PL3577067T3 - Wysoko reaktywny, bezpyłowy i swobodnie płynący siarczek litu oraz sposób jego wytwarzania - Google Patents

Wysoko reaktywny, bezpyłowy i swobodnie płynący siarczek litu oraz sposób jego wytwarzania

Info

Publication number
PL3577067T3
PL3577067T3 PL18704197.5T PL18704197T PL3577067T3 PL 3577067 T3 PL3577067 T3 PL 3577067T3 PL 18704197 T PL18704197 T PL 18704197T PL 3577067 T3 PL3577067 T3 PL 3577067T3
Authority
PL
Poland
Prior art keywords
free
dust
producing
highly reactive
lithium sulfide
Prior art date
Application number
PL18704197.5T
Other languages
English (en)
Inventor
Hannes Vitze
Vera NICKEL
Sebastian Lang
Marc-Christian Müller
Sebastian Pietzner
Armine PLATH
Original Assignee
Albemarle Germany Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Albemarle Germany Gmbh filed Critical Albemarle Germany Gmbh
Publication of PL3577067T3 publication Critical patent/PL3577067T3/pl

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/04—Halides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/22—Alkali metal sulfides or polysulfides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/22—Alkali metal sulfides or polysulfides
    • C01B17/38—Dehydration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/02—Oxides; Hydroxides
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0561—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of inorganic materials only
    • H01M10/0562—Solid materials
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/24—Alkaline accumulators
    • H01M10/26—Selection of materials as electrolytes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/581—Chalcogenides or intercalation compounds thereof
    • H01M4/5815—Sulfides
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M6/00—Primary cells; Manufacture thereof
    • H01M6/14—Cells with non-aqueous electrolyte
    • H01M6/18—Cells with non-aqueous electrolyte with solid electrolyte
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/20—Powder free flowing behaviour
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028—Positive electrodes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00—Electrolytes
    • H01M2300/0017—Non-aqueous electrolytes
    • H01M2300/0065—Solid electrolytes
    • H01M2300/0068—Solid electrolytes inorganic
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
PL18704197.5T 2017-02-03 2018-02-02 Wysoko reaktywny, bezpyłowy i swobodnie płynący siarczek litu oraz sposób jego wytwarzania PL3577067T3 (pl)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102017201772 2017-02-03
PCT/EP2018/052688 WO2018141919A1 (de) 2017-02-03 2018-02-02 Hochreaktives, staubfreies und freifliessendes lithiumsulfid und verfahren zu dessen herstellung

Publications (1)

Publication Number Publication Date
PL3577067T3 true PL3577067T3 (pl) 2026-04-07

Family

ID=61189440

Family Applications (1)

Application Number Title Priority Date Filing Date
PL18704197.5T PL3577067T3 (pl) 2017-02-03 2018-02-02 Wysoko reaktywny, bezpyłowy i swobodnie płynący siarczek litu oraz sposób jego wytwarzania

Country Status (14)

Country Link
US (1) US11542162B2 (pl)
EP (2) EP3577067B1 (pl)
KR (1) KR102485791B1 (pl)
CN (1) CN110475745B (pl)
AR (1) AR110926A1 (pl)
AU (1) AU2018214232B2 (pl)
CA (1) CA3050338A1 (pl)
ES (1) ES3063468T3 (pl)
IL (1) IL268424B (pl)
MX (1) MX2019008901A (pl)
PL (1) PL3577067T3 (pl)
TW (1) TWI748052B (pl)
WO (1) WO2018141919A1 (pl)
ZA (1) ZA201905012B (pl)

