PL2705020T3 - Sposób i urządzenie do oczyszczania produktów nitrowania - Google Patents
Sposób i urządzenie do oczyszczania produktów nitrowaniaInfo
- Publication number
- PL2705020T3 PL2705020T3 PL12723831T PL12723831T PL2705020T3 PL 2705020 T3 PL2705020 T3 PL 2705020T3 PL 12723831 T PL12723831 T PL 12723831T PL 12723831 T PL12723831 T PL 12723831T PL 2705020 T3 PL2705020 T3 PL 2705020T3
- Authority
- PL
- Poland
- Prior art keywords
- purification
- nitration products
- nitration
- products
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/16—Separation; Purification; Stabilisation; Use of additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/06—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/24—Stationary reactors without moving elements inside
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- General Preparation And Processing Of Foods (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102011102059 | 2011-05-19 | ||
| EP12723831.9A EP2705020B2 (de) | 2011-05-19 | 2012-05-18 | Verfahren und vorrichtung zur aufreinigung von nitrierprodukten |
| PCT/EP2012/002139 WO2012156095A1 (de) | 2011-05-19 | 2012-05-18 | Verfahren und vorrichtung zur aufreinigung von nitrierprodukten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL2705020T3 true PL2705020T3 (pl) | 2015-09-30 |
Family
ID=46172762
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL12723831T PL2705020T3 (pl) | 2011-05-19 | 2012-05-18 | Sposób i urządzenie do oczyszczania produktów nitrowania |
| PL13005208T PL2772304T3 (pl) | 2011-05-19 | 2012-05-18 | Urządzenia do oczyszczania poddanych nitrowaniu produktów |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL13005208T PL2772304T3 (pl) | 2011-05-19 | 2012-05-18 | Urządzenia do oczyszczania poddanych nitrowaniu produktów |
Country Status (15)
| Country | Link |
|---|---|
| US (2) | US9115048B2 (pl) |
| EP (2) | EP2772304B2 (pl) |
| JP (1) | JP5818287B2 (pl) |
| KR (1) | KR101587109B1 (pl) |
| CN (1) | CN103562174B (pl) |
| BR (1) | BR112013029323A2 (pl) |
| CA (1) | CA2835121C (pl) |
| DE (1) | DE102012009787A1 (pl) |
| EA (1) | EA024988B1 (pl) |
| ES (2) | ES2633799T3 (pl) |
| HU (2) | HUE033730T2 (pl) |
| PL (2) | PL2705020T3 (pl) |
| PT (2) | PT2705020E (pl) |
| UA (1) | UA108437C2 (pl) |
| WO (1) | WO2012156095A1 (pl) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3061239B2 (ja) | 1994-03-31 | 2000-07-10 | 矢崎総業株式会社 | ハウジング分離供給装置及びハウジング分離供給方法 |
| WO2014122596A2 (pt) * | 2013-02-05 | 2014-08-14 | Cuf - Químicos Industriais S.A. | Processo de remoção de compostos nitrofenólicos na produção de mononitrobenzeno |
| PT106909B (pt) * | 2013-04-26 | 2017-06-01 | Cuf - Quim Ind S A | Processo e equipamento para remoção de impurezas de compostos aromáticos nitrados |
| DE102013110952B4 (de) * | 2013-08-15 | 2015-11-26 | Josef Meissner Gmbh & Co. Kg | Verfahren zur Entfernung von bei der Herstellung von aliphatischen Nitratestern anfallenden Verunreinigungen |
