PL3605703T3 - Sposób wytwarzania elektrolitu stałego na bazie lgps - Google Patents

Sposób wytwarzania elektrolitu stałego na bazie lgps

Info

Publication number
PL3605703T3
PL3605703T3 PL18771992T PL18771992T PL3605703T3 PL 3605703 T3 PL3605703 T3 PL 3605703T3 PL 18771992 T PL18771992 T PL 18771992T PL 18771992 T PL18771992 T PL 18771992T PL 3605703 T3 PL3605703 T3 PL 3605703T3
Authority
PL
Poland
Prior art keywords
lgps
production method
solid electrolyte
based solid
electrolyte
Prior art date
Application number
PL18771992T
Other languages
English (en)
Inventor
Aki KATORI
Kotaro Kawakami
Masahiro Shimada
Yuki Takase
Tomohiro Ito
Original Assignee
Mitsubishi Gas Chemical Company, Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Gas Chemical Company, Inc. filed Critical Mitsubishi Gas Chemical Company, Inc.
Publication of PL3605703T3 publication Critical patent/PL3605703T3/pl

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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/056Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0561Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of inorganic materials only
    • H01M10/0562Solid materials
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/22Alkali metal sulfides or polysulfides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/14Sulfur, selenium, or tellurium compounds of phosphorus
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/547Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on sulfides or selenides or tellurides
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605Treating the starting powders individually or as mixtures
    • C04B35/6261Milling
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B1/00Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
    • H01B1/06Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances
    • H01B1/10Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances sulfides
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/82Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • CCHEMISTRY; METALLURGY
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    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201Alkali metal oxides or oxide-forming salts thereof
    • C04B2235/3203Lithium oxide or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
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    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3287Germanium oxides, germanates or oxide forming salts thereof, e.g. copper germanate
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3418Silicon oxide, silicic acids or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/42Non metallic elements added as constituents or additives, e.g. sulfur, phosphor, selenium or tellurium
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    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/44Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
    • C04B2235/444Halide containing anions, e.g. bromide, iodate, chlorite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5418Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5436Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5418Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5445Particle size related information expressed by the size of the particles or aggregates thereof submicron sized, i.e. from 0,1 to 1 micron
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5463Particle size distributions
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00Electrolytes
    • H01M2300/0017Non-aqueous electrolytes
    • H01M2300/0065Solid electrolytes
    • H01M2300/0068Solid electrolytes inorganic
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Ceramic Engineering (AREA)
  • Structural Engineering (AREA)
  • Materials Engineering (AREA)
  • Secondary Cells (AREA)
  • Conductive Materials (AREA)
  • Silicon Compounds (AREA)
PL18771992T 2017-03-22 2018-03-16 Sposób wytwarzania elektrolitu stałego na bazie lgps PL3605703T3 (pl)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2017055754 2017-03-22
JP2017173878 2017-09-11
PCT/JP2018/010373 WO2018173939A1 (ja) 2017-03-22 2018-03-16 Lgps系固体電解質の製造方法
EP18771992.7A EP3605703B1 (en) 2017-03-22 2018-03-16 Production method for lgps-based solid electrolyte

Publications (1)

Publication Number Publication Date
PL3605703T3 true PL3605703T3 (pl) 2021-10-25

Family

ID=63586010

Family Applications (1)

Application Number Title Priority Date Filing Date
PL18771992T PL3605703T3 (pl) 2017-03-22 2018-03-16 Sposób wytwarzania elektrolitu stałego na bazie lgps

Country Status (10)

Country Link
US (1) US10930973B2 (pl)
EP (1) EP3605703B1 (pl)
JP (1) JP6996553B2 (pl)
KR (1) KR102452778B1 (pl)
CN (1) CN110431703B (pl)
HU (1) HUE054696T2 (pl)
PL (1) PL3605703T3 (pl)
RU (1) RU2754868C2 (pl)
TW (1) TWI733998B (pl)
WO (1) WO2018173939A1 (pl)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20220123359A1 (en) * 2019-01-25 2022-04-21 Solid Power, Inc. Solid electrolyte material synthesis method
PL3936473T3 (pl) * 2019-03-05 2023-09-25 Mitsubishi Gas Chemical Company, Inc. Sposób wytwarzania siarczkowego elektrolitu stałego
US11799126B2 (en) * 2019-05-31 2023-10-24 Samsung Electronics Co., Ltd. Method of preparing solid electrolyte and all-solid battery including solid electrolyte prepared by the method
JP7402619B2 (ja) * 2019-05-31 2023-12-21 三星電子株式会社 固体電解質の製造方法
EP4092691B1 (en) * 2020-01-17 2025-04-23 Mitsubishi Gas Chemical Company, Inc. Method for producing sulfide solid electrolyte including sn
JP7400492B2 (ja) * 2020-01-22 2023-12-19 三菱瓦斯化学株式会社 硫化物系固体電解質の製造方法
JP2021150289A (ja) * 2020-03-17 2021-09-27 国立大学法人東京工業大学 硫化物固体電解質材料の製造方法
CN111463479B (zh) * 2020-04-10 2022-11-22 上海电气集团股份有限公司 固态电解质、复合固态电解质、锂离子电池及其制备方法和应用
CN117083684A (zh) 2021-04-07 2023-11-17 三菱瓦斯化学株式会社 Lgps系固体电解质的制造方法
JP7578571B2 (ja) * 2021-10-07 2024-11-06 国立大学法人東京科学大学 硫化物固体電解質、全固体電池および硫化物固体電解質の製造方法
WO2024014382A1 (ja) * 2022-07-11 2024-01-18 Agc株式会社 硫化物系固体電解質及びその製造方法、電極合剤、固体電解質層、並びに、全固体リチウムイオン二次電池
JPWO2024257743A1 (pl) 2023-06-12 2024-12-19
JP2025037080A (ja) * 2023-09-05 2025-03-17 トヨタ自動車株式会社 全固体電池および全固体電池の製造方法