Families Citing this family (39)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10147968B2 (en) 2014-12-02 2018-12-04 Polyplus Battery Company Standalone sulfide based lithium ion-conducting glass solid electrolyte and associated structures, cells and methods
US20190173128A1 (en) 2014-12-02 2019-06-06 Polyplus Battery Company Making and inspecting a web of vitreous lithium sulfide separator sheet and lithium electrode assemblies and battery cells
US12454478B2 (en) 2022-09-09 2025-10-28 Polyplus Battery Company Ionically conductive glass preform
US12051824B2 (en) 2020-07-10 2024-07-30 Polyplus Battery Company Methods of making glass constructs
US10164289B2 (en) 2014-12-02 2018-12-25 Polyplus Battery Company Vitreous solid electrolyte sheets of Li ion conducting sulfur-based glass and associated structures, cells and methods
US11984553B2 (en) 2014-12-02 2024-05-14 Polyplus Battery Company Lithium ion conducting sulfide glass fabrication
US12294050B2 (en) 2014-12-02 2025-05-06 Polyplus Battery Company Lithium ion conducting sulfide glass fabrication
US11749834B2 (en) 2014-12-02 2023-09-05 Polyplus Battery Company Methods of making lithium ion conducting sulfide glass
US12482827B2 (en) 2021-04-13 2025-11-25 Polyplus Battery Company Binary phosphorus nitride protective solid electrolyte intermediary structures for electrode assemblies
US10707536B2 (en) 2016-05-10 2020-07-07 Polyplus Battery Company Solid-state laminate electrode assemblies and methods of making
US11631889B2 (en) 2020-01-15 2023-04-18 Polyplus Battery Company Methods and materials for protection of sulfide glass solid electrolytes
US10629950B2 (en) 2017-07-07 2020-04-21 Polyplus Battery Company Encapsulated sulfide glass solid electrolytes and solid-state laminate electrode assemblies
US10868293B2 (en) 2017-07-07 2020-12-15 Polyplus Battery Company Treating sulfide glass surfaces and making solid state laminate electrode assemblies
CN112125283A (zh) * 2020-08-03 2020-12-25 浙江工业大学 一种利用固液混合加热制备硫化锂的方法
US12021238B2 (en) 2020-08-04 2024-06-25 Polyplus Battery Company Glassy embedded solid-state electrode assemblies, solid-state batteries and methods of making electrode assemblies and solid-state batteries
US12021187B2 (en) 2020-08-04 2024-06-25 Polyplus Battery Company Surface treatment of a sulfide glass solid electrolyte layer
US12034116B2 (en) 2020-08-04 2024-07-09 Polyplus Battery Company Glass solid electrolyte layer, methods of making glass solid electrolyte layer and electrodes and battery cells thereof
CN112002939B (zh) * 2020-08-31 2021-10-15 成都新柯力化工科技有限公司 一种锂电池固体电解质的清洁制备方法
EP3964480A1 (en) * 2020-09-02 2022-03-09 AMG Lithium GmbH Process for preparing lithium salts
KR102603627B1 (ko) * 2020-12-18 2023-11-16 주식회사 포스코 황화리튬 및 이의 제조방법
JP7484737B2 (ja) * 2021-01-19 2024-05-16 トヨタ自動車株式会社 硫化物固体電解質、前駆体、全固体電池および硫化物固体電解質の製造方法
CN112939034B (zh) * 2021-03-19 2023-08-15 江西云威新材料有限公司 一种工业级碳酸锂制备电池级无水氢氧化锂的方法
US20250002342A1 (en) 2021-07-07 2025-01-02 Specialty Operations France Process of obtaining a powder of lithium sulfide, and use thereof to prepare a lps compound
JP7801857B2 (ja) * 2021-07-19 2026-01-19 古河機械金属株式会社 硫化リチウムの製造方法
WO2023032701A1 (ja) * 2021-09-02 2023-03-09 Agc株式会社 硫化リチウムの製造方法
