PL413441A1 - Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles - Google Patents

Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles

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Publication number
PL413441A1
PL413441A1 PL413441A PL41344115A PL413441A1 PL 413441 A1 PL413441 A1 PL 413441A1 PL 413441 A PL413441 A PL 413441A PL 41344115 A PL41344115 A PL 41344115A PL 413441 A1 PL413441 A1 PL 413441A1
Authority
PL
Poland
Prior art keywords
solution
suspension
chamomile
silver nanoparticles
prepared
Prior art date
Application number
PL413441A
Other languages
Polish (pl)
Other versions
PL234470B1 (en
Inventor
Agnieszka Sobczak-Kupiec
Dagmara Malina
Bożena Tyliszczak
Klaudia Pluta
Katarzyna Bialik-Wąs
Original Assignee
Politechnika Krakowska im. Tadeusza Kościuszki
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Krakowska im. Tadeusza Kościuszki filed Critical Politechnika Krakowska im. Tadeusza Kościuszki
Priority to PL413441A priority Critical patent/PL234470B1/en
Publication of PL413441A1 publication Critical patent/PL413441A1/en
Publication of PL234470B1 publication Critical patent/PL234470B1/en

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  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)

Abstract

Przedmiotem zgłoszenia są: sposób wytwarzania zawiesiny nanocząstek srebra i zawiesina nanocząstek srebra. Sposób wytwarzania zawiesiny nanocząstek srebra polega na redukcji soli srebra środkiem redukującym pochodzenia roślinnego, który to sposób charakteryzuje się tym, że jako środek redukujący stosuje się wywar, odwar lub ekstrakt z surowca zielarskiego: rumianku, przy czym redukcję prowadzi się w obecności polimerowego stabilizatora. Sposób obejmuje następujące etapy: a) sporządza się roztwór polimerowego stabilizatora w wodzie lub w rozpuszczalniku organicznym, po czym w roztworze tym rozpuszcza się sól srebra (roztwór A); b) sporządza się ekstrakt z koszyczków rumianku, korzystnie w tym samym rozpuszczalniku, w którym sporządza się roztwór A, przy czym stosunek wagowy koszyczków rumianku do rozpuszczalnika zawarty jest w granicach od 1 : 100 do 10 : 1 (roztwór B); c) roztwór B dodaje się do roztworu A, przy ciągłym mieszaniu, w temperaturze pokojowej lub podwyższonej maksymalnie do temperatury wrzenia rozpuszczalnika, przy czym stosunek objętościowy roztworu A do roztworu B zawarty jest w granicach od 1 : 100 do 100 : 1. W innym wariancie wykonania sposób wytwarzania zawiesiny obejmuje następujące etapy: 1) przygotowuje się roztwór polimerowego stabilizatora w wodzie lub w rozpuszczalniku organicznym i przy użyciu tego roztworu sporządza się napar lub odwar z koszyczków rumianku; II) do mieszaniny uzyskanej w etapie I) dodaje się sól srebra, podczas stałego mieszania w temperaturze pokojowej lub podwyższonej maksymalnie do temperatury wrzenia rozpuszczalnika. Zgłoszenie obejmuje także zawiesinę nanocząstek srebra, zawierającą surowiec zielarski rumianek, korzystnie w formie ekstraktu, naparu lub odwaru oraz polimerowy stabilizator, w której stężenie nanocząstek srebra korzystnie zawarte jest w przedziale od 100 mg/dm3 do 2000 mg/dm3.The subject of the application are: a method of producing silver nanoparticles suspension and silver nanoparticles suspension. The method of producing a suspension of silver nanoparticles consists in reducing the silver salt with a reducing agent of plant origin, which method is characterized in that as a reducing agent decoction, decoction or extract of herbal raw material: chamomile is used, the reduction being carried out in the presence of a polymeric stabilizer. The method comprises the following steps: a) a solution of the polymeric stabilizer is prepared in water or in an organic solvent, after which the silver salt (solution A) is dissolved in the solution; b) an extract of chamomile baskets is prepared, preferably in the same solvent in which solution A is prepared, the weight ratio of chamomile baskets to solvent being in the range from 1: 100 to 10: 1 (solution B); c) solution B is added to solution A, with continuous stirring, at room temperature or elevated to the boiling point of the solvent, with the volume ratio of solution A to solution B being in the range from 1: 100 to 100: 1. In another variant embodiment, the method of producing a suspension includes the following steps: 1) a solution of a polymeric stabilizer is prepared in water or an organic solvent, and with this solution an infusion or decoction of chamomile chamomile is prepared; II) The silver salt is added to the mixture obtained in step I) while continuously stirring at room temperature or raised to the maximum boiling point of the solvent. The application also includes a suspension of silver nanoparticles containing herbal raw material chamomile, preferably in the form of an extract, infusion or decoction, and a polymeric stabilizer in which the concentration of silver nanoparticles is preferably in the range from 100 mg / dm3 to 2000 mg / dm3.

PL413441A 2015-08-06 2015-08-06 Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles PL234470B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL413441A PL234470B1 (en) 2015-08-06 2015-08-06 Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL413441A PL234470B1 (en) 2015-08-06 2015-08-06 Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles

Publications (2)

Publication Number Publication Date
PL413441A1 true PL413441A1 (en) 2017-02-13
PL234470B1 PL234470B1 (en) 2020-02-28

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Family Applications (1)

Application Number Title Priority Date Filing Date
PL413441A PL234470B1 (en) 2015-08-06 2015-08-06 Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles

Country Status (1)

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PL (1) PL234470B1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11878043B1 (en) 2023-06-12 2024-01-23 King Faisal University Method for synthesizing silver nanoparticles from Amaranthus hybridus

Also Published As

Publication number Publication date
PL234470B1 (en) 2020-02-28

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