PL1496043T3 - Sposób uzdatniania ścieków powstających przy wytwarzaniu dinitrotoluenu - Google Patents

Sposób uzdatniania ścieków powstających przy wytwarzaniu dinitrotoluenu

Info

Publication number
PL1496043T3
PL1496043T3 PL04014227T PL04014227T PL1496043T3 PL 1496043 T3 PL1496043 T3 PL 1496043T3 PL 04014227 T PL04014227 T PL 04014227T PL 04014227 T PL04014227 T PL 04014227T PL 1496043 T3 PL1496043 T3 PL 1496043T3
Authority
PL
Poland
Prior art keywords
aqueous
toluene
waste waters
dinitrotoluene
phase
Prior art date
Application number
PL04014227T
Other languages
English (en)
Inventor
JüRGEN MüNNIG
Dietmar Wastian
Wolfgang Lorenz
Berthold Keggenhoff
Original Assignee
Bayer Materialscience Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Materialscience Ag filed Critical Bayer Materialscience Ag
Publication of PL1496043T3 publication Critical patent/PL1496043T3/pl

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/26Treatment of water, waste water, or sewage by extraction
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06Preparation of nitro compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06Preparation of nitro compounds
    • C07C201/16Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/66Treatment of water, waste water, or sewage by neutralisation; pH adjustment
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/34Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
    • C02F2103/36Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Water Treatments (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Separation Of Suspended Particles By Flocculating Agents (AREA)
  • Degasification And Air Bubble Elimination (AREA)
PL04014227T 2003-06-30 2004-06-17 Sposób uzdatniania ścieków powstających przy wytwarzaniu dinitrotoluenu PL1496043T3 (pl)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10329304A DE10329304A1 (de) 2003-06-30 2003-06-30 Verfahren zur Aufarbeitung des bei der Herstellung von Dinitrotoluol anfallenden Abwassers
EP04014227A EP1496043B1 (de) 2003-06-30 2004-06-17 Verfahren zur Aufarbeitung des bei der Herstellung von Dinitroluol anfallenden Abwassers

Publications (1)

Publication Number Publication Date
PL1496043T3 true PL1496043T3 (pl) 2010-09-30

Family

ID=33441612

Family Applications (1)

Application Number Title Priority Date Filing Date
PL04014227T PL1496043T3 (pl) 2003-06-30 2004-06-17 Sposób uzdatniania ścieków powstających przy wytwarzaniu dinitrotoluenu

Country Status (9)

Country Link
US (1) US6936741B2 (pl)
EP (1) EP1496043B1 (pl)
JP (1) JP4778209B2 (pl)
KR (1) KR101093862B1 (pl)
CN (1) CN1285514C (pl)
AT (1) ATE462686T1 (pl)
DE (2) DE10329304A1 (pl)
PL (1) PL1496043T3 (pl)
TW (1) TW200516051A (pl)