EP4186997A1 (en) * 2021-11-26 2023-05-31 K-UTEC AG Salt Technologies Preparation of lithium hydroxide
KR102707192B1 (ko) * 2022-02-28 2024-09-20 주식회사 레이크테크놀로지 황화리튬 제조 장치
CN115535968A (zh) * 2022-10-12 2022-12-30 天津大学 一种硫化锂的制备方法及硫化锂
FR3143861B1 (fr) * 2022-12-20 2025-04-18 Eurecat Sa Procédé de production de sulfure de lithium dans un réacteur à lit circulant
DE102023102404A1 (de) * 2023-02-01 2024-08-01 Albemarle Germany Gmbh Verfahren zur Herstellung von an Kohlenstoffverunreinigung reduziertem/Kohlenstoffverunreinigung freiem Lithiumsulfid, das Kohlenstoffverunreinigung reduzierte/Kohlenstoffverunreinigung freie Lithiumsulfid sowie dessen Verwendung zur Herstellung von Festelektrolyten und Feststoffbatterien
JP2026510038A (ja) * 2023-03-10 2026-03-27 スペシャルティ オペレーションズ フランス 硫化物固体材料の粒子の調製方法
KR20250156773A (ko) 2023-03-10 2025-11-03 스페셜티 오퍼레이션스 프랑스 황화리튬 분말을 제조하는 방법
CN116354315B (zh) * 2023-03-30 2025-08-01 宁波容百新能源科技股份有限公司 一种硫化锂的制备方法及硫化锂
KR20240153192A (ko) * 2023-04-14 2024-10-22 주식회사 이수스페셜티케미컬 황화 리튬의 제조 방법
KR20250041384A (ko) * 2023-09-18 2025-03-25 에스케이이노베이션 주식회사 황화리튬 제조 방법
KR20250064382A (ko) * 2023-11-02 2025-05-09 에스케이이노베이션 주식회사 황화리튬 제조 방법
WO2025262067A1 (en) * 2024-06-19 2025-12-26 Specialty Operations France Process for preparing a powder of lithium sulfide
WO2026019439A1 (en) * 2024-07-18 2026-01-22 Kellogg Brown & Root Llc System and process for converting lithium hydroxide into lithium sulfide
CN120987268A (zh) * 2025-08-25 2025-11-21 无锡零一未来新材料技术研究院有限公司 硫化锂及其制备方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3510420B2 (ja) * 1996-04-16 2004-03-29 松下電器産業株式会社 リチウムイオン伝導性固体電解質およびその製造方法
JP3816141B2 (ja) * 1996-04-16 2006-08-30 古河機械金属株式会社 硫化リチウムの製造方法
JP4833539B2 (ja) * 2004-11-26 2011-12-07 日本化学工業株式会社 硫化リチウム粒子粉末、その製造方法および無機固体電解質
DE102007048289A1 (de) 2007-10-08 2009-04-09 Universität Siegen Lithium-Argyrodite
GB2464455B (en) * 2008-10-14 2010-09-15 Iti Scotland Ltd Lithium-containing transition metal sulfide compounds
JP6055770B2 (ja) * 2011-09-22 2016-12-27 出光興産株式会社 ガラス粒子
DE102012220428A1 (de) * 2011-11-09 2013-05-16 Chemetall Gmbh Li2S@C beschichtetes Lithiummetallprodukt, Verfahren zu dessen Herstellung und Verwendung
JP5701808B2 (ja) * 2012-03-30 2015-04-15 三井金属鉱業株式会社 硫化物系固体電解質の製造方法
JP2014041720A (ja) * 2012-08-21 2014-03-06 Idemitsu Kosan Co Ltd 全固体リチウムイオン電池及び正極合材
JP6179558B2 (ja) * 2015-06-12 2017-08-16 トヨタ自動車株式会社 リチウム組成物の製造方法および硫化物固体電解質材料の製造方法
CN105016310A (zh) * 2015-07-30 2015-11-04 广东先导稀材股份有限公司 一种高纯硫化锂的制备方法及装置

Also Published As

Publication number Publication date
AR110926A1 (es) 2019-05-15
AU2018214232B2 (en) 2020-06-25
IL268424B (en) 2021-03-25
BR112019015828A2 (pt) 2020-03-31
KR102485791B1 (ko) 2023-01-05
MX2019008901A (es) 2020-01-30
TWI748052B (zh) 2021-12-01
IL268424A (en) 2019-09-26
EP3577067B1 (de) 2025-11-19
EP4723293A3 (de) 2026-05-06
TW201840468A (zh) 2018-11-16
AU2018214232A1 (en) 2019-08-29
CN110475745B (zh) 2023-03-31
CN110475745A (zh) 2019-11-19
ZA201905012B (en) 2021-05-26
CA3050338A1 (en) 2018-08-09
ES3063468T3 (en) 2026-04-16
EP4723293A2 (de) 2026-04-08
EP3577067A1 (de) 2019-12-11
KR20190114977A (ko) 2019-10-10
US20200165129A1 (en) 2020-05-28
US11542162B2 (en) 2023-01-03
WO2018141919A1 (de) 2018-08-09

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