| DE102015106617B4 (de) | 2014-07-07 | 2017-09-21 | Josef Meissner Gmbh & Co. Kg | Verfahren zur Aufreinigung von Rohdinitrotoluolen |
| CN107750244B (zh) | 2015-06-12 | 2021-01-01 | 诺拉姆国际公司 | 一种纯化来自硝化过程的硝化芳香族化合物的方法 |
| DE102017110084C5 (de) * | 2017-02-03 | 2026-02-26 | Josef Meissner Gmbh & Co. Kg | Verwendungen von Nitroaromaten in der adiabatischen Nitrierung von Aromaten |
| CN109627170B (zh) * | 2018-12-17 | 2021-09-14 | 湖北东方化工有限公司 | 从硝基甲苯酸性废水提取多硝基甲苯的方法 |
| RU2712699C1 (ru) * | 2019-02-20 | 2020-01-30 | Федеральное Казенное Предприятие "Бийский Олеумный Завод" | Способ получения смеси динитротолуола с тринитротолуолом (варианты) |
| CN117567289A (zh) * | 2024-01-17 | 2024-02-20 | 万华化学集团股份有限公司 | 一种粗dnt一次洗涤工艺 |
Family Cites Families (43)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE528983A (pl) | ||||
| BE518008A (pl) | ||||
| DE732742C (de) | 1940-01-09 | 1943-03-10 | Meissner Fa Josef | Verfahren zum kontinuierlichen Waschen von Trinitrotoluol |
| DE1057081B (de) | 1955-06-16 | 1959-05-14 | Dynamit Nobel Ag | Verfahren und Vorrichtung zur kontinuierlichen Reinigung von Trinitrotoluol unter Gewinnung eines besonders reinen Trinitrotolulols |
| US3111538A (en) | 1957-02-07 | 1963-11-19 | Hercules Powder Co Ltd | Continuous manufacture of explosive liquid nitric acid esters |
| NL258275A (pl) | 1959-12-03 | |||
| DE1222904B (de) | 1963-10-29 | 1966-08-18 | Bayer Ag | Verfahren zur Reinigung von nitrophenolhaltigen rohen aromatischen Nitroverbindungen |
| GB1081092A (en) | 1964-01-08 | 1967-08-31 | Ici Ltd | Purification of dinitrotoluenes |
| US3409620A (en) | 1967-02-06 | 1968-11-05 | Mario Biazzi Sa Dr Ing | Continuous manufacture in vacuum of nitric esters and/or organic nitro compounds |
| US3704006A (en) | 1971-01-25 | 1972-11-28 | Kenics Corp | Dispersion producing method |
| BE790131A (fr) | 1971-10-14 | 1973-04-16 | Basf Ag | Procede et dispositif de melange de liquides |
| US3847375A (en) * | 1972-10-12 | 1974-11-12 | Basf Ag | Method and apparatus for mixing liquids |
| CA1034603A (en) | 1973-10-05 | 1978-07-11 | Allied Chemical Corporation | Water washing of nitroaromatic compounds prior to catalytic reduction |
| NL7403883A (nl) | 1974-03-22 | 1975-09-24 | Philips Nv | Werkwijze en inrichting voor extraktie bij vloei- stoffen. |
| US4091042A (en) | 1977-08-19 | 1978-05-23 | American Cyanamid Company | Continuous adiabatic process for the mononitration of benzene |
| US4314974A (en) | 1979-04-30 | 1982-02-09 | Chemineer, Inc. | Solvent extraction method using static mixers |
| US4453027A (en) | 1982-12-10 | 1984-06-05 | Monsanto Company | Adiabatic process for the nitration of halobenzenes |
| US4482769A (en) * | 1983-09-16 | 1984-11-13 | Air Products And Chemicals, Inc. | Reducing 2,4-dinitroortho-cresol in effluent stream from dinitrotoluene process |