Families Citing this family (56)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10345601A1 (de) * 2003-09-29 2005-05-12 Basf Ag Verfahren zur Entfernung von Nitrokresolen aus Abwasser der Mononitrotoluolherstellung und zur weiteren Verwendung des Extraktes
DE102005047460A1 (de) * 2005-09-30 2007-04-05 Basf Ag Verfahren zur Behandlung von Abwasser aus Aldolisierungsverfahren
DE102005050106B4 (de) * 2005-10-18 2008-04-30 Josef Meissner Gmbh & Co. Kg Rückgewinnung von Nitriersäuregemischen aus Nitrienprozessen
CN100369885C (zh) * 2006-01-17 2008-02-20 甘肃银光化学工业集团有限公司 连续制备二硝基甲苯的方法及其装置
ATE520646T1 (de) * 2006-03-07 2011-09-15 Basf Se Verfahren zur destillativen abtrennung von dinitrotoluol aus einem prozessabwasser aus der herstellung von dinitrotoluol durch nitrierung von toluol mit nitriersäure
CN100368325C (zh) * 2006-04-03 2008-02-13 华仁清 硝基甲苯污水处理方法
KR100834589B1 (ko) * 2006-04-12 2008-06-02 정흥호 니트로 톨루엔류 제조 과정에서 발생하는 폐기물을 이용한분산제의 제조 방법 및 그 분산제
DE102006033722A1 (de) * 2006-07-21 2008-01-24 Bayer Materialscience Ag Verfahren zur Herstellung von Dinitrotoluol
EP2067749A1 (en) * 2007-11-29 2009-06-10 Total Petrochemicals France Process for purification of an aqueous phase containing polyaromatics
US8673163B2 (en) 2008-06-27 2014-03-18 Apple Inc. Method for fabricating thin sheets of glass
US7810355B2 (en) 2008-06-30 2010-10-12 Apple Inc. Full perimeter chemical strengthening of substrates
CN102388003B (zh) 2009-03-02 2014-11-19 苹果公司 用于强化用于便携式电子设备的玻璃盖的技术
KR101150159B1 (ko) 2009-12-01 2012-05-25 휴켐스주식회사 니트로 화합물의 제조 과정에서 발생하는 폐수의 처리방법
US8529771B2 (en) 2009-12-16 2013-09-10 Basf Se Acidic sludge adsorption of DNT wastewaters
KR20120102120A (ko) * 2009-12-16 2012-09-17 바스프 에스이 Dnt 폐수의 산성 톨루엔 추출
WO2011082977A1 (de) * 2009-12-16 2011-07-14 Basf Se VERFAHREN ZUR AUFARBEITUNG VON NOx-HALTIGEN ABGASEN AUS ABWASSERSTRÖMEN VON NITRIERANLAGEN
US9778685B2 (en) 2011-05-04 2017-10-03 Apple Inc. Housing for portable electronic device with reduced border region
US9213451B2 (en) 2010-06-04 2015-12-15 Apple Inc. Thin glass for touch panel sensors and methods therefor
US8923693B2 (en) 2010-07-30 2014-12-30 Apple Inc. Electronic device having selectively strengthened cover glass
EP2418176A1 (de) * 2010-08-12 2012-02-15 Basf Se Verfahren zur Aufreinigung von Abwässern aus der Aufarbeitung vom rohem Mononitrobenzol
US10189743B2 (en) 2010-08-18 2019-01-29 Apple Inc. Enhanced strengthening of glass
US8873028B2 (en) 2010-08-26 2014-10-28 Apple Inc. Non-destructive stress profile determination in chemically tempered glass
US8824140B2 (en) 2010-09-17 2014-09-02 Apple Inc. Glass enclosure
US9725359B2 (en) 2011-03-16 2017-08-08 Apple Inc. Electronic device having selectively strengthened glass
US10781135B2 (en) 2011-03-16 2020-09-22 Apple Inc. Strengthening variable thickness glass
US9128666B2 (en) 2011-05-04 2015-09-08 Apple Inc. Housing for portable electronic device with reduced border region
CN102295380A (zh) * 2011-08-19 2011-12-28 杭州江南科学研究院有限公司 芳香族硝基化合物废水的处理和回收方法
US9944554B2 (en) 2011-09-15 2018-04-17 Apple Inc. Perforated mother sheet for partial edge chemical strengthening and method therefor
US9516149B2 (en) 2011-09-29 2016-12-06 Apple Inc. Multi-layer transparent structures for electronic device housings
CN102557179A (zh) * 2011-11-17 2012-07-11 南京理工大学 一种高浓度废酸中硝基甲苯的去除方法
US10144669B2 (en) 2011-11-21 2018-12-04 Apple Inc. Self-optimizing chemical strengthening bath for glass
US10133156B2 (en) 2012-01-10 2018-11-20 Apple Inc. Fused opaque and clear glass for camera or display window
US8684613B2 (en) 2012-01-10 2014-04-01 Apple Inc. Integrated camera window
US8773848B2 (en) 2012-01-25 2014-07-08 Apple Inc. Fused glass device housings
US9249083B2 (en) 2012-04-25 2016-02-02 Basf Se Process for scrubbing dinitrotoluene
JP6193358B2 (ja) 2012-04-25 2017-09-06 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se ジニトロトルエンを洗浄する方法
