PL1496043T3 - Sposób uzdatniania ścieków powstających przy wytwarzaniu dinitrotoluenu - Google Patents
Sposób uzdatniania ścieków powstających przy wytwarzaniu dinitrotoluenuInfo
- Publication number
- PL1496043T3 PL1496043T3 PL04014227T PL04014227T PL1496043T3 PL 1496043 T3 PL1496043 T3 PL 1496043T3 PL 04014227 T PL04014227 T PL 04014227T PL 04014227 T PL04014227 T PL 04014227T PL 1496043 T3 PL1496043 T3 PL 1496043T3
- Authority
- PL
- Poland
- Prior art keywords
- aqueous
- toluene
- waste waters
- dinitrotoluene
- phase
- Prior art date
Links
- 239000002351 wastewater Substances 0.000 title abstract 5
- DYSXLQBUUOPLBB-UHFFFAOYSA-N 2,3-dinitrotoluene Chemical compound CC1=CC=CC([N+]([O-])=O)=C1[N+]([O-])=O DYSXLQBUUOPLBB-UHFFFAOYSA-N 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 18
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 4
- 239000008346 aqueous phase Substances 0.000 abstract 4
- 238000006396 nitration reaction Methods 0.000 abstract 3
- 230000002378 acidificating effect Effects 0.000 abstract 2
- 239000012074 organic phase Substances 0.000 abstract 2
- 239000011369 resultant mixture Substances 0.000 abstract 2
- 238000005406 washing Methods 0.000 abstract 2
- 239000012071 phase Substances 0.000 abstract 1
- 238000005191 phase separation Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/26—Treatment of water, waste water, or sewage by extraction
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/16—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/34—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
- C02F2103/36—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Water Treatments (AREA)
- Extraction Or Liquid Replacement (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
- Degasification And Air Bubble Elimination (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10329304A DE10329304A1 (de) | 2003-06-30 | 2003-06-30 | Verfahren zur Aufarbeitung des bei der Herstellung von Dinitrotoluol anfallenden Abwassers |
| EP04014227A EP1496043B1 (de) | 2003-06-30 | 2004-06-17 | Verfahren zur Aufarbeitung des bei der Herstellung von Dinitroluol anfallenden Abwassers |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL1496043T3 true PL1496043T3 (pl) | 2010-09-30 |
Family
ID=33441612
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL04014227T PL1496043T3 (pl) | 2003-06-30 | 2004-06-17 | Sposób uzdatniania ścieków powstających przy wytwarzaniu dinitrotoluenu |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6936741B2 (pl) |
| EP (1) | EP1496043B1 (pl) |
| JP (1) | JP4778209B2 (pl) |
| KR (1) | KR101093862B1 (pl) |
| CN (1) | CN1285514C (pl) |
| AT (1) | ATE462686T1 (pl) |
| DE (2) | DE10329304A1 (pl) |
| PL (1) | PL1496043T3 (pl) |
| TW (1) | TW200516051A (pl) |
Families Citing this family (56)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10345601A1 (de) * | 2003-09-29 | 2005-05-12 | Basf Ag | Verfahren zur Entfernung von Nitrokresolen aus Abwasser der Mononitrotoluolherstellung und zur weiteren Verwendung des Extraktes |