| US4597875A (en) | 1985-05-07 | 1986-07-01 | Air Products And Chemicals, Inc. | Precipitative removal of nitrocresols from dinitrotoluene waste streams |
| DE3705091A1 (de) * | 1987-02-18 | 1988-09-01 | Bayer Ag | Verfahren zur abtrennung von schwefelsaeure und salpetersaeure aus bei der nitrierung von toluol erhaltenen dinitrotoluolgemischen |
| US4994242A (en) | 1988-08-15 | 1991-02-19 | Noram Engineering And Constructors Ltd. | Jet impingement reactor |
| US5514820A (en) | 1989-09-29 | 1996-05-07 | Henkel Kommanditgesellschaft Auf Aktien | Continuous process for the production of lower alkyl esters |
| DE4121212A1 (de) | 1991-06-27 | 1993-01-14 | Bayer Ag | Verfahren zur herstellung von polycarbonat |
| DE4227372A1 (de) | 1991-10-12 | 1993-04-22 | Bayer Ag | Verfahren zur herstellung von polycarbonaten |
| DE4238390A1 (de) | 1992-11-13 | 1994-05-19 | Bayer Ag | Verfahren zur Herstellung von Dinitrotoluol |
| DE4437047A1 (de) | 1994-10-17 | 1996-04-18 | Bayer Ag | Verfahren zur Dinitrierung von aromatischen Verbindungen |
| DE19512114C2 (de) | 1995-04-04 | 2000-04-27 | Meissner Gmbh & Co Kg Josef | Rückgewinnung von Salpetersäure aus Nitrierprozessen |
| DE19539205A1 (de) | 1995-10-22 | 1997-04-24 | Meissner Gmbh & Co Kg Josef | Verfahren zur Aromatennitrierung |
| US6350354B1 (en) | 1999-09-03 | 2002-02-26 | Koch-Glitsch, Inc. | Modular solvent extraction plant |
| US6288289B1 (en) | 2000-01-27 | 2001-09-11 | Noram Engineering And Constructors Ltd. | Integrated effluent treatment process for nitroaromatic manufacture |
| JP4485731B2 (ja) | 2000-03-02 | 2010-06-23 | ダウ グローバル テクノロジーズ インコーポレイティド | 管状反応器、管状反応器中で液/液多相反応を行うための方法及び管状反応器中で芳香族化合物を環ニトロ化するための方法 |
| DE10307140A1 (de) * | 2003-02-20 | 2004-09-09 | Bayer Ag | Verfahren zur zweistufigen Herstellung von Dinitrotoluol |
| DE102004017628A1 (de) | 2004-04-10 | 2005-11-03 | Bayer Materialscience Ag | Verfahren zur Aufarbeitung von aromatische Nitroverbindungen enthaltenden Abwässern |
| CN1597557A (zh) † | 2004-09-01 | 2005-03-23 | 中国石化集团南京化学工业有限公司 | 采用静态混合器进行芳烃硝化物中和水洗方法 |
| CN2729072Y (zh) † | 2004-10-09 | 2005-09-28 | 沈阳化工学院 | 硝基苯洗涤生产装置 |
| CN1757630A (zh) | 2004-10-09 | 2006-04-12 | 沈阳化工学院 | 硝基苯洗涤生产装置和洗涤生产方法 |
| DE102005050106B4 (de) * | 2005-10-18 | 2008-04-30 | Josef Meissner Gmbh & Co. Kg | Rückgewinnung von Nitriersäuregemischen aus Nitrienprozessen |
| DE102006004943A1 (de) * | 2006-02-03 | 2007-08-09 | Bayer Materialscience Ag | Verfahren zur Herstellung von Nitrobenzol |
| CN101735066A (zh) | 2008-11-18 | 2010-06-16 | 董安成 | 芳烃硝化物中和水洗新方法 |
| RU2404171C2 (ru) | 2008-12-16 | 2010-11-20 | Алексей Андреевич Брункин | Способ непрерывного получения 2-меркаптобензтиазола в трубчатом реакторе и устройство для его проведения |
| CN102471092B (zh) | 2009-08-18 | 2013-11-06 | 诺拉姆国际公司 | 用于硝基芳族化合物的洗涤系统 |
