych oraz tuf porfirowy w ilosci 15-30 czesci wagowych, chalcedonit w ilosci 2-12 czesci wagowych i talk w ilosci 3-15 czesci wagowych.Pracownia Poligraficzna UP PRL. Naklad 100 egz.Cena 100 zl PLThe subject of the invention is matt glaze, used for covering ceramic floor and wall tiles as well as precious ceramics. The formation of matt glazes consists in causing crystallization in the glass mass during its cooling. Crystallization in glazes can be caused by: - addition of alkaline earth metal compounds to induce crystallization of calcium or barium silicates; for example, introducing 0.4-0.5 moles of CaO, and BaO in the amount of 0.2 moles makes the glazes dull, - the addition of rithile - TiO2 introduced in the amount of 3-15% makes the glazes dull, - supersaturation of the glaze with quartz, giving tridimite when cooled - reducing the SiCl 2 content or increasing the Al 2 O 3 content in order to induce crystallization of the mullite during cooling, the ratio of Al 2 O 3 and SiO 2 determining the viscosity of the glaze in the liquid state to achieve a large number of fine crystals is usually in the range 1: 3 to 1: 6. Matt glazes should have a high nucleation rate and a low crystal growth rate, depending on factors such as the chemical composition and the firing curve. Matt glazes are difficult to obtain, as any fluctuations in the chemical composition, viscosity of the glaze and firing temperature result in a loss of mattness. According to the invention, matt glazes contain porphyry tuff in the amount of 15-30 parts by weight, frit ceramic transparent or chilled in the amount of 60-80 parts by weight, Chalcedonite in the amount of 2-12 parts by weight and talc in the amount of 3-15 parts by weight. Tuforphyry and chalcedonite add small amounts of quartz to the set, which does not completely melt, creating a matte surface of the enamel. The addition of talcum to the enamel prevents it from sedimentation, improves thermal resistance and lowers the coefficient of thermal expansion. Moreover, such a composition of the glaze according to the invention provides a favorable ratio of Al2O3 to SiO2, which facilitates the formation of mattness. According to the invention, the glazing is characterized by the following technological properties: coefficient of thermal expansion cl *** and 50-55-10 61 / ° C2 129 512 microhardness 450-550 kG / mm2 abrasion 50-55 mg hairline fracture resistance 160-180 ° C Ex. 67.5 kg of boron-lead ceramic frit is wet ground together with 22.5 kg porphyry tuff, 4.5 kg of chalcedony and 5.5 kg of talcum powder to a sieve residue of 10,000 mesh / cm2 row 0.1%. Then the glaze suspension with a density of 1.52 g / cm2 is applied to the stoneware floor tiles pre-fired at 1080 ° C. The glaze is dried to a humidity of 1-3%, after which the glazed tiles burn out at a temperature of 980 ° C. The glaze is characterized by the following properties: coefficient of thermal expansion a60 ° 2o -5.25-10 ~ 6l / ° C microhardness 480 kG / mm2 abrasion 50 mg resistance to hairline cracks 160 ° C Patent claim Matt glaze, characterized by the fact that it contains a ceramic frit transparent or choked in the amount of 60-80 parts by weight and porphyry tuff in the amount of 15-30 parts by weight, chalcedony in the amount of 2-12 parts by weight and talc in the amount of 3-15 parts by weight. Pracownia Poligraficzna UP PRL. Mintage 100 copies Price PLN 100 PL

Claims (3)

1. Zastrzezenie patentowe1. Patent claim 2. Szkliwo matowe, znamienne tym, ze zawiera fryte ceramiczna transparentna lub zmetniona w ilosci 60-80 czesci wagowych oraz tuf porfirowy w ilosci 15-30 czesci wagowych, chalcedonit w ilosci 2-12 czesci wagowych i talk w ilosci2. Matt glaze, characterized by the fact that it contains transparent or thinned ceramic frits in the amount of 60-80 parts by weight and porphyry tuff in the amount of 15-30 parts by weight, chalcedony in the amount of 2-12 parts by weight and talc in the amount of 3. -15 czesci wagowych. Pracownia Poligraficzna UP PRL. Naklad 100 egz. Cena 100 zl PL3. -15 parts by weight. Printing workshop of the UP PRL. Mintage 100 copies. Price PLN 100 PL
PL23814282A 1982-09-03 1982-09-03 Matt glaze PL129512B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL23814282A PL129512B2 (en) 1982-09-03 1982-09-03 Matt glaze

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL23814282A PL129512B2 (en) 1982-09-03 1982-09-03 Matt glaze

Publications (2)

Publication Number Publication Date
PL238142A2 PL238142A2 (en) 1983-07-04
PL129512B2 true PL129512B2 (en) 1984-05-31

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Application Number Title Priority Date Filing Date
PL23814282A PL129512B2 (en) 1982-09-03 1982-09-03 Matt glaze

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PL238142A2 (en) 1983-07-04

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