| DE102005047460A1 (de) * | 2005-09-30 | 2007-04-05 | Basf Ag | Verfahren zur Behandlung von Abwasser aus Aldolisierungsverfahren |
| DE102005050106B4 (de) * | 2005-10-18 | 2008-04-30 | Josef Meissner Gmbh & Co. Kg | Rückgewinnung von Nitriersäuregemischen aus Nitrienprozessen |
| CN100369885C (zh) * | 2006-01-17 | 2008-02-20 | 甘肃银光化学工业集团有限公司 | 连续制备二硝基甲苯的方法及其装置 |
| ATE520646T1 (de) * | 2006-03-07 | 2011-09-15 | Basf Se | Verfahren zur destillativen abtrennung von dinitrotoluol aus einem prozessabwasser aus der herstellung von dinitrotoluol durch nitrierung von toluol mit nitriersäure |
| CN100368325C (zh) * | 2006-04-03 | 2008-02-13 | 华仁清 | 硝基甲苯污水处理方法 |
| KR100834589B1 (ko) * | 2006-04-12 | 2008-06-02 | 정흥호 | 니트로 톨루엔류 제조 과정에서 발생하는 폐기물을 이용한분산제의 제조 방법 및 그 분산제 |
| DE102006033722A1 (de) * | 2006-07-21 | 2008-01-24 | Bayer Materialscience Ag | Verfahren zur Herstellung von Dinitrotoluol |
| EP2067749A1 (en) * | 2007-11-29 | 2009-06-10 | Total Petrochemicals France | Process for purification of an aqueous phase containing polyaromatics |
| US8673163B2 (en) | 2008-06-27 | 2014-03-18 | Apple Inc. | Method for fabricating thin sheets of glass |
| US7810355B2 (en) | 2008-06-30 | 2010-10-12 | Apple Inc. | Full perimeter chemical strengthening of substrates |
| CN102388003B (zh) | 2009-03-02 | 2014-11-19 | 苹果公司 | 用于强化用于便携式电子设备的玻璃盖的技术 |
| KR101150159B1 (ko) | 2009-12-01 | 2012-05-25 | 휴켐스주식회사 | 니트로 화합물의 제조 과정에서 발생하는 폐수의 처리방법 |
| US8529771B2 (en) | 2009-12-16 | 2013-09-10 | Basf Se | Acidic sludge adsorption of DNT wastewaters |
| KR20120102120A (ko) * | 2009-12-16 | 2012-09-17 | 바스프 에스이 | Dnt 폐수의 산성 톨루엔 추출 |
| WO2011082977A1 (de) * | 2009-12-16 | 2011-07-14 | Basf Se | VERFAHREN ZUR AUFARBEITUNG VON NOx-HALTIGEN ABGASEN AUS ABWASSERSTRÖMEN VON NITRIERANLAGEN |
| US9778685B2 (en) | 2011-05-04 | 2017-10-03 | Apple Inc. | Housing for portable electronic device with reduced border region |
| US9213451B2 (en) | 2010-06-04 | 2015-12-15 | Apple Inc. | Thin glass for touch panel sensors and methods therefor |
| US8923693B2 (en) | 2010-07-30 | 2014-12-30 | Apple Inc. | Electronic device having selectively strengthened cover glass |
| EP2418176A1 (de) * | 2010-08-12 | 2012-02-15 | Basf Se | Verfahren zur Aufreinigung von Abwässern aus der Aufarbeitung vom rohem Mononitrobenzol |
| US10189743B2 (en) | 2010-08-18 | 2019-01-29 | Apple Inc. | Enhanced strengthening of glass |
| US8873028B2 (en) | 2010-08-26 | 2014-10-28 | Apple Inc. | Non-destructive stress profile determination in chemically tempered glass |
| US8824140B2 (en) | 2010-09-17 | 2014-09-02 | Apple Inc. | Glass enclosure |
| US9725359B2 (en) | 2011-03-16 | 2017-08-08 | Apple Inc. | Electronic device having selectively strengthened glass |
| US10781135B2 (en) | 2011-03-16 | 2020-09-22 | Apple Inc. | Strengthening variable thickness glass |