| BR112012004604A2 (pt) | 2009-08-31 | 2016-04-05 | Basf Se | processo para preparar de maneira contínua aromáticos nitrados |
| DE102011120587A1 (de) | 2011-12-08 | 2013-06-13 | Oxea Gmbh | Verfahren zur Gewinnung von aliphatischen Monocarbonsäuren aus Destillationsrückständen |
-
2012
- 2012-05-18 EP EP13005208.7A patent/EP2772304B2/de active Active
- 2012-05-18 EP EP12723831.9A patent/EP2705020B2/de active Active
- 2012-05-18 PT PT127238319T patent/PT2705020E/pt unknown
- 2012-05-18 KR KR1020137033709A patent/KR101587109B1/ko active Active
- 2012-05-18 US US14/118,737 patent/US9115048B2/en active Active
- 2012-05-18 JP JP2014510693A patent/JP5818287B2/ja active Active
- 2012-05-18 CA CA2835121A patent/CA2835121C/en active Active
- 2012-05-18 UA UAA201314700A patent/UA108437C2/ru unknown
- 2012-05-18 PL PL12723831T patent/PL2705020T3/pl unknown
- 2012-05-18 HU HUE13005208A patent/HUE033730T2/en unknown
- 2012-05-18 PT PT130052087T patent/PT2772304T/pt unknown
- 2012-05-18 ES ES13005208.7T patent/ES2633799T3/es active Active
- 2012-05-18 WO PCT/EP2012/002139 patent/WO2012156095A1/de not_active Ceased
- 2012-05-18 ES ES12723831.9T patent/ES2539787T3/es active Active
- 2012-05-18 HU HUE12723831A patent/HUE026436T2/en unknown
- 2012-05-18 CN CN201280024399.6A patent/CN103562174B/zh active Active
- 2012-05-18 BR BR112013029323A patent/BR112013029323A2/pt active Search and Examination
- 2012-05-18 PL PL13005208T patent/PL2772304T3/pl unknown
- 2012-05-18 DE DE102012009787A patent/DE102012009787A1/de not_active Withdrawn
- 2012-05-18 EA EA201391727A patent/EA024988B1/ru not_active IP Right Cessation
-
2015
- 2015-02-26 US US14/632,086 patent/US9540313B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP2705020A1 (de) | 2014-03-12 |
| PL2772304T3 (pl) | 2017-10-31 |
| US20140221703A1 (en) | 2014-08-07 |
| WO2012156095A1 (de) | 2012-11-22 |
| CN103562174B (zh) | 2015-05-20 |
| EP2772304A3 (de) | 2014-11-05 |
| EP2705020B1 (de) | 2015-04-08 |
| DE102012009787A1 (de) | 2012-11-22 |
| CA2835121A1 (en) | 2012-11-22 |
| US20150174551A1 (en) | 2015-06-25 |
| ES2633799T3 (es) | 2017-09-25 |
| EP2772304B1 (de) | 2017-05-10 |
| CN103562174A (zh) | 2014-02-05 |
| HUE026436T2 (en) | 2016-06-28 |
| ES2539787T3 (es) | 2015-07-06 |
| HUE033730T2 (en) | 2018-01-29 |
| EP2772304A2 (de) | 2014-09-03 |
| US9115048B2 (en) | 2015-08-25 |
| PT2772304T (pt) | 2017-07-14 |
| CA2835121C (en) | 2015-12-29 |
| BR112013029323A2 (pt) | 2017-01-31 |
| US9540313B2 (en) | 2017-01-10 |
| UA108437C2 (uk) | 2015-04-27 |
| KR20140032446A (ko) | 2014-03-14 |
| EA024988B1 (ru) | 2016-11-30 |
| KR101587109B1 (ko) | 2016-01-20 |
| EA201391727A1 (ru) | 2014-03-31 |
| JP5818287B2 (ja) | 2015-11-18 |
| EP2705020B2 (de) | 2025-11-05 |
| EP2772304B2 (de) | 2024-08-07 |
| JP2014518866A (ja) | 2014-08-07 |
| PT2705020E (pt) | 2015-07-24 |
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