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JP3433173B2 (ja) * 2000-10-02 2003-08-04 大阪府 硫化物系結晶化ガラス、固体型電解質及び全固体二次電池
JP2008535154A (ja) * 2005-03-22 2008-08-28 オクシス・エナジー・リミテッド 硫化リチウム電池およびこれを製造する方法
CN102823049B (zh) * 2010-03-26 2015-04-01 国立大学法人东京工业大学 硫化物固体电解质材料、电池和硫化物固体电解质材料的制造方法
RU2585252C2 (ru) * 2010-12-03 2016-05-27 Инмэт Глобал, Ллк Термостойкий слой для неводной и твердотельной батареи и способ его получения
WO2012176267A1 (ja) * 2011-06-20 2012-12-27 トヨタ自動車株式会社 二次電池用電極層、固体電解質層および全固体二次電池
JP5617794B2 (ja) 2011-08-08 2014-11-05 トヨタ自動車株式会社 硫化物固体電解質材料の製造方法、および、硫化物固体電解質材料
JP5880581B2 (ja) * 2012-02-06 2016-03-09 トヨタ自動車株式会社 硫化物固体電解質材料、電池および硫化物固体電解質材料の製造方法
JP5561383B2 (ja) * 2013-01-11 2014-07-30 トヨタ自動車株式会社 硫化物固体電解質材料、電池および硫化物固体電解質材料の製造方法
DE112014001986B4 (de) * 2013-04-16 2024-06-27 Toyota Jidosha Kabushiki Kaisha Sulfid-Festelektrolytmaterial, Batterie und Herstellverfahren für Sulfid-Festelektrolytmaterial
CN105518906B (zh) * 2013-05-15 2019-04-16 量子世界公司 用于使用LiAMPBSC的电池的固态阴极电解质或电解质(M=Si、Ge和/或Sn)
EP3007262B1 (en) 2013-06-07 2019-05-15 Toyota Jidosha Kabushiki Kaisha Sulfide solid electrolyte material, cell, and method for producing sulfide solid electrolyte material
JP6077403B2 (ja) * 2013-06-28 2017-02-08 トヨタ自動車株式会社 硫化物固体電解質材料の製造方法
JP2015050153A (ja) * 2013-09-04 2015-03-16 トヨタ自動車株式会社 全固体電池用積層体
JP6425426B2 (ja) * 2014-06-10 2018-11-21 三星電子株式会社Samsung Electronics Co.,Ltd. 硫化物固体電解質、および硫化物固体電解質の製造方法
US20150093652A1 (en) 2013-10-02 2015-04-02 Samsung Electronics Co., Ltd. Sulfide solid electrolyte, method of preparing the same, and solid state battery including the same
JP6678405B2 (ja) 2015-07-09 2020-04-08 国立大学法人東京工業大学 リチウム固体電解質
JP6742031B2 (ja) * 2016-03-11 2020-08-19 国立大学法人東京工業大学 硫化物固体電解質

Also Published As

Publication number Publication date
RU2019130768A3 (pl) 2021-05-28
KR102452778B1 (ko) 2022-10-07
HUE054696T2 (hu) 2021-09-28
KR20190127851A (ko) 2019-11-13
TW201842705A (zh) 2018-12-01
EP3605703A1 (en) 2020-02-05
JPWO2018173939A1 (ja) 2020-01-30
RU2019130768A (ru) 2021-04-22
JP6996553B2 (ja) 2022-02-04
CN110431703B (zh) 2022-03-22
EP3605703A4 (en) 2020-03-25
EP3605703B1 (en) 2021-04-21
RU2754868C2 (ru) 2021-09-08
TWI733998B (zh) 2021-07-21
CN110431703A (zh) 2019-11-08
US10930973B2 (en) 2021-02-23
US20200020977A1 (en) 2020-01-16
WO2018173939A1 (ja) 2018-09-27

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