| US9128666B2 (en) | 2011-05-04 | 2015-09-08 | Apple Inc. | Housing for portable electronic device with reduced border region |
| CN102295380A (zh) * | 2011-08-19 | 2011-12-28 | 杭州江南科学研究院有限公司 | 芳香族硝基化合物废水的处理和回收方法 |
| US9944554B2 (en) | 2011-09-15 | 2018-04-17 | Apple Inc. | Perforated mother sheet for partial edge chemical strengthening and method therefor |
| US9516149B2 (en) | 2011-09-29 | 2016-12-06 | Apple Inc. | Multi-layer transparent structures for electronic device housings |
| CN102557179A (zh) * | 2011-11-17 | 2012-07-11 | 南京理工大学 | 一种高浓度废酸中硝基甲苯的去除方法 |
| US10144669B2 (en) | 2011-11-21 | 2018-12-04 | Apple Inc. | Self-optimizing chemical strengthening bath for glass |
| US10133156B2 (en) | 2012-01-10 | 2018-11-20 | Apple Inc. | Fused opaque and clear glass for camera or display window |
| US8684613B2 (en) | 2012-01-10 | 2014-04-01 | Apple Inc. | Integrated camera window |
| US8773848B2 (en) | 2012-01-25 | 2014-07-08 | Apple Inc. | Fused glass device housings |
| US9249083B2 (en) | 2012-04-25 | 2016-02-02 | Basf Se | Process for scrubbing dinitrotoluene |
| JP6193358B2 (ja) | 2012-04-25 | 2017-09-06 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | ジニトロトルエンを洗浄する方法 |
| DE102012215903A1 (de) * | 2012-09-07 | 2014-03-13 | Evonik Industries Ag | Verfahren zur Behandlung eines Abwasserstroms, der bei der Aufarbeitung eines Triacetonamin-haltigen Reaktionsgemisches entsteht |
| CN102836570A (zh) * | 2012-09-19 | 2012-12-26 | 辽宁庆阳特种化工有限公司 | 一种对间二硝基苯生产过程中产生废酸的萃取分离方法及装置 |
| US9946302B2 (en) | 2012-09-19 | 2018-04-17 | Apple Inc. | Exposed glass article with inner recessed area for portable electronic device housing |
| US9459661B2 (en) | 2013-06-19 | 2016-10-04 | Apple Inc. | Camouflaged openings in electronic device housings |
| US9886062B2 (en) | 2014-02-28 | 2018-02-06 | Apple Inc. | Exposed glass article with enhanced stiffness for portable electronic device housing |
| JP6736547B2 (ja) * | 2014-10-02 | 2020-08-05 | コベストロ、ドイチュラント、アクチエンゲゼルシャフトCovestro Deutschland Ag | ジニトロトルエンの連続的製造方法における排出ガス清浄 |
| CN106145481A (zh) * | 2016-08-31 | 2016-11-23 | 格斯瑞科技有限公司 | 基于空化技术处理有机工业废水的装置和方法 |
| KR101890209B1 (ko) | 2016-12-08 | 2018-08-21 | 주식회사 풍산 | Tnt 폐수의 처리 방법 및 장치 |
| CN107055899A (zh) * | 2017-02-27 | 2017-08-18 | 广东工业大学 | 一种含高浓度酚废水的处理方法 |
| CN108440300A (zh) * | 2018-05-15 | 2018-08-24 | 福建省东南电化股份有限公司 | 一种硝化废酸浓缩过程中防止堵塞的方法 |
| KR20180093857A (ko) | 2018-08-14 | 2018-08-22 | 주식회사 풍산 | Tnt 또는 방향족 화합물이 포함된 오염수의 처리방법 및 장치 |
| DE102018217955B4 (de) * | 2018-10-19 | 2020-06-04 | Plinke Gmbh | Verfahren zur Aufarbeitung von Mischsäure und Abwasser aus der Nitrierung von Aromaten sowie Vorrichtung zur Durchführung des Verfahrens |
| CN109627170B (zh) * | 2018-12-17 | 2021-09-14 | 湖北东方化工有限公司 | 从硝基甲苯酸性废水提取多硝基甲苯的方法 |
| CN110170185B (zh) * | 2019-05-30 | 2023-07-25 | 湖北东方化工有限公司 | 一种废硫酸硝基化合物分离的装置及方法 |
| CN111620504A (zh) * | 2020-06-04 | 2020-09-04 | 湖北东方化工有限公司 | 一种多硝基甲苯生产预洗废水处理新工艺的生产方法 |
