PL404757A1 - Production method of (+) - 5- (1-hydroxy-3-methylbutyl) -4,4-dimethyltetrahydrofuran-2-one - Google Patents
Production method of (+) - 5- (1-hydroxy-3-methylbutyl) -4,4-dimethyltetrahydrofuran-2-oneInfo
- Publication number
- PL404757A1 PL404757A1 PL404757A PL40475713A PL404757A1 PL 404757 A1 PL404757 A1 PL 404757A1 PL 404757 A PL404757 A PL 404757A PL 40475713 A PL40475713 A PL 40475713A PL 404757 A1 PL404757 A1 PL 404757A1
- Authority
- PL
- Poland
- Prior art keywords
- dimethyltetrahydrofuran
- methylbutyl
- hydroxy
- production method
- production
- Prior art date
Links
- FRJSHMHNUJCAKL-UHFFFAOYSA-N 5-(1-hydroxy-3-methylbutyl)-4,4-dimethyloxolan-2-one Chemical compound CC(C)CC(O)C1OC(=O)CC1(C)C FRJSHMHNUJCAKL-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- UYMAOGRRVJRHMY-UHFFFAOYSA-N 5-iodo-4,4-dimethyl-6-(2-methylpropyl)oxan-2-one Chemical compound CC(C)CC1OC(=O)CC(C)(C)C1I UYMAOGRRVJRHMY-UHFFFAOYSA-N 0.000 abstract 1
- 244000286779 Hansenula anomala Species 0.000 abstract 1
- 241001632576 Hyacinthus Species 0.000 abstract 1
- 240000007472 Leucaena leucocephala Species 0.000 abstract 1
- 235000010643 Leucaena leucocephala Nutrition 0.000 abstract 1
- 239000002537 cosmetic Substances 0.000 abstract 1
- 238000006704 dehydrohalogenation reaction Methods 0.000 abstract 1
- 230000002255 enzymatic effect Effects 0.000 abstract 1
- 239000003205 fragrance Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 230000000813 microbial effect Effects 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
Landscapes
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
Wynalazek dotyczy sposobu wytwarzania (+)-5-(1-hydroksy-3-metylobutylo)-4,4-dimetylotetrahydrofuran-2-onu o wzorze 2, na drodze mikrobiologicznej dehydrohalogenacji i translaktonizacji substratu, przy uzyciu systemu enzymatycznego drozdzy z gatunku Candida pelliculosa. Jako substrat stosuje sie 5-jodo-4,4-dimetylo-6-(2-metylopropylo)tetrahydro-2H-piran-2-on. Produkt charakteryzuje sie zapachem kwiatowym z nuta hiacyntowo-akacjowa, dzieki czemu moga znalezc zastosowanie w przemysle kosmetycznym. The invention relates to a method for the production of (+)-5-(1-hydroxy-3-methylbutyl)-4,4-dimethyltetrahydrofuran-2-one of the formula 2 by microbial dehydrohalogenation and translactonization of the substrate, using an enzymatic system of Candida pelliculosa yeast . 5-iodo-4,4-dimethyl-6-(2-methylpropyl)tetrahydro-2H-pyran-2-one is used as the starting material. The product is characterized by a floral fragrance with a hint of hyacinth and acacia, thanks to which it can be used in the cosmetics industry.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL404757A PL221641B1 (en) | 2013-07-18 | 2013-07-18 | Method for preparing (+) -5 - (1-hydroxy-3-methylbutyl) -4,4-dimethyltetrahydrofuran-2-one |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL404757A PL221641B1 (en) | 2013-07-18 | 2013-07-18 | Method for preparing (+) -5 - (1-hydroxy-3-methylbutyl) -4,4-dimethyltetrahydrofuran-2-one |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL404757A1 true PL404757A1 (en) | 2014-01-20 |
| PL221641B1 PL221641B1 (en) | 2016-05-31 |
Family
ID=49920885
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL404757A PL221641B1 (en) | 2013-07-18 | 2013-07-18 | Method for preparing (+) -5 - (1-hydroxy-3-methylbutyl) -4,4-dimethyltetrahydrofuran-2-one |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL221641B1 (en) |
-
2013
- 2013-07-18 PL PL404757A patent/PL221641B1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PL221641B1 (en) | 2016-05-31 |
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