DE102012215903A1 (de) * 2012-09-07 2014-03-13 Evonik Industries Ag Verfahren zur Behandlung eines Abwasserstroms, der bei der Aufarbeitung eines Triacetonamin-haltigen Reaktionsgemisches entsteht
CN102836570A (zh) * 2012-09-19 2012-12-26 辽宁庆阳特种化工有限公司 一种对间二硝基苯生产过程中产生废酸的萃取分离方法及装置
US9946302B2 (en) 2012-09-19 2018-04-17 Apple Inc. Exposed glass article with inner recessed area for portable electronic device housing
US9459661B2 (en) 2013-06-19 2016-10-04 Apple Inc. Camouflaged openings in electronic device housings
US9886062B2 (en) 2014-02-28 2018-02-06 Apple Inc. Exposed glass article with enhanced stiffness for portable electronic device housing
JP6736547B2 (ja) * 2014-10-02 2020-08-05 コベストロ、ドイチュラント、アクチエンゲゼルシャフトCovestro Deutschland Ag ジニトロトルエンの連続的製造方法における排出ガス清浄
CN106145481A (zh) * 2016-08-31 2016-11-23 格斯瑞科技有限公司 基于空化技术处理有机工业废水的装置和方法
KR101890209B1 (ko) 2016-12-08 2018-08-21 주식회사 풍산 Tnt 폐수의 처리 방법 및 장치
CN107055899A (zh) * 2017-02-27 2017-08-18 广东工业大学 一种含高浓度酚废水的处理方法
CN108440300A (zh) * 2018-05-15 2018-08-24 福建省东南电化股份有限公司 一种硝化废酸浓缩过程中防止堵塞的方法
KR20180093857A (ko) 2018-08-14 2018-08-22 주식회사 풍산 Tnt 또는 방향족 화합물이 포함된 오염수의 처리방법 및 장치
DE102018217955B4 (de) * 2018-10-19 2020-06-04 Plinke Gmbh Verfahren zur Aufarbeitung von Mischsäure und Abwasser aus der Nitrierung von Aromaten sowie Vorrichtung zur Durchführung des Verfahrens
CN109627170B (zh) * 2018-12-17 2021-09-14 湖北东方化工有限公司 从硝基甲苯酸性废水提取多硝基甲苯的方法
CN110170185B (zh) * 2019-05-30 2023-07-25 湖北东方化工有限公司 一种废硫酸硝基化合物分离的装置及方法
CN111620504A (zh) * 2020-06-04 2020-09-04 湖北东方化工有限公司 一种多硝基甲苯生产预洗废水处理新工艺的生产方法
CN111603869A (zh) * 2020-06-04 2020-09-01 湖北东方化工有限公司 一种多硝基甲苯粉尘收集新工艺
CN113354006A (zh) * 2021-05-31 2021-09-07 湖北东方化工有限公司 一种多硝基甲苯废硫酸真空浓缩装置高酸度废水处理工艺及装置
CN115477286B (zh) * 2022-10-27 2024-08-16 湖北东方化工有限公司 一种一硝基甲苯废硫酸预处理装置及其处理方法
CN116375127A (zh) * 2023-04-17 2023-07-04 沧州大化股份有限公司 一种二硝基甲苯生产中废水的处理方法
CN119430364B (zh) * 2024-10-22 2025-05-13 安徽华尔泰化工股份有限公司 一种混二硝基苯生产废酸分离装置及分离方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3742072A (en) * 1972-03-28 1973-06-26 M Roth Nitration of toluene and nitrotoluenes to form tnt
DE2818680A1 (de) * 1978-04-27 1979-10-31 Bayer Ag Verfahren zur aufarbeitung von nitro-hydroxy-aromaten enthaltenden abwaessern
US4257986A (en) * 1979-02-02 1981-03-24 Air Products And Chemicals, Inc. Process for refining aqueous acid mixtures utilized in nitration of aromatics
US4241229A (en) * 1979-08-08 1980-12-23 American Cyanamid Company Recovery of nitrated aromatic compounds from nitration wash liquors
US4642396A (en) * 1984-08-07 1987-02-10 Air Products And Chemicals, Inc. Process for separating nitroaromatic compounds from spent nitric acid
US4597875A (en) * 1985-05-07 1986-07-01 Air Products And Chemicals, Inc. Precipitative removal of nitrocresols from dinitrotoluene waste streams
US5606948A (en) * 1996-02-27 1997-03-04 Briggs & Stratton Corporation Speed governing method and apparatus for an internal combustion engine
US5762802A (en) * 1997-05-01 1998-06-09 Air Products And Chemicals, Inc. Dilute acid oxidation of dinitrotoluene alkaline wash water
FR2767319B1 (fr) * 1997-08-13 1999-10-29 Rhone Poulenc Chimie Procede de traitement de solutions aqueuses comprenant des acides et des composes nitres
US6288289B1 (en) * 2000-01-27 2001-09-11 Noram Engineering And Constructors Ltd. Integrated effluent treatment process for nitroaromatic manufacture
US6506948B1 (en) * 2002-02-07 2003-01-14 Air Products And Chemicals, Inc. Toluene extraction of dinitrotoluene wash water

Also Published As

Publication number Publication date
KR20050002620A (ko) 2005-01-07
EP1496043B1 (de) 2010-03-31
DE10329304A1 (de) 2005-02-03
ATE462686T1 (de) 2010-04-15
EP1496043A1 (de) 2005-01-12
JP4778209B2 (ja) 2011-09-21
CN1285514C (zh) 2006-11-22
TW200516051A (en) 2005-05-16
US6936741B2 (en) 2005-08-30
US20040262238A1 (en) 2004-12-30
KR101093862B1 (ko) 2011-12-13
CN1576236A (zh) 2005-02-09
JP2005021890A (ja) 2005-01-27
DE502004010954D1 (de) 2010-05-12

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