| CN111603869A (zh) * | 2020-06-04 | 2020-09-01 | 湖北东方化工有限公司 | 一种多硝基甲苯粉尘收集新工艺 |
| CN113354006A (zh) * | 2021-05-31 | 2021-09-07 | 湖北东方化工有限公司 | 一种多硝基甲苯废硫酸真空浓缩装置高酸度废水处理工艺及装置 |
| CN115477286B (zh) * | 2022-10-27 | 2024-08-16 | 湖北东方化工有限公司 | 一种一硝基甲苯废硫酸预处理装置及其处理方法 |
| CN116375127A (zh) * | 2023-04-17 | 2023-07-04 | 沧州大化股份有限公司 | 一种二硝基甲苯生产中废水的处理方法 |
| CN119430364B (zh) * | 2024-10-22 | 2025-05-13 | 安徽华尔泰化工股份有限公司 | 一种混二硝基苯生产废酸分离装置及分离方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3742072A (en) * | 1972-03-28 | 1973-06-26 | M Roth | Nitration of toluene and nitrotoluenes to form tnt |
| DE2818680A1 (de) * | 1978-04-27 | 1979-10-31 | Bayer Ag | Verfahren zur aufarbeitung von nitro-hydroxy-aromaten enthaltenden abwaessern |
| US4257986A (en) * | 1979-02-02 | 1981-03-24 | Air Products And Chemicals, Inc. | Process for refining aqueous acid mixtures utilized in nitration of aromatics |
| US4241229A (en) * | 1979-08-08 | 1980-12-23 | American Cyanamid Company | Recovery of nitrated aromatic compounds from nitration wash liquors |
| US4642396A (en) * | 1984-08-07 | 1987-02-10 | Air Products And Chemicals, Inc. | Process for separating nitroaromatic compounds from spent nitric acid |
| US4597875A (en) * | 1985-05-07 | 1986-07-01 | Air Products And Chemicals, Inc. | Precipitative removal of nitrocresols from dinitrotoluene waste streams |
| US5606948A (en) * | 1996-02-27 | 1997-03-04 | Briggs & Stratton Corporation | Speed governing method and apparatus for an internal combustion engine |
| US5762802A (en) * | 1997-05-01 | 1998-06-09 | Air Products And Chemicals, Inc. | Dilute acid oxidation of dinitrotoluene alkaline wash water |
| FR2767319B1 (fr) * | 1997-08-13 | 1999-10-29 | Rhone Poulenc Chimie | Procede de traitement de solutions aqueuses comprenant des acides et des composes nitres |
| US6288289B1 (en) * | 2000-01-27 | 2001-09-11 | Noram Engineering And Constructors Ltd. | Integrated effluent treatment process for nitroaromatic manufacture |
| US6506948B1 (en) * | 2002-02-07 | 2003-01-14 | Air Products And Chemicals, Inc. | Toluene extraction of dinitrotoluene wash water |
-
2003
- 2003-06-30 DE DE10329304A patent/DE10329304A1/de not_active Withdrawn
-
2004
- 2004-06-17 EP EP04014227A patent/EP1496043B1/de not_active Expired - Lifetime
- 2004-06-17 AT AT04014227T patent/ATE462686T1/de not_active IP Right Cessation
- 2004-06-17 PL PL04014227T patent/PL1496043T3/pl unknown
- 2004-06-17 DE DE502004010954T patent/DE502004010954D1/de not_active Expired - Lifetime
- 2004-06-28 US US10/878,211 patent/US6936741B2/en not_active Expired - Lifetime
- 2004-06-29 KR KR1020040049538A patent/KR101093862B1/ko not_active Expired - Fee Related
- 2004-06-29 TW TW093118911A patent/TW200516051A/zh unknown
- 2004-06-29 CN CNB2004100633015A patent/CN1285514C/zh not_active Expired - Fee Related
- 2004-06-30 JP JP2004194525A patent/JP4778209B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| KR20050002620A (ko) | 2005-01-07 |
