PL3568389T3 - Proces oczyszczania kaprolaktamu z roztworu surowego kaprolaktamu bez ekstrakcji rozpuszczalnikiem organicznym - Google Patents

Proces oczyszczania kaprolaktamu z roztworu surowego kaprolaktamu bez ekstrakcji rozpuszczalnikiem organicznym

Info

Publication number
PL3568389T3
PL3568389T3 PL17838004T PL17838004T PL3568389T3 PL 3568389 T3 PL3568389 T3 PL 3568389T3 PL 17838004 T PL17838004 T PL 17838004T PL 17838004 T PL17838004 T PL 17838004T PL 3568389 T3 PL3568389 T3 PL 3568389T3
Authority
PL
Poland
Prior art keywords
caprolactam
purification
solution
organic solvent
solvent extraction
Prior art date
Application number
PL17838004T
Other languages
English (en)
Inventor
Anacleto Dal Moro
Michele CECCHETTO
Denis Jahic
Vid Margon
Original Assignee
Aquafilslo D.O.O.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aquafilslo D.O.O. filed Critical Aquafilslo D.O.O.
Publication of PL3568389T3 publication Critical patent/PL3568389T3/pl

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/16—Separation or purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0492—Applications, solvents used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10—Vacuum distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/148—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/04—Preparation of lactams from or via oximes by Beckmann rearrangement
    • C07D201/06—Preparation of lactams from or via oximes by Beckmann rearrangement from ketones by simultaneous oxime formation and rearrangement
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
    • C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D223/08—Oxygen atoms
    • C07D223/10—Oxygen atoms attached in position 2

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
PL17838004T 2017-12-15 2017-12-15 Proces oczyszczania kaprolaktamu z roztworu surowego kaprolaktamu bez ekstrakcji rozpuszczalnikiem organicznym PL3568389T3 (pl)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PCT/SI2017/050010 WO2019117817A1 (en) 2017-12-15 2017-12-15 Process for the purification of caprolactam from a solution of crude caprolactam without organic solvent extraction
EP17838004.4A EP3568389B1 (en) 2017-12-15 2017-12-15 Process for the purification of caprolactam from a solution of crude caprolactam without organic solvent extraction

Publications (1)

Publication Number Publication Date
PL3568389T3 true PL3568389T3 (pl) 2021-06-28

Family

ID=61148459

Family Applications (1)

Application Number Title Priority Date Filing Date
PL17838004T PL3568389T3 (pl) 2017-12-15 2017-12-15 Proces oczyszczania kaprolaktamu z roztworu surowego kaprolaktamu bez ekstrakcji rozpuszczalnikiem organicznym

Country Status (10)

Country Link
US (2) US10787417B2 (pl)
EP (1) EP3568389B1 (pl)
JP (1) JP6852181B2 (pl)
CN (1) CN110494420B (pl)
EA (1) EA038223B1 (pl)
ES (1) ES2860825T3 (pl)
HU (1) HUE053673T2 (pl)
PL (1) PL3568389T3 (pl)
SI (1) SI3568389T1 (pl)
WO (1) WO2019117817A1 (pl)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT201800021409A1 (it) * 2018-12-28 2020-06-28 Aquafil S P A Processo per la produzione di epsilon caprolattame dall’acido 6-aminocaproico.
IT202100028601A1 (it) 2021-11-10 2023-05-10 Aquafil S P A Procedimento per produrre epsilon-caprolattame mediante depolimerizzazione di policaprolattame (pa6).
CN115253380B (zh) * 2022-08-19 2023-09-01 清元智能科技研究院(湖北)有限公司 一种己内酰胺萃取系统和方法
WO2024175671A1 (en) 2023-02-22 2024-08-29 Basf Se Process for depolymerizing polyamide prepared from caprolactam

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1258810A (pl) * 1968-03-30 1971-12-30
DE1926932A1 (de) * 1968-07-19 1970-01-22 Leuna Werke Veb Verfahren zur Reinigung von Lactamen
DE2301587C3 (de) * 1973-01-13 1981-02-26 Bayer Ag, 5090 Leverkusen Verfahren zur Entfernung von Borsäure aus Lactamen
CH593934A5 (pl) * 1974-09-03 1977-12-30 Inventa Ag
IT1113404B (it) * 1979-02-28 1986-01-20 Snia Viscosa Internazionale brevetti s.r.l.via brentano 2 milano
JPS57165364A (en) * 1981-04-06 1982-10-12 Unitika Ltd Purification of recovered lactam
US6162906A (en) * 1991-08-08 2000-12-19 Fmc Corporation Clarified konjac glucomannan
EP1373201B1 (en) * 2001-03-01 2011-02-16 DSM IP Assets B.V. Process for recovering and purifying caprolactam from an organic solvent
EP1764542A1 (de) * 2005-09-19 2007-03-21 Siemens Aktiengesellschaft Bausatz zur Erstellung einer Industrieanlage
JP2008056620A (ja) * 2006-08-31 2008-03-13 Toray Ind Inc 回収ε−カプロラクタムの精製法
DE102011055889B4 (de) * 2011-11-30 2013-08-01 Otc Gmbh Verfahren zur Herstellung eines Protein-Hydrolysates

Also Published As

Publication number Publication date
US10787417B2 (en) 2020-09-29
EP3568389A1 (en) 2019-11-20
EA038223B1 (ru) 2021-07-27
CN110494420B (zh) 2023-05-12
US20190382339A1 (en) 2019-12-19
JP6852181B2 (ja) 2021-03-31
EP3568389B1 (en) 2021-01-20
CN110494420A (zh) 2019-11-22
US20210040036A1 (en) 2021-02-11
SI3568389T1 (sl) 2021-03-31
US11208380B2 (en) 2021-12-28
JP2020514350A (ja) 2020-05-21
WO2019117817A1 (en) 2019-06-20
EA201991703A1 (ru) 2020-01-09
ES2860825T3 (es) 2021-10-05
HUE053673T2 (hu) 2021-07-28

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