| EP1496043B1 (de) | 2010-03-31 |
| DE10329304A1 (de) | 2005-02-03 |
| ATE462686T1 (de) | 2010-04-15 |
| EP1496043A1 (de) | 2005-01-12 |
| JP4778209B2 (ja) | 2011-09-21 |
| CN1285514C (zh) | 2006-11-22 |
| TW200516051A (en) | 2005-05-16 |
| US6936741B2 (en) | 2005-08-30 |
| US20040262238A1 (en) | 2004-12-30 |
| KR101093862B1 (ko) | 2011-12-13 |
| CN1576236A (zh) | 2005-02-09 |
| JP2005021890A (ja) | 2005-01-27 |
| DE502004010954D1 (de) | 2010-05-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| PL1496043T3 (pl) | Sposób uzdatniania ścieków powstających przy wytwarzaniu dinitrotoluenu | |
| US7470826B2 (en) | Recovery of nitrating acid mixtures from nitration processes | |
| ATE444947T1 (de) | Verfahren zur aufarbeitung von nebenkomponenten der dinitroluolherstellung | |
| EA200401458A1 (ru) | Способ (варианты) для обработки жидких сред обратным осмосом в кислых условиях | |
| DK1330414T3 (da) | Fremgangsmåde til behandling af vand og spildevand | |
| TW200513454A (en) | Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid | |
| TWI265045B (en) | Water-generating process and water generator | |
| CA2467001A1 (en) | Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid | |
| BR0311930A (pt) | Processo para a produção de água purificada a partir da água de reação de fischer-tropsch | |
| EA200700200A1 (ru) | Способ заводнения | |
| KR890003435A (ko) | 연도가스 및 연소잔류물의 처리방법 | |
| EP0399573A3 (en) | Process for recovery of amino acid from aqueous mixtures | |
| IL132347A (en) | Method for removing acidic gases from waste gas | |
| PL1993990T3 (pl) | Sposób destylacyjnego wydzielania dinitrotoluenu ze ścieków procesowych z wytwarzania dinitrotoluenu przez nitrowanie toluenu mieszaniną nitrującą | |
| ES2189764T3 (es) | Proceso para la separacion y purificacion de una mezcla acuosa que tiene como componentes principales acido acetico y acido formico. | |
| MX2010002870A (es) | Proceso para la produccion de di y poliaminas de las series del difenilmetano. | |
| KR20160078387A (ko) | 시안화수소산의 존재하에 디니트로톨루엔의 산 스크러빙 방법 | |
| RU2015110046A (ru) | Гидрометаллургический способ с применением многоступенчатой нанофильтрации | |
| WO2004028986A3 (fr) | Procede de traitement d'eaux residuaires par bio-reacteur a membranes | |
| FI20010475A0 (fi) | Menetelmä kalsiumin poistamiseksi sinkkiprosessin sulfaattiliuoksista | |
| ATE549310T1 (de) | Verfahren zur herstellung von dinitrotoluol wobei nitrokresolhaltige extrakte als einsatzstoff mitverwendet werden. | |
| ATE529383T1 (de) | Verfahren und vorrichtung zur herstellung von calciumbromid durch flüssig-flüssig extraktion | |
| RU2003105364A (ru) | Способ переработки твердых отходов или шламов | |
| HUP0402631A2 (en) | Method for decreasing the organic compound content of alkaline wash water occuring during the production of dinitrotoluene | |
| RU2002111626A (ru) | Способ экстракции кобальта из водных растворов |